A new precipitate phase in Al-4wt. % Cu thin-film interconnects

We report here the identification of a new precipitate phase in thin-film Al-4wt.%Cu metallization used for interconnects on integrated circuits. The phase is based on a trigonal distortion of a face centered cubic lattice. Computer simulation of electron diffraction intensities suggests that the basis structure is isomorphous with Al₂Ca but with a large and ordered population of vacancies on Cu sites. The reason for the formation of the new phase and its implications for electromigration reliability are discussed.     

Rapid analysis of polymer homologues and additives with SFE/SFC-MS coupling

A rapid and easy analysis method for polymers is presented. The method involves sample preparation by SFE, separation of the extracted compounds by SFC and simultaneous quantitative detection by FID, as well as identification of unknowns by MS. The applications illustrate how structural research work and routine polymer analysis can be done with this time saving method.     

硼酸使掺铁铝酸锂发光增强的现象

在硼酸存在下合成了掺铁铝酸锂荧光体,研究了在不同温度下硼酸加入量对荧光体发光强度的影响,并通过X射线粉末衍射和粒度分析,初步探讨了发光增加的原因。     

Application of SiC-Si functionally gradient material to thermoelectric energy conversion device

Because of its high–temperature chemical stability, SiC ceramic is a promising material for high-temperature device applications such as thermoelectric energy converters. However, the electrical conductivity of SiC ceramic is too low for it to be used as a thermoelectric energy converter at the cold junction. Therefore, we propose a SiC-Si functionally gradient material (FGM) in order to improve the electrical conductivity of the SiC ceramic at the cold junction. An SiC rod was fired in a temperature gradient furnace. One end of the SiC rod was maintained at 2473 K and the other end was maintained at 1973 K for 30 min. After firing, the porous SiC edge fired at 1973 K was dipped into molten Si in order to infiltrate molten Si into the porous SiC. The microstructure of the FGM is classified into three regions: the SiC-Si composite material; the porous SiC ceramic; and the densified SiC ceramic. The electrical conductivity, the Seebeck coefficient and the thermal conductivity for each region of SiC-Si FGM was measured at 300 K; a figure of merit was calculated. The figure of merit of the SiC-Si FGM at the cold junction, at room temperature, was 10⁸ times higher than that of a nongradient SiC ceramic.     

树脂热解炭制备碳化硅晶须

用自制的配合醛树脂热解和炭源，用ＳＩＯ２超细汾作原，根据碳热还原原理，利用常规加热和微波加热两种方式，分别制备了直径在纳米级的ＳｉＣ晶须，Ｘ射线衍射、透射电检测结果表明：制备工艺和条件对ＳｉＣ晶须的性质有较大的影响。     

Pb（Sc1／2Ta1／2）O3铁电体的有序结构和介电性质）

通过铌铁矿预合成法制备Ｐｂ（Ｓｃ１／２Ｔａ１／２）Ｏ３（ＰＳＴ）陶瓷，经适当的热处理获得了钙钛矿化合物Ｂ位离子的高有序和高无序试样，ＰＳＴ陶瓷的介电性质研究结果表明，高有序试样（Ｓ＝０．７７）的居里温度为２９℃，并具有较低的介电常数表现出普通铁电体性质特征，而高元序试样（Ｓ＝０）具有很高的介电常数，并表现出明显的弥散性相转变和Ｔｍ的频率色散行为，即高介电常数的驰豫铁电体性质。文中还利用ＸＲＤ，ＳＥ     

随钻气侵检测仪在胜利油田的应用

简要介绍了随钻气侵检测仪的结构特点、工作原理、现场模拟试验及应用情况。中原油田全尺寸实验井和胜利油田６口井的现场试验及应用结果表明，该仪器能实现早期气侵检测，比常规方法检测到气侵的时间明显提前，对高压气井和复杂地层井控具有重要的现实意义。     

Development of an integrated model for airflow in building spaces

In building energy simulation, an integrated modelling of airflow in the building needed. Therefore, in this paper two approaches are used for building energy simulation: zonal network for modelling of the building segments and Computational Fluid Dynamics (CFD) for modelling of the airflow. It is noted that a synchronize solution process is needed for the building and the CFD equation-sets. For this purpose an iterative procedure is used to corresponding solution of these equations.     

基于故障树与灰关联分析的鱼雷故障诊断

将灰色关联度与故障树联合运用于鱼雷故障诊断,为鱼雷的故障诊断提供了一种新途径。在鱼雷动力系统故障树诊断模式识别中,运用灰色系统理论中的灰关联分析,通过进行关联度计算及排序,对各种故障模式发生的可能性大小作出了判断,从而为处理故障的轻重缓急、控制故障的发生以及改进系统的可靠性提供了理论依据。实例诊断表明,这种方法是有效可行的,并且诊断结果可靠。     

环境友好油层保护钻井液的研究及应用

针对江苏油田地层特性和地面生态环境具体情况开展了钻井液防塌性能、油层保护与环境保护的协同研究。在研制和筛选能满足环境保护要求的钻井液处理剂如润滑剂、降滤失剂和油层保护剂等的基础上,通过配方优化研制出了环境友好油层保护钻井液体系,并进行了防塌、油层保护、裂缝封堵等性能的室内评价。评价结果表明:该钻井液体系具有较强的抑制泥页岩膨胀和分散能力,渗透率恢复值大于85%,润滑性及滤失性好,而且无生物毒性,化学毒性低,易生物降解。应用该钻井液体系在江苏油田AF地区进行了现场试验,现场应用表明,该钻井液体系防塌性和油层保护效果好,各项环境指标达到农用污染标准,可直接排放,从源头控制了钻井液的污染,可进一步推广应用。