Fracture behaviour of 8%Ni 980 MPa high strength steel at various temperatures Part 3 – Four-point notched bend tests

Abstract

Based on the results of four-point notched bend tests together with detailed microscopic observations of fracture surfaces and crack configurations below the unbroken notch roots of double notch specimens, the fracture mechanisms in notched specimens of 8%Ni high strength (980 MPa) steel have been observed to be as follows. A fibrous crack initiates in the bainitic matrix at the notch root and then develops into a cleavage crack at a critical length. The cleavage crack propagates in an unstable manner and causes the final fracture of specimen. The critical event controlling the cleavage fracture is the propagation of the bainitic packet-sized crack, and the local fracture stress is measured as around 1845–2200 MPa.     

Effect of Nb on Mechanical Properties of HAZ for High-Nb X80 Pipeline Steels

The mechanical properties of heat affected zone (HAZ) of two commercial high-Nb X80 grade pipeline steels with different alloy elements were investigated using thermal simulation performed on a Gleeble-3500 thermal simulator. The results showed that the high-Nb steels have excellent weldability. Embrittlement regions appear in coarse grain heat affected zone (CGHAZ) and intercritically heat affected zone (ICHAZ); Softening region appears in fine-grain heat affected zone (FGHAZ), and the strength here was even lower than 555 MPa as required in the standard. Meanwhile, with the increase of heat input, the strength and the toughness of HAZ of steel with high Nb, C and lower alloy decrease notably. Therefore, take into account the welding procedure during manufacture of weld pipe, suitable amount of alloy elements, such as Cr, Ni, Cu, Mo and so on, is necessary for high Nb X80 heavy-thick steel plate.     

高分辨ICP-MS测定电子级高纯异丙醇中杂质元素

利用高分辨电感耦合等离子体质谱测定电子级高纯异丙醇中的痕量金属杂质,用膜去溶进样系统直接进样,用标准加入法进行上机检测,无需前处理、快速,避免了在样品前处理时的污染问题。高分辨电感耦合等离子体质谱可以消除多分子离子干扰,降低检出限,提高定量准确性。方法的检出限为0.45~20.79 ng/L,加标法回收率为88.2%~102.6%。方法简单,结果可靠,适用于高纯异丙醇中痕量元素的快速测定。     

城市配网规划电压等级合理配置及经济比较

通过建立电压等级与投资、运行成本的函数关系,以成本最小为原则对电压等级进行优化。提出了考虑经济性因素的＂几何均值＂原则,并从经济性角度对电压等级序列优化提出数学模型。     

铜矿床一般工业指标研究

针对2002年铜地质勘查规范中一般工业指标存在的问题,基于大量实际生产数据,对铜矿床实际采用的边界品位指标、最低工业品位、矿床平均品位、最小可采厚度、夹石剔除厚度、开采技术条件等进行研究,论证了铜矿床的一般工业指标,并首次明确了铜矿床工业指标的适用条件,解决了铜矿床一般工业指标体系应用不一致和指标区间取值主观性的问题。     

Improvement of Grain Size and Dome Height of Microalloyed Steels Using Taguchi Method Based on Grey Relational Grade in Controlled Rolling

An efficient approach was introduced for improving the condition of major controlled rolling process parameters of roughing, finishing and coiling temperatures and optimizing these parameters to obtain minimum grain size and maximum dome height simultaneously. Taguchi method combined with grey relational analysis was applied to achieve optimum grain size and dome height during controlled rolling process. For this purpose, four levels for the above temperatures were chosen and sixteen experiments were conducted based on orthogonal array of Taguchi method. Based on Taguchi approach, signal-to-noise (S/N) ratios were calculated and used in order to obtain the optimum levels for every input parameter. Analysis of variance revealed that finishing and coiling temperatures have the maximum effect on the grain size and dome height of microalloyed steels. The confirmation tests with the optimal levels of parameters indicated that the grain size and dome height of controlled rolled microalloyed steels can be improved effectively through this approach.     

对《屋面工程技术规范》（GB50345-2012）中若干问题的理解

新修订的《屋面工程技术规范）（GB50345--2012）已由住建部于2012年5月批准发布，并于2012年10月1日起实施。新规范在原规范的基础上进行了较大的修改，包括屋面工程设计、施工按构造层划分章节，修改了屋面防水等级，取消了防水层合理使用年限和刚性防水屋面，增加了消防、节能的有关条文，补充了金属板屋面、玻璃采光顶等新内容。本文对新规范中若干重大修改理由作了较详细的阐述。     

竞技二打一游戏中同等牌力的研究

全国竞技二打一扑克锦标赛是国家体育总局棋牌运动管理中心推出的新兴项目，比赛采用复式赛赛制，然而这种赛制存在无法杜绝线上比赛作弊的问题，为此提出用同等牌力赛制来代替复式赛制进行比赛的设想。本文主要针对如何判定和选取具有同等牌力的初始手牌进行研究，提出用等级难度评估指标来计算初始手牌的难度，初始手牌难度相近的牌认定为同等牌力，并给出了同等牌力的选取方法；为保证一副牌所得等级难度评估指标的可靠性，提出用多个不同水平的“二打一AI程序”来代替真人打牌产生牌谱的方法。实验证明了同等牌力生成方法的有效性，本文提出的同等牌力方法应用于比赛是可行的。     

鲕状赤铁矿微波碳热还原-磁选提铁脱磷实验研究

采用微波碳热还原-磁选工艺对鲕状赤铁矿提铁脱磷进行了研究,考察了还原温度、碱度、添加剂用量和原矿粒度等因素对提铁脱磷效果的影响。结果表明,最佳还原条件为:还原温度1 150 ℃、碱度0.8、配碳量1.0、钠盐添加剂用量15%、原矿粒度0.15 mm;将还原所得球团磨至-0.15 mm,在65 mT磁场强度下磁选,可得到全铁含量87.98%、铁回收率95.48%、脱磷率69.42%的指标。     

Effect of bacterial inoculum ratio in mixed culture for decolourization and detoxification of pulp paper mill effluent

BACKGROUND: Effluent released from industry is a mixture of various pollutants. For the degradation of complex pollutants, mixed bacterial cultures can be more effective than a single culture. This study investigated the balance of bacterial populations in a mixed culture for maximum reduction of pollutants. RESULTS: This study deals with the degradation and detoxification of pulp paper mill effluent (PPME) by three bacterial strains, i.e. Serratia marcescens, Serratia liquefaciens and Bacillus cereus in different ratios, and found that two ratios, 4:1:1 and 1:4:1, were effective for the degradation of PPME. These ratios reduced the various pollution parameters. Enzyme bioassay revealed that more enzyme was produced during degradation for the ratio 4:1:1. High performance liquid chromatography (HPLC) analysis showed that the ratio 4:1:1 degraded 95% of lignin and related compounds, and chlorophenols up to 98%, whereas ratio 1:4:1 reduced lignin by 84% and chlorophenols by 58% after 7 days incubation. Degradation products were confirmed by gas chromatography–mass spectrometry (GC‐MS) analysis. A seed germination bioassay on Phaseolous mungo L. revealed that toxicity was reduced by the ratio 4:1:1. CONCLUSION: Due to variable potential of different bacteria show variation in their growth pattern at any contaminated site. This study shows that an appropriate ratio of mixed cultures is required for maximum degradation and detoxification of PPME. Copyright © 2012 Society of Chemical Industry