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171.
裂解汽油加氢一段催化剂失活原因分析 总被引:1,自引:0,他引:1
介绍了中国石油辽阳石化分公司烯烃厂裂解汽油加氢装置一段全馏分镍系加氢催化剂失活情况及原因分析。通过对酸性硫来源的分析及酸性硫对催化剂影响的评价,总结了处理酸性硫的对策及方法。 相似文献
172.
Sugarcane can be very susceptible to damage by freezes. Freeze-deteriorated cane can cause problems in processing and sometimes leads to a factory shut-down. This study was undertaken during the 2000/2001 harvest season to assess the cold tolerance performance of six commercial sugarcane varieties and to establish new and more sensitive criteria to measure cold tolerance. Two varieties CP 70-321 and CP 79-318, with known cold tolerance, were planted in the study as controls. The other varieties included LHo 83-153, LCP 85-384, HoCP 85-845 and HoCP 91-555. Freezing temperatures occurred on 20 December 2000 when the min. field temperature was −4.4 °C, and again on 21 December, 30 December through 5 January 2001, 9–10 January and 20–21 January. The lowest field temperature recorded was −5.6 °C on 4 January. Freezing conditions prevailed for 8–15 h during each freeze incident. Stalks of all varieties were frozen to the ground following the initial freeze, with freeze cracks evident only after the 4 January freeze. For this study, samples were taken on the date of the first freeze, 20 December, and subsequently again at 7, 14, 22 and 30 days after the first freeze. Criteria used to measure overall stalk cold-tolerance included changes in pH, Brix, dextran (ASI-II method), sucrose, glucose, and fructose concentrations. Mannitol, ethanol and the oligosaccharides, palatinose, leucrose, iso-maltotriose and 1-kestose, were simultaneuously measured using IC-IPAD. Marked differences were observed in most criteria for all varieties, particularly 22 and 30 days after the first freeze. Mannitol was strongly correlated (r2=0.84) with dextran, confirming its use as an indicator for cane dextran deterioration. In comparison, ethanol was only weakly correlated (r2=0.55) with dextran and did not always predict cane dextran deterioration. Iso maltotriose was the most sensitive oligosaccharide indicator of freeze deterioration, although both leucrose and palatinose could be used to confirm whether severe dextran formation (>1500 ppm/Brix) has occurred in cane. Isomaltotriose was strongly correlated (r2=0.89) with dextran and pH (r2=−0.83); pH was also a strong indicator of both dextran (r2=−0.85) and mannitol (r2=−0.92) formation. Four of the varieties, CP 79-318, LCP 85-384, HoCP 85-845 and HoCP 91-555, were shown to be susceptible to other sources of microbial and enzymic deterioration as well as dextran deterioration from Leuconostoc bacteria, especially 30 days after the first freeze. This was indicated by increased glucose/fructose ratios, ethanol formation, changes in 1-kestose concentration, and further sucrose losses. 相似文献
173.
侧重研究了破片式战斗部装药外形的优化设计技术。提出了装药外形与破片飞散特性(如破片飞散角,分布带宽等)之间的数学描述;建立了圆弧和对数螺线装药外形母线与战斗部其他设计参数间的数学模型。在假定约束条件下,优化设计了破片了聚焦式战斗部的结构参数;静爆试验结果表明,破片分布与理论计算吻合较好。 相似文献
174.
175.
Hexagonal AlN films have been obtained by arc ion plating at different negative biases ,X-ray diffraction and scanning electron microscopy results show that AlN films with smooth surfaces and (002) preferred orientation are obtained at low biases ,whereas those with coarse surfaces and (100) preferred orientation are obtained at high biases,The formation mechanism of AlN is analyzed and the experiment results are discussed,The effect of bias on adhesion strength has also been examined. 相似文献
176.
Electrochemical impedance spectroscopy was used for the study of two-component lipid membranes. Phosphatidylcholine (PC) and phosphatidylethanolamine (PE) were to be investigated, because of their presence in biological membranes. Capacitance values of pure components are 0.62 and 0.32 μF cm−2, respectively. The 1:1 complex was formed during formation of the PC-PE lipid membrane. Formation of the complex can explain the deviation from the additivity rule. This equilibrium was described by mathematical equations and was further verified experimentally. Adequate equations let us calculate such parameters as: capacitance of the complex molecule, area occupied by the complex molecule as well as the stability constant of the complex. 相似文献
177.
178.
Yu Zheng Haiyi Zhang Li Zhao Liujing Wei Xingyuan Ma Dongzhi Wei 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2008,83(10):1409-1412
BACKGROUND: 2,3‐Butanediol (2,3‐BD) is a valuable chemical that can be biosynthesized from many kinds of substrates. For commercial biological production of 2,3‐BD, it is desirable to use cheap substrate without pretreatment, such as starch. However, there have been few reports on the production of 2,3‐BD directly from starch. RESULTS: In this work, gene malS coding for α‐amylase (EC 3.2.1.1) precursor was inserted into plasmid pUC18K, and secretory over‐expression of α‐amylase was achieved by engineered Klebsiella pneumoniae. The extracellular recombinant amylase accelerated the hydrolyzation of starch, and one‐step production of 2,3‐BD from starch was carried out by engineered K. pneumoniae. A 2,3‐BD concentration of 3.8 g L?1 and yield of 0.19 g 2,3‐BD g?1 starch were obtained after 24 h fermentation. CONCLUSION: The one‐step production of 2,3‐BD from starch was achieved by secretory over‐expression of amylase in K. pneumoniae. This would simplify the process and reduce the production cost considerably by enabling use of starch with minimal pretreatment. Copyright © 2008 Society of Chemical Industry 相似文献
179.
以硫脲和水合肼合成了可用于检验醛的试剂——4-氨基-3-肼基-5-巯基-1,2,4-三唑(别名:紫醛),其结构通过红外光谱、核磁进行了确定。试验表明,紫醛对醛的检验敏感、专一、快速、操作简单。 相似文献
180.
HLA-DRB1等位基因主要参与人类的抗原免疫功能,对其进行比较研究,有助于追溯人类的进化迁移史,开发类群特异性药物.本研究以Matlab为平台,用自组织竞争网络(Self-Organizing Competitive Neural Network),对世界54个民族和人群、14个HLA-DRB1等位基因,进行了无监督模式分类.结果表明,各民族之间存在差异性,同民族的各人群之间有相似性.西伯利亚各人群,澳洲各土著人群,黑人各人群,南美印第安各人群,犹太族各人群,日本各人群,及欧美白人各人群有相对独立性:南美印第安人与西伯利亚人有高度相似性;中国民族在南方人群和北方人群间存在较大差异;中国汉族中,广东汉族地位特殊,与少数民族如拉祜族、瑶族关系密切. 相似文献