Anhydrous esterification of myristic acid with propylene: Ion exchange resin and acid-treated clay as catalysts

Anhydrous esterification of myristic acid with propylene was carried out in the temperature range of 110–145°C and pressure from 190–195 psig in the presence of Amberlyst-15 (cation exchange resin) and Filtrol-24 (acid-treated clay) as catalysts. The product ester, isopropyl myristate finds use in cosmetic and topical medicinal preparations where good absorption through the skin is desired. Filtrol-24 is the catalyst of choice, and the recommended operating temperature is 130°C with a pressure of 190 psig.     

The effects of glycol methacrylate as a dehydrating agent on the dimensional changes of liver tissue

The dimensional changes of liver sections during the course of processing with glycol methacrylate (GMA) or with ethanol are described. Tissue processing with ethanol served as a control. During prolonged processing steps (24 h each), linear shrinkage of tissue specimens dehydrated with GMA at room temperature was 13.2%. Subsequent infiltration with GMA resulted in trivial swelling, and polymerization in slight shrinkage (2.3%). In comparison, processing with cold GMA resulted in shrinkage during dehydration (about 10.8%), a slight swelling in pure GMA, followed by shrinkage during polymerization (2.2%). Short routine processing schedules resulted in similar shrinkage/swelling patterns, although precise values differed slightly. In all experiments, ethanolic dehydration resulted in smaller dimensional tissue changes than did GMA dehydration. The dimensional changes of tissue sections during stretching on water, mounting and drying compensated for the major part of the shrinkage manifested during processing.     

山西铝厂锅炉水冷壁膨胀异常原因分析及对策

针对山西铝厂160t／h锅炉在实际运行中膨胀异常的问题，对不同的施工方法下，水冷壁膨胀量是否正常这一问题进行分析，找出了水冷壁膨胀异常的原因，并提出了解决对策。     

阳离子交换树脂铁中毒的复苏研究

软化器中使用的阳离子交换树脂容易受到铁离子的污染。采用均匀设计的方法,利用回归分析和最优化技术,研究了复苏剂中各组分对阳离子复苏效果的影响,得出了最佳复苏配方,开发出了一种新的复苏方法。这种方法具有腐蚀性低和复苏效果良好的特点,为生产现场树脂的复苏提供了有益的借鉴。     

J-199热熔胶膜的研制

讨论了不同VA含量不同熔体指数的EVA和各种增粘剂对热熔胶膜耐热性、软化点、剪切强度、拉伸强度、剥离强度等性能的影响。通过采用不同材料试验和配方的筛选，研制出一种90℃剪切强度0．07MPa、拉伸强度0．47MPa、耐热性好、粘接强度高的热熔胶膜，从而拓宽了热熔胶的使用范围。     

某炼油厂一级浮床除盐系统阳床工艺特性及调整试验

论述了某厂一级除盐系统阳床工艺特性及调整试验过程，对存在问题进行分析并改进，得到了实际运行最佳方式和参数，取得良好效果。     

中国冷库的现状与发展趋势

本文从的设计建造、制冷工艺和管理维护这三个方面，介绍了近三年来中国冷库的现状，说明中国冷库正朝着灵活、自动化、节能和环保的方向进一步发展。     

Phenol novolac/poly(4- hydroxyphenylmaleimide) blend hardeners for DGEBA-type epoxy resin

Phenol novolac/poly (4-hydroxyphenylmaleimide) (PHPMI) blends were used as an epoxy resin hardener. The curing behavior of the above system and the thermal and mechanical properties of the cured epoxy resin were studied. It was not necessary to use a curing accelerator for this system, because PHPMI caused acceleration of the curing reaction. The curing mechanism of this system was investigated by using model compounds. Test pieces from the neat resins and the glass fiber reinforced resins were evaluated in terms of thermal and mechanical properties, respectively. It was found that heat resistance and mechanical properties were improved by increasing the amount of PHPMI in the hardener.     

树脂悬浮光度法测定微量银

在ｐＨ６．９的缓冲溶液中，银与硫代米Ｃｈｉ酮（ＴＭＫ）形成的螯合物在树脂甘油相中悬浮富集，用光度法测定银在波长４６１ｎｍ处有最大吸收，银在０～６μｇ／１０ｍＬ范围内遵守比尔定律，可用于样品中微量银的测定。