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71.
The temperature programmed (palladium) hydride decomposition appeared very effective method for diagnosing the extent of alloying in Pd-Pt/SiO2 catalysts. Introduction of Pt to Pd catalysts moves the TPHD peak gradually towards lower temperatures and the shift in hydride decomposition peak is accompanied by a decrease in the amount of released hydrogen. The catalysts prepared the direct redox method showed much better alloy homogeneity than the samples prepared by coimpregnation. The results of probing with other techniques, i.e. catalytic probing with hydrodechlorination of CCl2F2 and XRD, were in line with TPHD data. The catalytic probing showed the presence of synergistic effect, a clear indication of Pd-Pt mixing. XRD data of post-reaction samples showed carbon incorporation into Pd-rich phase, whereas separate Pt-rich phase did not experience any bulk carbiding. 相似文献
72.
本文研究了用金属有机物热发解法制备PLT8薄膜的工艺过程和基片对薄膜结构的影响,并且给出了铁电性能的测量结果。 相似文献
73.
A new synthesis procedure for titanium-containing aluminosilicate zeolites has been obtained using a clear colloidal dispersion (sol) which was prepared with titanium isopropoxide, water, hydrochloric acid and colloidal silica, Ludox. When NaY, KL, offretite, mordenite and ZSM-5 zeolites were crystallized from the sol following conventional hydrothermal crystallization procedures, all the aluminosilicate zeolites showed the same X-ray absorption fine structure at the Ti K edge indicating framework Ti. The zeolites showed remarkable catalytic activity for the partial oxidation of cyclohexene using H2O2 as an oxidant and the photocatalytic decomposition of trichloroethene using water. 相似文献
74.
采用奇异值分解设计广义系统的最优滤波器 总被引:6,自引:2,他引:4
本文讨论广义离散随机线性系统的状态估计问题,通过矩阵奇值分解,本文给出了一种设计降阶最优滤波器的实用方法,该方法同时还得到了动态系统和量测系统的干扰噪声的估计。 相似文献
75.
The decomposition of NO and of N2O over a CuZSM-5 zeolite and a Fe-mordenite, respectively, has been studied using tracer techniques. The results demonstrate the high mobility of the lattice oxygen ions in self-diffusion. They afford a possible explanation for the problem of how two extralattice oxygens located at positions remote from each other may combine to form the O2 molecules which are spontaneously desorbed in these redox reactions. They show that a portion of the lattice oxygen mixes into the O2 released on decomposition. The data also show that N18O and N2
18O undergo exchange with the catalyst oxygen under reaction conditions.On leave from Central Research Institute for Chemistry, Hungarian Academy of Sciences, H-1525 Budapest, Hungary. 相似文献
76.
77.
Numerical simulations of acoustic scattering in the frequency domain based on hybrid methods coupling finite elements and boundary elements are the most suited for dealing with problems involving wave propagation in inhomogeneous media. Furthermore, it is necessary to resort to high performance computing to effectively solve the large size problems. However, the direct coupling yields a linear system with a matrix which is partly dense and partly sparse and thus not adapted to high performance computing. To avoid this difficulty, we present a new iterative method constructed from a non overlapping domain decomposition technique. 相似文献
78.
Yvon Maday Frédéric Magoulès 《Computer Methods in Applied Mechanics and Engineering》2007,196(8):1541-1553
In this paper an original variant of the Schwarz domain decomposition method is introduced for heterogeneous media. This method uses new optimized interface conditions specially designed to take into account the heterogeneity between the sub-domains on each sides of the interfaces. Numerical experiments illustrate the dependency of the proposed method with respect to several parameters, and confirm the robustness and efficiency of this method based on such optimized interface conditions. Several mesh partitions taking into account multiple cross points are considered in these experiments. 相似文献
79.
A method of processing complex signals in passive multi-element antenna arrays based on an analysis of the natural values of the correlation matrix of the signal is considered. By means of the method it is possible to substantially increase the output signal-to-noise ratio. An iterational process by means of which optimal estimators of both the signal and the amplitude-phase distribution may be obtained, is proposed. Theoretical estimators of the efficiency of the method are given. It is proved that, in terms of the efficiency, the approach considered in the article comes close to the technique of matched filtration. Results of statistical modeling that confirm the statistical results are presented. 相似文献
80.
B. E. Rytsar 《Cybernetics and Systems Analysis》2007,43(2):192-207
The paper considers the set-theoretical approach to the joint decomposition of systems of Boolean functions of variables specified
in different representation forms. The approach is based on the method of q-partitions of conjuncterms and concept of decomposition
clones. Theorems on joint decomposition of a system of full and partial functions are formulated. The approach is illustrated
by examples.
Parts I and II of this article are published in No. 5 (2001) and No. 1 (2002).
__________
Translated from Kibernetika i Sistemnyi Analiz, No. 2, pp. 39–58, March–April 2007. 相似文献