Early detection of ageing in solder joints through laser probe thermal analysis of the peltier effect

We have recently developed an optical contactless method for testing the quality of solder joints during accelerated thermal cycling ageing processes.¹ The method was based upon the measurement of the dynamic thermal behaviour of the joint to short bursts of Joule heating. It has proved to be efficient in revealing the formation of cracks at the lead-solder interface. We present a method to evaluate ageing at a much earlier stage in the cycling process. We have observed in earlier work,¹ that before cracks appear, structural changes occur in the solder at the lead-solder interface. The thermal response of the solder joint is recorded over time to a Peltier heat perturbation produced by flowing a current pulse through the interface where structural changes occur. The key point in this method is to discriminate the Peltier effect from the Joule thermal response because both effects generate heat. The variation of the early Peltier response in the thermal cycling ageing tests is seen as a quantitative signature of the structural changes in the lead-solder interface.     

轴端沟槽底部激光强化工艺参数优化研究

分析了选用不同激光能量密度对HT300进行表面强化处理时，材料表面呈现的四种状况；未相变硬化、相变硬化、表面微熔与表面熔凝的金相组织。根据工艺要求，选取相变硬化方法对轴端沟槽底表面进行处理。分析了工件激光处理方法并通过试验研究，寻找轴端沟槽底部激光强化工艺参数；激光功率（P）、光斑直径（D）及扫描速度（V）的优化组合。硬度测试及耐磨性能试验表明：激光相变处理和激光熔凝处理后轴端沟槽底部表面较表面感应淬火硬度分别提高7%和34%，绝对磨损体积分别下降了13%和25%。实践证实，对轴端沟槽底部激光相变硬化处理方法较其他表面处理方法工艺简单，加工工件符合技术要求，试验结果对零件表面处理提供了可靠依据。     

高性能2.5Gb／s用的DFB—LD／EA单片集成器件

报导了采用全ＭＯＣＶＤ生长的１．５５μｍ的单片集成ＤＦＢ＝ＬＤ／ＥＡ组件的 在ＤＷＤＭ系统上的传输测试结果，出纤功率Ｐｆ≥２．５ｍＷ＠Ｉｆ＝７５ｍＡ，边模抑制比ＳＭＳＲ〉３５ｄＢ，调制器反向偏压为２．５Ｖ时的消光比为１４ｄＢ，该发射模块在２．５Ｇｂ／ｓＤＷＤＭ系统上进行了传输试验，传输２４０Ｋｍ后无误码，其通道代价≤１ｄＢ＠ＢＥＲ＝１０＾－１２。     

Crystal orientation of β-phase isotactic polypropylene induced by magnetic orientation of N,N′-dicyclohexyl-2,6-naphthalenedicarboxamide

Melt crystallization of isotactic polypropylene (iPP), containing crystallites of N,N′-dicyclohexyl-2,6-naphthalenedicarboxamide (DCNDCA) as a nucleating agent of the the β-phase iPP crystal, is carried out under a magnetic field (6 T) to obtain the alignment of the iPP crystal induced by magnetic alignment of DCNDCA. In a previous paper, DCNDCA was reported to undergo magnetic alignment in a liquid suspension. The obtained iPP sample exhibits alignment of the β-phase crystal with the c-axis aligned perpendicular to the magnetic field. The comparison of this alignment of iPP with the reported magnetic alignment of DCNDCA indicates that the β-phase crystal grows epitaxially on the DCNDCA crystal. The (330)_β plane of the iPP crystal lies on the bc-plane of the DCNDCA crystal in which the direction of the c-axis of the iPP coincides with the direction of the b-axis of the DCNDCA crystal.     

Complete corrosion inhibition of lamellar zinc pigment in aqueous alkaline media

Lamellar zinc pigment reacts in aqueous alkaline media (e.g., water-borne paints) with the evolution of hydrogen. This corrosion reaction can be inhibited by 2-nitrophenol (2-NP), 2,4-dinitrophenol (2,4-DNP), 2-hydroxy-3,5-dinitro-benzoic acid (HDNBA) and 2-hydroxy-3-nitro-benzoic acid (2-H-3-NBA) which all have a nitro-group ortho to a hydroxy-group; this structural part of the inhibitors can be considered as a potential chelating group which may explain the corrosion inhibiting effect. As a rule, with triethylamine (TEA) as neutralizing agent corrosion inhibition is slightly better when compared to dimethylethanolamine (DMEA). With TEA there is complete corrosion inhibition with addition of 2,4-DNP at pH 8 and 10; with 2-H-3-NBA there is complete inhibition at pH 10.     

Stickiness, Functionality, and Microstructure of Food Powders

Three major aspects of food powder are described and discussed. Stickiness is one issue that can cause production and product handling difficulties. Stickiness has been interpreted in a number of ways and thus measured differently. Functionality of the primary (single) particles or agglomerated powders is of practical interest to the consumers. The desired quality will have to be matched or exceeded by the powder manufacturers. Finally, microstructure provides a key linkage between the production and the functionality. Its formation has impacts on both the stickiness and functionality.     

科研人员业绩考核设计

对科研人员业绩的考核，应具有一定程度可量化的考核指标和一套完整的考核体系。文章对科研人员业绩评价的内容及其指标体系、考核与管理办法进行了设计，认为科研人员业绩考核指标可以分为劳动数量、劳动质量和劳动成果3类，具体内容包括其科研工作量、科研责任、科研成果的表现形式及其数量、成果的学术价值与利用率，以及科研人员科研技能水平等。     

基于图像处理的炮管轴线直线度检测方法

在分析国内外直线度检测现状和比较了直线度测量的激光准直法、圆度法、杠杆法优缺点的基础上,提出了一种基于图像处理的炮管轴线直线度检测激光反射法.该方法通过激光器发出激光,经准直后射向分光镜,部分反射后射向测量元件.测量元件在炮管内移动并感知炮管实际轴线位置的变化.激光经反射后透射过分光镜到光靶上,CCD摄像机摄得光靶上被测信息的图像.经过图像处理及数据处理得出对应被测截面图像中的激光束中心,按照角度积累的公式计算出轴线直线度误差.同时论述了在Win98和VC++6.0环境下软件实现的步骤.实验结果表明该方法具有灵敏度高、测量速度快,对被测对象尺寸要求较低,适合在工厂内使用等优点.     

激光陀螺随机噪声参数估计和滤波方法研究

激光陀螺(RLG)中随机噪声是影响其精度的一个重要因素,针对其噪声的特殊性质,采用小波方法去除随机噪声,提高激光陀螺的精度。通过小波分析的参数估计方法获得噪声参数,并用小波阈值滤波方法去除噪声,对某型号的RLG的滤波结果表明了该方法的有效性。     

HHD型核子秤电离室物理性能检测

HHD型核子秤电离室已成功地使用于HCS型核子秤.对它的各种物理性能指标进行了检测,各项性能指标都达到了设计要求。