High temperature controlled atmosphere experiments for catalysts in a transmission electron microscope

A new transmission electron microscopy (TEM) specimen preparation procedure for high temperature experiments using a controlled atmosphere specimen holder (HTCASH) has been developed. It is designed for studying the microstructure of catalyst specimens before and after treatments in various gases. The procedure involved (1) finding a new formula for the embedding material, (2) devising a new method of making specimen supports, and (3) developing a method for removing the embedding material after the specimen has been microtomed. These techniques were then brought together to produce the ideal specimens for the HTCASH experiments. As an extra benefit, this procedure is also suitable for preparing specimens for ultrahigh resolution imaging experiments. The application of the new procedure in HTCASH experiments is illustrated through a high temperature reduction of a Co/SiO₂-923 catalyst.     

The suitability of round clinching tools for high strength structural steel

The use of light gauge steel framing is increasing rapidly. New methods for joining frames are being sought. One of the most promising methods is clinching. Clinching has been used for almost 20 years. There has been much research into the method, the tools, suitable materials and applications. Few articles have been published concerning clinching of high strength structural steels, which are currently the most relevant materials for house construction.This study included 11 different clinching methods. In total, 469 test pieces were produced. Despite the high strength of the materials, all the clinching methods that were examined could be used satisfactorily. The most significant result was that a round tool is appropriate for all the materials tested. In fact, in comparison with results obtained using other types of tool, when the methods were ranked by maximum shear load capacity, the round design appeared in the top three classes seven times out of nine.     

挖金湾矿近距离煤层联合布置开采可行性研究

提出挖金湾矿近距离煤层联合布置开采方案，并对开采方案的技术难点进行了分析，找出了解决方法。     

电潜泵中压变频调速系统的改进

电潜泵中压变频器输出端产生高次谐波和脉冲电流 ,对电潜泵电动机的绝缘性能和轴承寿命造成不利影响。为此 ,提出 3项改进对策 :①采用谐振软性开关逆变电路 ,使功率开关器件在零电压条件下导通 ;②在变频器逆变输出端设置电抗滤波器抑制高次谐波电流 ;③改变电动机内部结构 ,如加大定子槽宽 ,增加转子导条尺寸 ,变星接法为星 角接法 ,采用绝缘轴承等。实践证明 ,采取改进对策后 ,不仅提高了电潜泵的产量 ,而且变频器滤波后电动机端的过电压明显减小 ,电潜泵和电缆的寿命延长     

建筑墙体表面传热系数辨识研究

对实验房间南向墙体内表面中心区域的换热过程进行实验，发现当风速在0－5．5m/s之间时，表面传热系数在8－18W（m^2.K）之间波动，而风向对墙体表面传热系数影响不大；用辅助变量法分析墙体表面传热过程，并结合实验推导出墙体表面传热系数。模型的预测结果与实测结果吻合良好。     

高压玻璃钢管道的研制及在油田中的应用

本文介绍了高压玻璃钢管道的特性及在我国油田的应用情况。     

Effects of hot-carrier stress on high performance polycrystalline silicon thin film transistor with a single perpendicular grain boundary

This paper is a report on the effect of a single perpendicular grain boundary on the hot-carrier and high current stability in high performance polycrystalline silicon (poly-Si) thin film transistors (TFTs). Under a hot carrier stress condition (Vg = Vth + 1 V, Vd = 12 V), the poly-Si TFT with a single grain boundary is superior to the poly-Si without any grain boundary because of the smaller free carriers available for electric conduction. The shift of transconductance in poly-Si TFT with a single grain boundary is less than 5% after hot carrier stress during a period of 1000 s. The shift of transconductance is about 25% in the case of the poly-Si TFTs without a grain boundary in the channel. On high current stress, the poly-Si TFT without the grain boundary is less degraded than the poly-Si TFT with the grain boundary because the concentrated electric field near the drain junction is lower.     

Preparation of CeO2-ZrO2 mixed oxide with high surface area and high thermal stability

Ceria-zirconia solid particles have been recognized as a key material of the automotive exhaust catalysts since they can release and uptake oxygen owing to the rapid reversible oxidation states of cerium between Ce³⁺ and Ce⁴⁺. Several methods have recently been described to prepare the CeO₂-ZrO₂ solid particles used in the catalysts. In this paper, a new coprecipitation method is used to prepare the CeO₂-ZrO₂ solid particles. The Ce-Zr alcogel is dried and calcined in flowing N₂ not in flowing air under atmospheric pressure. The results show that the ceria-zirconia sample calcined at 650 °C has high surface area over 90 m²g⁻¹, which drops to 40 m²g⁻¹ following treatment at 900°C.     

Experience, Context, and the Visual Perception of Human Movement.

Why are human observers particularly sensitive to human movement? Seven experiments examined the roles of visual experience and motor processes in human movement perception by comparing visual sensitivities to point-light displays of familiar, unusual, and impossible gaits across gait-speed and identity discrimination tasks. In both tasks, visual sensitivity to physically possible gaits was superior to visual sensitivity to physically impossible gaits, supporting perception-action coupling theories of human movement perception. Visual experience influenced walker-identity perception but not gait-speed discrimination. Thus, both motor experience and visual experience define visual sensitivity to human movement. An ecological perspective can be used to define the conditions necessary for experience-dependent sensitivity to human movement. (PsycINFO Database Record (c) 2010 APA, all rights reserved)     

计算机高速并行通信的实现方案

利用CPLD芯片实现单片机与ISA总线接口之间的高速并行通信，给出系统的总体设计方法及程序框图。采用这种通信方式，在12MHz晶振的MCS51单片机控制的数据采集系统中，可以满足与PCI04 ISA总线接口实时通信的要求，通信速率达200khit／s。在开发工具MAX plusⅡ下，完成了整个设计的输入、编译和仿真，达到了预期效果。本设计方案能够推广应用到计算机的高速并行通信中。