DEFORMATION BEHAVIOR AND CONSTITUTIVE EQUATION FOR Zr55Cu30Al10Ni5 BULK METALLIC GLASS IN SUPERCOOLED LIQUID REGION

Zr₅₅Cu₃₀Al₁₀Ni₅块体非晶合金(BMG)在过冷液态区内的单向压缩实验表明: 材料在过冷液态区内的形变行为强烈依赖于温度和变形速率. 随着应变速率的增加, 材料的流变特征由Newtonian流变转变为非Newtonian流变.利用扩展指数本构方程模型建立了非晶合金的流变应力、应变速率和温度的关系.     

时效处理对7A55铝合金微观组织和性能的影响

系统研究了时效处理对7A55铝合金微观组织演变和性能的影响。测试了其显微硬度、力学性能和电化学腐蚀性能,表征了透射组织和腐蚀形貌。试验结果表明:固溶处理后的7A55试验铝合金,具有高的硬化响应速率。经160 ℃×12 h时效处理后,显微硬度达到峰值,由固溶处理后的56 HV0.5提高到87 HV0.5,提高了55.36%,且前期的硬度升高速率极快。预时效(PA)处理抑制了试验7A55铝合金的自然时效(NA)效应,提升了烘烤硬化(BH)响应。经BH处理后,PA+NA态的屈服强度明显提升,达到475 MPa,硬化增量达到190 MPa,提高了66.67%,伸长率降低为12.5%。PA+NA+BH状态下,析出相粒子尺寸更为细小,粒子直径在10~15 nm范围,且分布均匀。PA+NA+BH态的合金腐蚀电位最高,为－1.032 V(vs SCE),腐蚀坑数量最少,平均腐蚀深度约为33 μm,最不易被腐蚀。     

55SiCr弹簧钢中的残留奥氏体与碳化物

通过扫描电镜(SEM)、电子背散射衍射(EBSD)、透射电镜(TEM)、X射线衍射仪(XRD)、热膨胀仪、洛氏硬度计等手段研究了弹簧钢55SiCr的组织和相变点以及残留奥氏体和碳化物在热处理过程中的组织演变。结果表明:55SiCr弹簧钢淬火后残留奥氏体以块状分布在基体上;随回火温度的升高,残留奥氏体减少并呈粒状和薄膜状分布;C在残留奥氏体中富集,使其稳定性增强;Si抑制了碳化物的析出,提高了残留奥氏体的稳定性。低温回火时,Si延缓了渗碳体析出;高温回火时,C原子扩散速率提高,促进渗碳体析出,引起体积的收缩。慢速加热回火时,C有足够的时间扩散,从而促进渗碳体的形成,使渗碳体的形成温度提前;快速加热回火时,C来不及扩散,抑制了渗碳体的析出。回火加热速率一样时,试验钢的硬度随回火温度的提高而下降。当回火温度为400 ℃时,硬度值最大为51 HRC;当回火温度为650 ℃时,硬度值最小为37 HRC。当加热速率为0.1 ℃/s时,硬度值最小为33 HRC;当加热速率为200 ℃/s时,硬度值最大为40 HRC。     

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利用电子背散射衍射(EBSD)测试技术对国产和进口两种优质弹簧钢55Si Cr的珠光体团尺寸、分布和轧制织构进行了对比分析。结果表明,两种优质弹簧钢中的珠光体团尺寸细小,平均值在6~8μm;国产优质弹簧钢的珠光体团小于10μm的比例达84%。这两种优质弹簧钢中均有3种晶粒取向存在,即<101>、<001>和<111>,国产优质弹簧钢的晶粒在<001>和<111>取向附近的比例较高,而进口优质弹簧钢在<101>取向上的织构强度偏弱。     

热浸镀55%Al-Zn合金镀层钢板的镀层结构及防腐蚀机理

阐述了热浸镀55%Al-Zn合金镀层钢板的镀层结构及其在实际生产中的形成过程,并分析了镀层特殊的防腐蚀机理.     

基于89C55和FPGA的频率特性测试仪

为了能够直接显示待测网络的幅频相频特性,设计了一个以89C55和FPGA构成的最小系统为控制核心的频率特性测试仪。系统基于DDS（直接数字频率合成）原理和多周期同步计数相位测量法,由信号发生器,被测双T网络,真有效值检波,相位检测,LCD显示及幅频特性曲线显示等部分构成。其中,信号发生和相位检测在FPGA内部实现。用户可通过按键输入需求,频率特性曲线实时显示于示波器上。整个系统性能稳定,界面友好,操作简单,实现了数字化频率特性分析。     

New Uni-Resonance Approximation Technique for Reaction Rate of Higher Resonances in Activation Detectors

As a high efficiency solid sample analysis technique based on resonance ionization spectroscopy (RIS). Resonant Laser Ablation (RLA) is available. RLA combines Laser Ablation (LA) and RIS simultaneously with a single laser device. We have proposed the new dosimetry technique for a solid sample based on RLA.

We have attempted the detection of ²⁶Al (T _1/2: 7.2×10⁵yr) produced in the high purity Al irradiated by 14MeV neutrons at Fusion Neutronics Source (FNS). Japan Atomic Energy Research Institute. Some interference effects are observed in the trace element detection experiments. These interference effects interrupt the detection of ²⁶Al. In conclusion. it is difficult that ²⁶Al is recognized clearly. We have mainly discussed the origins and elimination methods of these interference effects to detect the trace elements produced by nuclear reactions.     

石油套管用热轧钢带J55缺陷原因分析

对热轧钢带J55在制造石油套管时焊缝附近出现的细裂纹缺陷进行分析。结果显示,此类缺陷是由于连铸板坯原始缺陷经热轧轧制后形成的。     

GC determination of synthetic hydrocarbon-based thermal heating fluid in vegetable oils

A combination of alumina column chromatography and GC procedures was developed for the determination of synthetic hydrocarbon-based thermal heating fluid (trademarked as Therminol 55^™) in vegetable oils. In each run, 3 g of sample solution was loaded onto the alumina (50 g) column and was eluted with 200 mL hexane. The eluate was then concentrated to 1 mL with the aid of a nitrogen stream prior to GC analysis. The GC chromatogram of the thermal heating fluid was characterized by the presence of a bell-shaped hump that could not be resolved into individual peaks. The lowest detection limit based on various spiked palm olein samples was 20 μg/g. The CV obtained were 6.5–8.9% for the intra-day study and 8.1–9.7% for the inter-day study. Overall recoveries of these samples ranged from 68.0 to 85.7% and the method was found to be good enough for quality control purposes.     

基于TMS320C55x DSP的USB通信研究与固件设计

首先介绍了USB设备开发相关的USB1．1规范，随后重点阐述了SIE和固件的分工，最后给出了固件设计思路及关键点。