Light scattering studies on crystallization in polyethylene terephthalate

The light scattering from the spherulites of polyethylene terephthalate grown near the glass transition temperature has been investigated. The Hv scattering profiles can be reproduced by the sum of the ideal spherulite scattering with the distribution of spherulite radius and the isotropic scattering from randomly oriented crystallites. The ratio of optical anisotropies in the isotropic scattering to the ideal spherulite scattering is obtained by the method established to eliminate the effects of the number density of spherulites and the coefficient depending on the experimental conditions. It is found that the anisotropy ratio is almost independent of the crystallization time and of temperature above 106 °C, while it is larger at a crystallization temperature of 103 °C. The spherulitic structure is discussed in terms of the anisotropy ratio.     

Accurate Cross Sections for Microanalysis

To calculate the intensity of x-ray emission in electron beam microanalysis requires a knowledge of the energy distribution of the electrons in the solid, the energy variation of the ionization cross section of the relevant subshell, the fraction of ionizations events producing x rays of interest and the absorption coefficient of the x rays on the path to the detector. The theoretical predictions and experimental data available for ionization cross sections are limited mainly to K shells of a few elements. Results of systematic plane wave Born approximation calculations with exchange for K, L, and M shell ionization cross sections over the range of electron energies used in microanalysis are presented. Comparisons are made with experimental measurement for selected K shells and it is shown that the plane wave theory is not appropriate for overvoltages less than 2.5 V.     

胆甾相液晶的光学特性

基于胆甾相液晶的特殊分子结构，综合阐述了胆甾相液晶的旋光性、选择性光散射和偏振光二色性等光学特性，揭示了它的光学特性主要源于它螺旋状的分子结构及其光学各相异性。     

用改进的逐次逼近解法计算二维井间电磁场

提出了一种计算积分方程的新方法——改进的逐次逼近解法 (MSAM) ,并用该方法计算了轴对称二维井间电磁场。与传统的逐次逼近解法 (SAM)相比 ,该方法收敛性强 ,应用范围广 ,可适用于高电导率对比地层。由于不必进行直接的大型矩阵求逆运算 ,因此与积分方程的直接解法 (IE)相比 ,该方法计算速度更快 ,所需内存更少。采用矩阵求逆方法计算了成层介质中的二维 Green函数 ,并对含 Green函数的积分进行了简化 ,从而加快了计算速度。数值计算结果显示 ,在地层电导率对比度达到 2个数量级时 MSAM仍收敛 ,且计算结果与直接求解积分方程的结果一致 ,因此 MSAM是一种有效的计算轴对称二维井间电磁场的方法     

CVD金刚石膜生长过程的Raman分析

采用激光Raman散射分析法对CVD金刚石膜的生长过程进行研究 ,讨论在金刚石膜生长的不同阶段 ,膜内金刚石和非金刚石成分的相对含量及其残余应力的变化情况     

宽带抽运情况下乙醇、丙酮溶液中受激拉曼散射光谱的实验研究

研究了乙醇、丙酮两种拉曼介质在宽带抽运情况下啁啾激光脉冲的受激拉曼散射频谱特性 ,得到的一级Stokes光频谱宽度与抽运光基本相当 ,且具有较高的转换效率 ,从而表明了利用“展宽—受激拉曼散射—压缩”的办法获得波长近 1μm的飞秒级超短脉冲激光信号源的实验方案具有可行性     

用于测量空间温度场的分布式光纤传感器的系统设计

文中首先介绍了喇曼散射，并对分布式光纤温度传感器进行了理论分析，最后着重介绍我们研制的一种能够实际使用的喇曼散射分布式光纤温度传感器系统的设计和应用。     

Accurate depth profiling through energy-dependent pulse height deficit compensation in gas ionization detectors

The impact of the pulse height deficit effect in gas ionization detectors on the accurate extraction of depth information from heavy ion elastic recoil detection spectra has been investigated. Thin GaN films and Ge_xSi_1−x/Si heterostructures have been analyzed with a 200 MeV ¹⁹⁷Au beam. Employing an empirical parameterisation of the pulse height deficit, a global energy calibration of the detector can be achieved. Energy spectra have been compared, calibrated with either a constant or a full energy-dependent compensation for the deficit. A constant compensation results in significant distortion of the extracted depth profile for heavier ions, whereas an energy-dependent compensation yields true concentration–depth profiles.     

横流均匀环境中三维线源型正负浮力射流特性研究

本文利用混合有限分析法及交错网格。对横流均匀环境中三维线源型正负浮力射流及负浮力射流的特性进行研究，分析了不同工况下流速，温度和湍动能在断面上的分布及影响射流轨迹线的因素，讨论了轨迹线上温度的变化及浮力射流的贴壁现象。对三维长线源型负浮力射流，分析了流速比，喷口弗汝德数对负浮力射流的影响。     

动态光散射法研究海藻酸钠凝胶松弛行为

在前文的基础上，用相关函数轮廓分析的方法剖析了运动模型模式的复杂性。通过海藻酸钠水溶液在０．１ｍｏｌ／ＬＣａＣｌ２水溶液透析凝胶化过程中交联网络的松弛时间谱表明它不是单一的峰，有两上特征运动模式，并随透析向更慢的运动模式发展，这很慢的运动模式估计与区域的结构的生成有关。