阀门内漏单声波传感器监测方法研究

针对阀门内漏模拟和阀门内漏监测问题，提出了阀门内漏模拟和阀门内漏非介入式单声波传感器监测方法。设计了由法兰、薄纸片和带孔铝片组成的虚拟阀门，可真实地模拟阀门内漏瞬态过程，克服了传统阀门内漏模拟方法中存在的各种缺点。分析、比较了不同条件下阀门上下游声波传感器输出信号的频域特征，验证了阀门上游声波传感器设置的冗余性和基于单声波传感器实现阀门内漏监测的可行性。分析、比较了不同条件下单声波传感器输出信号的时频域特征，提出了基于峰值系数和小波包能量分率的阀门内漏时频域特征提取方法，并以阀门密封良好状态下的声波信号为样本，建立了基于SVDD的阀门内漏诊断模型。测试结果表明：本文提出的单声波传感器阀门内漏监测方法可行、模型诊断准确，且具有较强的抗干扰能力和较高的阀门内漏检测灵敏度。     

Plastic deformation of ZnO thin films through edge and screw dislocation movements

Columnar wurtzite grains were formed in sputtered ZnO thin films deposited on a plastic polyethylene terephthalate substrate. Selected-area diffraction patterns reveal that the columnar grains in the sputtered films present two preferred growth planes, namely, the basal (0002) and prismatic (100) growth planes. The diffraction patterns obtained also confirm that the microstructure of sputtered indium tin oxide thin films is amorphous in nature. Tensile tests indicate that the fracture strain of the ZnO thin film occurs between 1.73% and 2.14%, while the fracture strain of the indium tin oxide thin film occurs between 0.24% and 0.67%. Thus, the fracture toughness of the sputtered ZnO thin film is greater than that of the sputtered indium tin oxide thin film. High-resolution transmission electron microscopic images demonstrate that edge and screw dislocations could be identified in the sputtered ZnO thin films. Moreover, edge and screw dislocation movements may, respectively, be observed in the basal- and prismatic-oriented ZnO columnar grains of the sputtered ZnO thin films. Our results indicate that movements of the edge and screw dislocations in the basal- and prismatic-oriented ZnO columnar grains account for the plastic deformation of the investigated ZnO thin films under tensile stress.     

Growth of β-Alumina (Na2O · 11Al2O3) Single Crystals by the Flux Method

The crystal-growth process and growth conditions of β-alumina (Na₂O · Al₂O₃) were investigated using the Na₂B₄O₇-Na₃AlF₆ flux method. β-Alumina (electric fusion brick) was used as both nutrient and seed. Weight loss of the flux varied widely for various runs: ≅ 10 wt% of flux evaporated at 100 h, ≅ 17 wt% at 150 h, and 43 wt% at 600 h. When β-alumina crystal was grown, only 20 wt% Na₂B₄O₇ was added to the Na₃AlF₆ flux. The linear growth rates of the β-alumina single crystal grown by an Na₃AlF₆-20 wt% Na₂B₄O₇ flux method at 1040°C and Δ t = 18°C were ≅ 1.0 × 10⁻³ mm/h ( a face) and ≅0.3 × 10⁻³ mm/h ( c face). The β-alumina single crystals grown were bounded by only c [001] and a [100] and were colorless and transparent.     

软件体系结构风格及其应用

本文以一个生产安全受控系统的开发为例,讨论了软件体系结构风格及其应用,首先介绍了通用架构风格,然后根据炼厂规模、工作性质、人员类型的特点,合理分析并选择了架构风格,从总体结构上满足需求,系统主体基于服务的分布式架构风格,在服务子系统中使用B/S、分层结构风格,在PDA子系统采用事件驱动风格,有效地指导系统的设计和开发,降低了系统的维护成本,提高了系统的可重用性。最后分析了实施效果和不足之处,以及改进方法。     

Influence of processing on ethylene propylene block copolymers (II): Fracture behavior

The present work investigates the relationships between the microstructural state and fracture properties in commercial polypropylene‐based materials. In this case an isopolypropylene homopolymer and three ethylene propylene block copolymers (EPBC) with different ethylene content (EC) have been studied. A variety of morphologies were obtained by a combination of several processing methods (injection molding, injection molding‐annealing, and compression molding) and thickness. Fracture behavior of deeply double‐edged notched specimens was evaluated by scanning electron microscopy (SEM) and by the essential work of fracture (EWF) method, analyzing the influence of processing, thickness (t), EC, and orientation respect to melt flow direction (MD and TD). The testing direction and EC are the most relevant variables that affect the ability of the crack tip to deform plastically during the crack propagation, determining the final fracture behavior. The fracture parameters obtained with the EWF method, specific EWF, w_e, and plastic item, βw_p, have proved to be very sensitive to the processing induced morphology, finding interesting relationships between such morphologies (characterized by crystallinity index, orientation level, and skin/core ratio) and the fracture parameters of the plaques. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 101: 2714–2724, 2006     

架空在“云”端的网络体系结构

随着近年来云技术的飞速发展,常规的数据网络在扩展性、带宽、规模、成本等方面都明显处于劣势地位,已经无法适应未来的发展需求。在这种情况下,云端网络技术在节约运算成本、提升公司运行效率方面有很好的效果。受到了企业的青睐。基于此本文对架空在“云”端的网络体系结构进行探讨。     

Pattern-induced multi-sequence alignment (PUMA) algorithm employing secondary structure-dependent gap penalties for use in comparative protein modelling

A multiple sequence alignment algorithm is described that usesa dynamic programming-based pattern construction method to aligna set of homologous sequences based on their common patternof conserved sequence elements. This pattern-induced multi-sequencealignment (PUMA) algorithm can employ secondary-structure dependentgap penalties for use in comparative modelling of new sequenceswhen the three-dimensional structure of one or more membersof the same family is known. We show that the use of secondarystructure information can significantly improve the accuracyof aligning structure boundaries in a set of homologous sequenceseven when the structure of only one member of the family isknown     

Heat Induced Structure Modifications in Polymer‐Layered Silicate Nanocomposites

Summary: The success of the use of layered silicates in polymer nanocomposites, to improve physical and chemical properties is strictly related to a deeper knowledge of the mechanistic aspects on which the final features are grounded. This work shows the temperature induced structural rearrangements of nanocomposites based on poly[ethylene‐co‐(vinyl acetate)] (EVA) intercalated‐organomodified clay (at 3–30 wt.‐% silicate addition) which occur in the range between 75 and 350 °C. In situ high temperature X‐ray diffraction (HT‐XRD) studies have been performed under both nitrogen and air to monitor the modifications of the nanocomposite structure at increasing temperatures under inert/oxidative atmosphere. Heating between 75 and 225 °C, under nitrogen or air, causes the layered silicate to migrate towards the nanocomposite surface and to increase its interlayer distance. The degradation of both the clay organomodifier and the VA units of the EVA polymer seems to play a key role in driving the evolution of the silicate phase in the low temperature range. The structural modifications of the nanocomposites in the high temperature range (250–350 °C), depended on the atmosphere, either inert or oxidizing, in which the samples were heated. Heating under nitrogen led to deintercalation and thus a decrease of the silicate interlayer space, whereas exfoliation was the main process under air leading to an increase of the silicate interlayer space.

Heat induced structural modification of EVA‐clay nanocomposite under nitrogen and air.