Structural change in diamond by hydrogen plasma treatment at room temperature

The structural change of diamond induced by hydrogen plasma exposure at room temperature, and its thermal stability, were investigated using electron spin resonance (ESR), X-ray photoelectron spectroscopy (XPS) and Fourier transform infrared spectroscopy (FTIR) techniques. ESR observation revealed that it gave rise to a highly defective structure (spin concentration of 10²⁰ cm^{− 3}), which is very similar to the structure of hydrogenated amorphous carbon (a-C : H) confirmed by XPS and FTIR. Post-annealing was also carried out to clarify the thermal stability of the defects. The number of spin centers decreased with increasing annealing temperature, and eventually, the defective structure changed to a graphitic one by annealing at 800 °C.     

Shock-induced phase transition of oriented pyrolytic graphite to diamond at pressures up to 15 GPa

In studies of shock-induced phase transition of ordered pyrolytic graphite to a diamond-like phase, the lowest transition onset pressure was observed at 19.6 GPa. The phase transition in that case was considered to be martensitic. In the present study ordered pyrolytic graphite with voids between particles was loaded at pressures up to 15 GPa using a planar shock wave propagating along the basal plane of the graphitic crystal structure. As a result, both diamond-like carbon and diamond were observed in the postshock sample. The phase transition of graphite to diamond was assumed to occur by the release of distortional energy stored in the graphite particles, that is, diffusional-controlled reconstructive mechanism, on the basis of the data by high resolution electron microscopy together with electron energy loss spectroscopy.     

金刚石光电导探测器研制及在软X光测量中的初步应用

介绍了我们自己设计制造的天然Ⅱａ型金刚石光导探测器的结构，原理，制造工艺，实验标定及其在ＩＣＦ实验中软Ｘ光测量中的应用等。     

粉末冶金压机的应用与进展

简要介绍了当前国内以压制方法生产粉末冶金零件的企业所用压机的基本情况；国内粉末冶金压机生产与开发状况；现代国外知名品牌压机的技术特点与最新发展；分析和总结。     

等离子体化学气相法沉积金刚石薄膜

本文介绍和评述了化学气相沉积法制备人造金刚石薄膜及其进展。重点评述了反应机理、发展历史、沉积方法、补底材料、检测手段。论述了有利于形成立方晶系金刚石材料的沉积条件。     

Surface characterization of 6H-SiC (0001) substrates in indentation and abrasive machining

Surface characterization of 6H-SiC (0001) substrates in indentation and abrasive machining was carried out to investigate microfracture, residual damage, and surface roughness associated with material removal and surface generation. Brittle versus plastic deformation was studied using Vickers indention and nano-indentation. To characterize the abrasive machining response, the 6H-SiC (0001) substrates were ground using diamond wheels with grit sizes of 25, 15 and 7 μm, and then polished with diamond suspensions of 3 and 0.05 μm. It is found that in indentation, there was a scale effect for brittle versus plastic deformation in 6H-SiC substrates. Also, in grinding, the scales of fracture and surface roughness of the substrates decreased with a decrease in diamond grit size. However, in polishing, a reduction in grit size of diamond suspensions gave no significant improvement in surface roughness. Furthermore, the results showed that fracture-free 6H-SiC (0001) surfaces were generated in polishing with the existence of the residual crystal defects, which were associated with the origin of defects in single crystal growth.     

液压机工作缸缸底部分几种常见结构力学模型的统一

本文根据缸壁对于缸底弯曲变形具有一定支承刚度的概念，为法兰支承式液压缸四种常见的缸底结构建立了统一的力学模型和强度设计方法。     

挤压机机电控制系统研究

本文探讨了12．5MN轻合金挤压机的机电系统控制问题，对应用电液比例技术，伺服控制技术、模／数、数／模转换器及可编程控制器实现等温挤压的具体方法作了深入细致的研究，文中论述方法对挤压机的机电系统控制具有一定的普遍意义。     

液压机本体柔性化设计相关技术的研究

针对液压机本体设计特点，在液压机本体CAD应用系统的开发中，引入了柔性化设计的概念，以Pro／E为建模后台、VB6．0为操作语言，研究了柔性化设计的相关技术，并提出了相关解决方案，并为以：Pro／E为后台的应用系统的开发提供了一种可行方案。     

挤压机的振动分析和数值计算

本文建立了3150吨卧式挤压机振动分析的力学-数学模型,进行了数值计算,并绘出了相应的相轨线图。理论计算的结果与现场测试数据基本一致。这种用集中质量法建立模型及用相轨线图进行定性分析的方法对各种型式的挤压机、压力机设计研究均有普遍的参考价值。