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61.
《稀有金属材料与工程》2006,23(1):32-34
叙述了用红外吸收法对钛及钛合金中氧和氢联合测定的方法,取得了测定的最佳条件。连续测定6次的相对标准偏差在10%以下,作加标回收试验的回收率为95.6%~103.9%。分析时间在3min以内,可应用于日常分析,结果满意。 相似文献
62.
A simple measuring procedure for low concentrations of H2 and H2S (at the level of ppm fractions) above the surface of water by using sensitive gas analyzers is suggested. The procedure is easily accomplished in conditions outside the laboratory (under field conditions). 相似文献
63.
本文研究了一种Zn-Ti合金新镀层,经盐水浸泡、中性盐雾和大气暴露试验结果试验,其耐蚀明显超过镀Zn层,并与镀Cd层相近,用缺口持久拉伸试验检验氢脆性,拉伸持续时间超过200h,达到原航空部部颁标准(HB5067-85),该镀层适用于高强度钢防护。 相似文献
64.
Gradient-corrected density functional theory was used to investigate the adsorption of H2S on Pd(1 1 1) surface. Molecular adsorption was found to be stable with H2S binding preferentially at top sites. In addition, the adsorption of other S moieties (SH and S) was investigated. SH and S were found to be preferentially bind at the bridge and fcc sites, respectively. The reaction pathways and energy profiles for H2S decomposition giving rise to adsorbed S and H were determined. Both H2S(ad) → SH(ad) + H(ad) and SH(ad) → S(ad) + H(ad) reactions were found to have low barriers and high exothermicities. This reveals that the decomposition of H2S on Pd(1 1 1) surface is a facile process. 相似文献
65.
有机介质中合成二硫化钛 总被引:1,自引:0,他引:1
本文研究了硫化氢与四氯化钛在某些有机介质中的反应,并提出了一个合成二硫化钛的新方法。该法是将干燥的硫化氢通入沸腾的四氯化铁的α-氯代萘溶液中,使硫化氢和四氯化钛发生复分解反应而生成二硫化钛。方法简便易行。X-射线物相鉴定及化学分析结果表明,产物为单一物相的、符合化学计量的二硫化钛。 相似文献
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68.
Edna R Meza‐Escalante Anne‐Claire Texier Flor Cuervo‐López Jorge Gómez Francisco J Cervantes 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2008,83(3):372-377
BACKGROUND: Many industrial discharges, such as those generated from petrochemical refineries, contain large amounts of sulfurous, nitrogenous and organic contaminants. Denitrification has emerged as a suitable technology for the simultaneous removal of these pollutants in a single reactor unit; however, more evidence is demanded to clarify the limitations of denitrification on the simultaneous removal of sulfide and phenolic contaminants and to optimize the biological process. The aim of this study was to evaluate the capacity of a denitrifying sludge to simultaneously convert sulfide and p‐cresol via denitrification. RESULTS: Sulfide was the preferred electron donor over p‐cresol, imposing a 5 h lag phase (required for complete sulfide removal) on organotrophic denitrification. Addition of sulfide (20 mg S2? L?1) to p‐cresol‐amended denitrifying cultures also decreased the reduction rate of nitrate and nitrite, as well as the production rate of nitrogen gas. Nitrite reduction rate was the most affected step by sulfide, decreasing from 35 to 21 mg N (g VSS d)?1. A synergistic inhibitory effect of nitrate and sulfide was also observed on nitrite reduction. Despite the effects of sulfide on the respiratory rates monitored, complete removal of nitrate, sulfide and p‐cresol could be achieved after 48 h of incubation. CONCLUSION: Our results suggest that simultaneous removal of sulfide and p‐cresol could be achieved in denitrifying reactors, but a large hydraulic residence time may be required to sustain an efficient process due to inhibitory effects of sulfide. Copyright © 2008 Society of Chemical Industry 相似文献
69.
按照IEC 61000-4-4/GB 17626.4—1998的要求,首先应用PSPICE仿真确定电路中各元件的参数值,然后基于拉普拉斯变换用MATLAB求解二阶电路验证各元件参数。在此基础上研制了一台以开关电源作为高压直流电源、以氢闸流管作为主控开关的脉冲群电源。该电源体积小、重量轻、效率高、成本低廉。试验结果表明,其输出信号符合标准要求,可用于快速瞬变脉冲群抗扰度试验。 相似文献
70.
The electron spin resonance (ESR) spectra of end‐group spin labelled poly(ethylene oxide) (SLPEO) using 2,2,6,6‐tetramethyl‐piperdine‐1‐oxyl nitroxide and its blends with poly(styrene‐co‐4‐vinylphenol) (STVPhs) of different hydroxyl contents were recorded over a wide temperature range. For a blend of SLPEO and pure polystyrene (PS), the ESR spectrum was composed of a single motion component, indicating that PS was immiscible with PEO. For blends composed of SLPEO and different‐hydroxyl‐content STVPhs, two spectral components with different motion rates were observed over a certain temperature range. The difference between the motion rates should be attributed to micro‐heterogeneity in the blends, with the faster rate corresponding to a nitroxide radical motion trapped in the PEO‐rich domain and the slower rate corresponding to a nitroxide radical motion trapped in the STVPh‐rich domain. Variations in the values of a number of the ESR parameters (Ta, Td and T50G) and the apparent activation energy (Ea) with hydroxyl content in the blends indicated that the miscibility of the blends increased with increasing hydrogen‐bonding density due to specific interactions between the hydroxyl groups in STVPh and the ether oxygens in PEO. Copyright © 2004 Society of Chemical Industry 相似文献