丙烯酸高碳醇酯的合成

介绍了降凝剂中间体丙烯酸高碳醇酯的合成和产品分离提纯方法。考察了合成条件对酯化反应的影响，结果表明，在原料丙烯酸与十八醇摩尔比1．2：1，阻聚剂对苯二酚用量占原料总量1．5％，催化剂对甲苯磺酸用量占原料总量1．5％，反应温度80-86℃，回流反应时间6h条件下，酯化率最高达89％。产品分离提纯方法与传统分离方法比较，所需分离时间短，洗涤用水量少，而产品收率远高于传统分离方法，达95％以上。     

Reducing Average and Peak Test Power Through Scan Chain Modification

Parallel test application helps reduce the otherwise considerable test times in SOCs; yet its applicability is limited by average and peak power considerations. The typical test vector loading techniques result in frequent transitions in the scan chain, which in turn reflect into significant levels of circuit switching unnecessarily. Judicious utilization of logic in the scan chain can help reduce transitions while loading the test vector needed. The transitions embedded in both test stimuli and the responses are handled through scan chain modifications consisting of logic gate insertion between scan cells as well as inversion of capture paths. No performance degradation ensues as these modifications have no impact on functional execution. To reduce average and peak power, we herein propose computationally efficient schemes that identify the location and the type of logic to be inserted. The experimental results confirm the significant reductions in test power possible under the proposed scheme.     

An introduction to Wu's method for mechanical theorem proving in geometry

Wu's algebraic method for mechanically proving geometry theorems is presented at a level as elementary as possible with sufficient examples for further understanding the complete method.The work reported here was supported by NSF Grant DCR-8503498.     

一种高速浮点加法器的设计实现

浮点加法器是协处理器的核心运算部件，是实现浮点指令各种运算的基础，其设计优化是提高浮点运算速度和精度的关键途径。文章从浮点加法器算法和电路实现的角度给出设计方法，并且提出动态与静态结合设计进位链的方案以及前导O预测面积与速度的折衷方法。动态与静态结合设计进位链的方法有效地降低了功耗，提高了速度，改善了性能。目前已经嵌入协处理器的设计中，并且流片测试成功。     

短半径水平井铰链式井下动力钻具组合力学模型的建立与分析

铰链式井下动力钻具组合是当前短半径水平钻井中最先进的一种新型工具。本文首先建立了铰接式井下动力钻具组合在二维井身条件下的力学模型并介绍了该模型的求解方法和过程,详细分析了若干结构学数、井身几何参数和钻井工艺参数对钻头侧向力的定量影响,为铰接式井下动力钻具组合的结构设计和短半径水平井轨道控制提供了力学分析基础。     

太阳电池板结构应力-应变状态分析

多层胶接是太阳电池板的结构特点,由于不同材料的弹性模量、热膨胀系数和泊松比不同,在温度场 作用下会产生热应力应变,在多次热交变过程中热应力．应变累积最后导致结构层间剥离,因此研究温度场作用 下太阳电池板结构应力应变状态具有非常重要的实际意义。本文推导了模拟太阳电池板结构应力-应变状态的一 维模型,该模型同样适用于分析多层胶接结构应力应变状态。     

Inside Front Cover: Three‐Dimensionally Ordered Gold Nanocrystal/Silica Superlattice Thin Films Synthesized via Sol–Gel Self‐Assembly (Adv. Funct. Mater. 7/2006)

The synthesis of three‐dimensionally ordered, transparent gold‐nanocrystal (NC)/silica superlattice thin films using the self‐assembly (by spin‐coating) of water‐soluble gold nanocrystal micelles and soluble silica is reported by Fan and co‐workers on p. 891. The robust, 3D NC/silica superlattice films are of interest for the development of collective optical and electronic phenomena, and, importantly, for the integration of NC arrays into device architectures. Nanocrystals and their ordered arrays hold many important applications in fields such as catalysis, surface‐enhanced Raman spectroscopy based sensors, memory storage, and electronic and optical nanodevices. Herein, a simple and general method to synthesize ordered, three‐dimensional, transparent gold nanocrystal/silica superlattice thin films by self‐assembly of gold nanocrystal micelles with silica or organosilsesquioxane by spin‐coating is reported. The self‐assembly process is conducted under acidic sol–gel conditions (ca. pH 2), ensuring spin‐solution homogeneity and stability and facilitating the formation of ordered and transparent gold nanocrystal/silica films. The monodisperse nanocrystals are organized within inorganic host matrices as a face‐centered cubic mesostructure, and characterized by transmission electron spectroscopy and X‐ray diffraction.