喷雾沉积快速凝固技术的发展与展望

喷雾沉积是制取大体积快凝材料的一种新工艺。本文综述了它的产生和发展，概述了其基本原理和过程控制。对该领域今后的发展动向，提出了一些新看法。     

High quality gate dielectrics formed by rapid thermal chemical vapor deposition of silane and nitrous oxide

In the present study, we have performed electrical characterization of oxides deposited via rapid thermal chemical vapor deposition using SiH₄ and N₂O. We have investigated the effect of temperature, pressure, and SiH₄ to N₂O ratio on the electrical and material properties of as-deposited films. We have found that as-deposited oxides deposited at low temperatures, low pressures, and with a low silane to nitrous oxide ratio of ～0.5% give good material and electrical properties. The as-deposited films are stoichiometric in nature and have high deposition rates. As-deposited films had very low D_it values, high breakdown fields, and excellent subthreshold swing. The leakage currents and metal oxide semiconductor field effect transistor current drive, although lower than thermal oxides, were found to be quite acceptable. We have also investigated the thickness dependence of the films and found that as the film thickness is reduced below 50Å, the reliability improves for all oxides including the silicon-rich deposited oxides.     

New Ferro Powder for Selective Laser Sintering of Dense Parts

The paper describes a new powder composition specially developed for selective laser sintering (SLS). The aim is to obtain a ferro powder that can be sintered without need for a (sacrificial) polymer binder and that results in quasi dense parts that do not need any post-processing like furnace sintering, infiltration or HIP. The powder is a mixture of different types of particles (Fe, Cu, Ni and Fe₃P). The composition and mixture ratio are justified by using phase diagrams. The powder has been tested using an own developed Nd: YAG SLS machine. The influence of process parameters (laser power, scan velocity, scan spacing and scan strategy) and the microstructural characteristics have been investigated. Attention is devoted to the binding mechanism (liquid phase sintering, through melting) and to the quality of resulting parts (density, balling effect,…).     

金属快速凝固方法的数学模型

本文综述了与几种典型的快速凝固方法相应的数学模型，并对每种模型作了相应的分析和评价。文中重点介绍了“活塞－砧法”，“双辊法”，“单辊法”和“雾化沉积法”数学模型的理论基础，建模过程，理论优缺点及实用局限性。     

Rapid Prototyping and Tooling of Custom-Made Tracheobronchial Stents

Rapid prototyping (RP) and rapid tooling (RT) techniques can be applied to the field of medicine primarily because of their ability to produce customised profiles and geometries in relatively short lead times. In this paper, the process by which these techniques can be applied for the production of customised tracheobronchial stents for the purpose of maintaining patency in an occluded respiratory tract is described. A comparison of RP systems was carried out to establish the preferred RP method to produce the master model. The vacuum casting RT process was then used to produce the stent.     

重油催化裂化反应技术的新进展

近十几年来，重油催化裂化技术作为主要的重质油轻质化手段得到了迅速发展，国内外围绕催化裂化装置的提升管反应器也开发了许多新技术。综述了重油催化裂化反应技术的新进展，并对新技术的开发进行了讨论。     

微机械谐振器的快速测试方法

为了缩短微机械谐振器的测量时间,提高测量效率.提出了一种针对压阻检测的微谐振器的频率特性测试新方法,该方法利用欧姆鉴相器,积分器和微处理器实现对微弱信号的有效检测.欧姆鉴相器以检测电阻为鉴相器,利用欧姆定律实现参考信号和被测信号的乘法鉴相运算;通过积分器实现对鉴相结果的积分运算,抑制干扰和噪声;微处理器用于对积分数据的...     

稀土钕对激光快速成形TC4合金组织及性能的影响

针对氢化脱氢钛合金粉末氧含量较高的问题，研究了添加稀土钕对激光快速成形TC4合金组织及性能的影响。结果发现，添加稀土Nd后，激光快速成形TC4合金的宏观晶粒尺寸变化不大；但随稀土添加量的增加，初始β列状晶逐渐转化为全β等轴晶，晶粒内部的魏氏α组织逐渐转变为网篮α，粗化α条不断增多，呈现团束聚集趋势，晶界α集束体积分数也不断增大；随稀土添加量的增加，激光快速成形TC4合金的室温塑性先大幅度提高，然后急剧降低；稀土添加量为0．1％～0．2％（质量分数，下同）时，氧含量为0．26％的氢化脱氢TC4合金粉末激光快速成形件沉积态的抗拉强度达975MPa，延伸率9．5％，满足锻件标准要求。     

铸态及快淬态无钴AB5型贮氢合金的循环稳定性

对AB5型LaxMm1-x(NiMnSiAlFe)49(x=0,0.45,0.75,1.00,摩尔分数)贮氢合金进行了快淬处理,研究了La含量及快淬工艺对合金微观结构及电化学循环稳定性的影响.结果表明:La含量的增加对铸态合金的循环稳定性没有明显影响,但使快淬态合金的循环稳定性下降,且快淬处理能显著提高合金的循环稳定性.当La替代量从0增加到1.00时,经300次充放循环后,铸态合金的容量保持率(Rh)从59.2%增加到59.8%;16 m/s淬速快淬态合金的容量保持率从83.9%下降到65.0%.对于x=0.45的合金,当淬速从0(铸态被定义为淬速等于0)增加到28 m/s时,容量保持率从59.8%增加到75.8%.