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71.
控制pH4-6,用锌粉还原氯化除汞上清液中的汞(Ⅱ)离子,取置换后液加入过量的硝酸银标准溶液,以硫酸铁铵溶液作指示剂,用硫氰酸钾标准滴定溶液滴定来测定氯量。该方法的检出限:0.25mg/100mL,回收率:98%-101%。 相似文献
72.
Chaosuan Kanchanomai Yukio Miyashita Yoshiharu Mutoh 《Journal of Electronic Materials》2002,31(5):456-465
Low-cycle fatigue (LCF) tests on as-cast Sn-3.5Ag, Sn-3Ag-0.5Cu, Sn-3Ag-0.5Cu-1Bi, and Sn-3Ag-0.5Cu-3Bi solders was carried
out using a noncontact strain-controlled system at 20°C with a constant frequency of 0.1 Hz. The addition of Cu does not significantly
affect the fatigue life of eutectic Sn-Ag solder. However, the fatigue life was significantly reduced with the addition of
Bi. The LCF behavior of all solders followed the Coffin-Manson relationship. The fatigue life of the present solders is dominated
by the fracture ductility and can be described by the ductility-modified Coffin-Manson’s relationship. Steps at the boundaries
of dendrite phases were the initiation sites for microcracks for Sn-3.5Ag, Sn-3Ag-0.5Cu, and Sn-3Ag-0.5Cu-1Bi solders, while
for Sn-3Ag-0.5Cu-3Bi solder, cracks initiated along both the dendrite boundaries and subgrain boundaries in the dendrite phases.
The linking of these cracks and the propagation of cracks inside the specimen occurred both transgranularly through eutectic
phases and intergranularly along dendrite boundaries or subgrain boundaries. 相似文献
73.
Optimal Conditions for Preparing Ultra-Fine CeO2 Powders in A Submerged Circulative Impinging Stream Reactor 总被引:1,自引:0,他引:1
Cerium carbonate powders were produced in a submerged circulation impinging stream reactor (SCISR) from Ce(NO3)3·6H2O. NH4HCO3 was used as a precipitant in the reaction. Cerium carbonate powders were roasted to produce ultra-fine cerium dioxide (CeO2) powders. The optimal conditions of such production process were obtained by orthogonal and one-factor experiments. The results showed that ultra-fine and narrowly distributed cerium carbonate powders were produced under the optimal flowing conditions. The concentrations of Ce(NO3)3 and NH4HCO3 solutions were 0.25 and 0.3 mol·L-1, respectively. The concentration of PEG4000 added in these two solutions was 4 g·L-1. The stirring ratio, reaction temperature, feeding time, solution pH, reaction time and digestion time were 900 r·min-1, 80 ℃, 20 min, 5~6, 5 min and 1 h, respectively. The final product, CeO2 powders, was obtained by roasting the produced cerium carbonate in air for 3 h at 500 ℃. The finally produced CeO2 powders were torispherical particles with a narrow size distribution of 0.8~2.5 μm. The crystal structure of CeO2 powders belonged to cubic crystal system and its space point group was O5H-FM3M. Under optimal conditions, powders produced by SCISR were finer and more narrowly distributed than that by Stirred Tank Reactor (STR). 相似文献
74.
F. H. Sam Froes 《Powder Metallurgy and Metal Ceramics》2007,46(5-6):303-310
The approaches to production of titanium powder injection molded parts are reviewed. Historically, oxygen levels have been
too high for structural use (particularly with the Ti-6Al-4V alloy). However, recent advances in starting powders, binders
and sintering facilities now allow oxygen levels in the Ti-6Al-4V alloy to be controlled to about 0.2 wt.% oxygen. This should
result in significant expansion of the titanium PIM market place into aerospace, automobiles, surgical instruments, dentistry,
communication devices (such as computers and cell phones), knives and guns.
__________
Translated from Poroshkovaya Metallurgiya, Vol. 46, No. 5–6 (455), pp. 118–125, 2007. 相似文献
75.
Wu Songping 《Microelectronics Journal》2007,38(1):41-46
The preparation of ultra fine nickel-copper bimetallic powder with two-stage chemical reduction method was investigated. Reductive sugar and hydrazine hydrate were employed as reducing agent in different reductive stage, respectively. Reaction of CuSO4·5H2O with reductive sugar at 70 °C gives cuprous oxide and copper particles, then as-prepared mixture and nickelous hydroxide were reduced by hydrazine hydrate, and nickel-copper powder having excellent dispersibility was prepared. Influences of nickel added on composition and dispersibility of powder were studied. TG/DTG/DTA of nickel-copper powder, which is stable in room temperature, were discussed with thermal analyzer. Relation of nickel content to oxidation temperature was investigated. Ni-Cu bimetallic powder particles have a fully coated structure when nickel content is up to 30%. As-prepared nickel-copper powder was applied in base metal electrode-multilayer ceramic capacitor (BME-MLCC). The end termination has high adhesion force, fairly good densification, low resistivity, excellent solderibility behavior and resistance behavior to soldering. 相似文献
76.
77.
激光焊接超细基胎体金刚石薄壁钻 总被引:6,自引:1,他引:5
采用激光焊接超细预合金粉胎体,开发了新的薄壁钻产品,通过对与现有的产品工艺、性能测试以及实际使用分析对比,结果表明:激光焊接与普通钎焊相比结合强度提高2-3倍,克服了胎体脱落问题,胎体耐磨性提高了50%-120%,其中轴向磨损速率提高1.2倍;钻削速度提高30.4%,工矿适应性增加,使用寿命提高25%-108%。 相似文献
78.
通过对AlSn20Cu/Steel双金属板(带)复合轧制过程变形区变形规律的分析,确定了轧制过程的总变形率与各分层变形率的关系,解决了实际生产中各分层原料的厚度匹配问题。 相似文献
79.
本文测算了自蔓延高温合成TiAl基合金粉末的爆炸烧结特性常数值:γ=1.44,lgβ=25.25,并为试验证实,这为获取大尺寸TiAl基合金提供了理论依据。 相似文献
80.
研究了添加高速钢粉对烧结钢组织与性能的影响。实验结果表明,含20%高速钢的烧结钢综合力学性能最好;添加高速钢粉能导致烧结钢密度减小的冲击韧性降低,当高速钢含量增中时,硬度随之增加,烧结钢中残余奥氏体和马氏体的含量与高速钢的含量呈线性关系。烧结钢中的马氏体显微硬度很高,它主要原高速钢粒子和原铁粒子的连接区域形成。 相似文献