邻重氮萘醌改性酚醛树脂碱溶解特性的定量评价

本文提出了一种利用紫外—可见光分光光度仪定量评价高分子膜溶解速度的方法。并着重考查了邻重氮萘醌改性后的酚醛树脂在碱溶液中的溶解特性。实验表明,曝光后的树脂在碱溶液中首先溶胀,然后才开始溶解,即存在溶解滞后现象。溶解滞后和溶解速度与溶液的碱度有关,与树脂膜厚无关。     

高效防气防砂一体化管柱的研制与应用

为解决文南油田高气液比井出砂易造成卡泵的问题,研制了高效防气防砂一体化管柱。该管柱主要由闭式气锚、重力式防气装置和激光割缝筛管3部分组成。闭式气锚的分离作用消除了气体对抽油泵的影响,提高了泵效;重力防气装置利用液气分离原理和高烟囱原理进行液气分离,液流回流时间可达10min,排气最高压差可达0.2MPa;经激光割缝筛管过滤后的液体含砂粒外径小于0.05mm。该管柱在文南油田现场应用16井次,累计增液6000t,增油2717t,平均单井泵效提高7%。     

钢管内外表面喷砂除锈半自动生产线设计

介绍了钢管内外表面喷砂除锈生产线的主要设备、工艺流程及主要参数,电气系统总体方案设计和程序设计。用可编程序控制器控制钢管内表面喷砂除锈作业线,提高了自动化程度,操作方便,运行可靠,并给出了自动控制程序顺序功能图。本生产作业线实现了钢管内外表面的半自动喷砂处理,提高了产品质量,改善了工作环境。     

Effect of reliability of grounding of the shaft of a turboset on the operation of devices for control and protection of exciting circuits

Disturbance of the grounding of the shaft of a turboset or its absence for technical reasons can result in failure, misoperation, limitation of the operating zone, errors or limitation of the sensitivity of devices for control and protection of exciting circuits from single-point leakage, and electroerosion of elements of the turboset structure. Measures for increasing the reliability of the grounding of the shaft are discussed. __________ Translated from élektricheskie Stantsii, No. 3, March 2006, pp. 61–66.     

唐山建龙900mm冷轧机组的工艺与设备

较系统地介绍了我国第1条国产化的中宽带钢冷连轧生产线，即唐山建龙钢铁控股有限公司900mm冷连轧生产线的工艺流程、主要设备组成及技术特点。重点介绍了900mm 4机架六辊轧机的技术参数、性能特点及自动控制系统。该生产线投产以来，取得了较好效果。     

Analysis of trace mercury in water by solid phase extraction using dithizone modified nanometer titanium dioxide and cold vapor atomic absorption spectrometry

A new method for analysis of trace mercury in water samples was developed, based on the combination of preconcentration/separation using dithizone-modified nanometer titanium dioxide (TiO2) as a solid phase extractant and determination by cold vapor atomic adsorption spectrometry (CVAAS). Dithizone was dissolved with alcohol and loaded on the surface of nano-sized TiO2 powders by stirring. The static adsorption behavior of Hg2 on the dithizone-modified nanoparticles was investigated in detail. It was found that excellent adsorption ratio for Hg2 could be obtained in the pH range of 7-8 with an oscillation time of 15 min, and a 5 mL of 3.5 mol·L-1 HCl solution could quantitatively elute Hg2 from nanometer TiO2 powder. Common coexisting ions caused no obvious influence on the determination of mercury. The mechanisms for the adsorption and desorption were discussed. The detection limit (3σ) for Hg2 was calculated to be 5 ng·L-1. The proposed method was applied to the determination of Hg2 in a mineral water sample and a Zhujiang River water sample. By the standard addition method, the average recoveries were found to be 94.4%-108.3% with RSD (n = 5) of 2.9%-3.5%.     

织物树脂层压复合材料抗弹性能研究

针对防弹织物树脂层压复合材料的研制，考察了层压复合材料面密度，纤维类型，树脂体系，铺层混杂方式及纤维混杂分数，织物铺层，预置分层等因素对层压复合材料靶板弹道冲击性能的影响。     

硅粉/酚醛制备低成本碳化硅陶瓷复合材料

以低成本的硅粉和酚醛为原料 ,采用浆料浸渍 热压成型 反应烧结法制备了Cf SiC单向板 ,并对工艺条件进行了探讨。制备得到的单向板的弯曲强度达到 45 6 .8MPa ,断裂韧性达到 7.94MPa·m1 2 。     

钡酚醛树脂体系化学流变特性研究

在粘度实验和DSC热分析实验的基础上,对用于RTM工艺的钡酚醛树脂体系的化学流变特性进行研究,并根据双阿累尼乌斯方程建立树脂体系的流变模型。模型与实验结果具有良好的一致性。模型可揭示树脂体系在不同工艺条件下的粘度变化规律,定量预报RTM工艺树脂的低粘度平台工艺窗口,为合理制定RTM工艺参数、保证产品质量和实现工艺参数的全局优化提供必要的科学依据。     

硫脲树脂对Cu~(2+)吸附性能研究

考察了不同吸附时间、pH值和吸附温度下,聚对苯甲酰基硫脲树脂和聚酯基硫脲树脂对Cu2+的吸附性能影响;并对吸附动力学和热力学进行了研究。