微波渗硼机理研究

利用渗硼介质吸收微波的特性成功地实现了钢铁表面渗硼层的制备，并与常规渗硼进行了比较，结果表明：微波场下渗层生长的硼原子来源于介质分解的硼原子及气态硼化物。渗层生长与常规渗层生长一样表现〈002〉晶向取向生长特征，微波渗硼的渗层生长速率比常规快，除温度效应外，还与微波提高硼原子活性加速硼原子在渗层的扩散有关。     

The Metal-Dielectric Resonator Method of Measuring the Parameters of Radio Materials

The use of symmetrical H- and E-modes and asymmetrical E-modes in a longitudinally anisotropic dielectric cylinder with metal mirrors at the ends to measure its permittivity and dielectric loss tangent is considered. It is shown that the method has wider possibilities compared with the IEC-61338 recommendations. The results of a measurement of the dielectric parameters of a number of materials in the 2–78 GHz frequency band, including the permittivity tensor of sapphire, are presented. __________ Translated from Izmeritel'naya Tekhnika, No. 9, pp. 65–70, September, 2005.     

快速测定化学需氧量的方法

利用分光光度法、微波密封消解法测定水样中的化学需氧量，并把测定的精密度、准确度与国标回流法相比较，结果证明：分光光度法、微波消解法是测定化学需氧量的快捷方法，具有省时、省试剂、工作效率高的特点。     

微波除冰方法研究

为解决我国北方寒冷地区冬季道路积冰不易清除的问题,提出了应用微波加热清除道路积冰的设想.通过实验证实了冰不易吸收微波,而路面材料能够吸收大量微波.因此,微波能够透过冰层加热路面,使贴近路面的冰层融化,消除冰层与路面之间的结合力,然后就可以很容易地利用除冰机械对其清除,这样,就消除了纯机械除冰的弊病.     

A comparison of 18 winter seasons of in situ and passive microwave-derived snow water equivalent estimates in Western Canada

The Meteorological Service of Canada (MSC) has developed an operational snow water equivalent (SWE) retrieval algorithm suite for western Canada that can be applied to both Scanning Multichannel Microwave Radiometer (SMMR) and Special Sensor Microwave/Imager (SSM/I) data. Separate algorithms derive SWE for open environments, deciduous, coniferous, and sparse forest cover. A final SWE value represents the area-weighted average based on the proportional land cover within each pixel. The combined SSM/I and SMMR time series of dual polarized, multichannel, spaceborne passive microwave brightness temperatures extends back to 1978, providing a lengthy time series for algorithm assessment. In this study, 5-day average (pentad) passive microwave-derived SWE imagery for 18 winter seasons (December, January, February 1978/79 through 1995/96) was compared to SWE estimates taken from a distributed network of surface measurements throughout western Canada.Results indicated both vegetative and snowpack controls on the performance of MSC algorithms. In regions of open and low-density forest cover, the in situ and passive microwave SWE data exhibited both strong agreement and similar levels of interannual variability. In locations where winter season SWE typically exceeded 75 mm, and/or dense vegetative cover was present, dataset agreement weakened appreciably, with little interannual variability in the passive microwave SWE retrievals. These results have important implications for extending the SWE monitoring capability of the MSC algorithm suite to northern regions such as the Mackenzie River basin.     

电离辐射及超氧阴离子基对人血淋巴细胞姐妹染色单体交换的诱发作用

用姐妹染色单体交换(SCE)作为指标,研究了~(60)Coγ射线辐照及NADH-PMS(吩嗪硫酸甲酯)系统中产生的超氧阴离子自由基(0_2~(·-))对胎儿脐血淋巴细胞染色体的损伤作用,及活性氧清除剂SOD和甘露醇的保护作用。结果显示γ射线及0_2~(·-)都能诱发细胞SCE频率显著升高,且存在一定的剂量-效应关系。SOD及甘露醇对0_2~(·-)诱发的损伤有明显的保护作用。     

Radiation synthesis of PVP/CMC hydrogels as wound dressing

Carboxymethyl cellulose (CMC) and poly(N-vinyl pyrrolidone) (PVP) were blended to synthesize hydrogels by ⁶⁰Co γ-ray irradiation. A series of hydrogels were prepared with three compositions, i.e. PVP:CMC = 5:5, 6:4 and 7:3. The properties of the hydrogels such as gel fraction, gel strength, swelling behavior and moisture retention were investigated. Compared with pure PVP and CMC hydrogels, PVP/CMC blend hydrogels possessed improved gel strength, flexibility and transparency. As the content of PVP in PVP/CMC blend hydrogels increased, the gel fraction increased while the swelling rate decreased. The hydrogels with optimal properties were obtained in a composition of PVP/CMC = 6/4 with sterilization dose (25 kGy) and further characterized by FT-IR and SEM. Properties concerning the application of wound dressing were performed by comparison with a commercial hydrogel wound dressing to find a similar moisture retention capability and improved swelling rate. The improved properties as well as the cheapness of the materials suggest that PVP/CMC blend hydrogel can be good candidate as wound dressing.     

铁尾矿为原料微波法制备介孔分子筛

以鞍山铁尾矿为硅源,CTAB为模板剂,采用微波辐照法合成出全硅介孔分子筛MCM-41。用N2低温吸附、FT-IR、XRD和TEM等表征手段考察了其比表面积、孔径分布、晶体形貌等特性。结果表明:微波辐射法合成的MCM-41分子筛诱导期极短,晶化速度很快,具有典型的按六方对称性排列的孔道结构,FT-IR证明了分子筛具有硅氧四面体骨架。     

辐射和热同时作用对膨润土物理化学性质和微观结构影响的初步研究北大核心CSCD

为了研究γ辐射和热同时作用对膨润土的影响,以高庙子改性钠基膨润土为研究对象,开展了90℃热作用下、不同剂量率和不同累积剂量的γ辐射老化试验。结果表明:γ辐射和90℃热同时作用引起了膨润土物理化学性质和微观结构的变化。在老化作用后,膨润土的吸水率、pH值、阳离子交换容量、层荷以及蒙脱石001晶面方向的微晶尺寸均减小,比参考样分别降低了(最大减幅)18.4%、7.8%、3.4%、2.9%和15.6%,且表现出剂量率效应;老化作用对膨润土的矿物成分及含量影响较小。在高放废物地质处置的工程屏障设计和安全评价中,应考虑膨润土性质变化的影响因素。