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991.
Thermal properties and crystalline structure of liquid crystalline (LC) poly(ethylene terephthalate‐co‐2(3)‐chloro‐1,4‐phenylene terephthalate) [copoly(ET/CPT)] were investigated using differential scanning calorimetry (DSC), thermogravimetry (TGA), limiting oxygen index (LOI) measurement, electron dispersive X‐ray analysis (EDX), X‐ray diffractometry, and infrared spectrometry (IR). The thermal transition temperatures of copoly(ET/CPT) were changed with the composition. Copoly(ET/CPT) showed two thermal decomposition steps and the residues at 700°C and LOI values of copoly(ET/CPT) were almost proportional to its chlorine content. The activation energy of thermal decomposition of LC units was very low compared to that of poly(ethylene terephthalate)(PET) units. Crystal structure of copoly(ET/CPT) (20/80) was of triclinic system with the lattice constants of a = 9.98 A?, b = 8.78 A?, c = 12.93 A?, α = 97.4°, β = 96.1°, and γ = 90.8°, which is very close to that of poly(chloro‐p‐phenylene terephthlate) (PCPT) with the lattice constants of a = 9.51 A?, b = 8.61 A?, c = 12.73 A?, α = 96.8°, β = 95.4°, and γ = 90.8°. When copoly(ET/CPT)(50/50) was annealed at 220°C in vacuum, crystallization induced sequential reordering (CISR) was not observed but the heat of fusion was slightly increased due to the increase of the trans isomer content in PET units. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 84: 1286–1294, 2002; DOI 10.1002/app.10451 相似文献
992.
993.
基于约束的设备维修方式选择 总被引:2,自引:0,他引:2
曲立 《北京机械工业学院学报》2002,17(4):60-63
企业选择合理的设备维修方式,对提高企业竞争力及企业经济效益有重要影响。将约束理论应用于设备维修方式选择中,分析设备系统约束的特征,识别设备系统约束,区分关键设备与非关键设备部分,并对2个中分分别选择不同的维修方式及组合,可在改善设备系统输出效率同时提高维修的效用。通过实例分析,指明约束理论在设备维修方式选择中的实际应用步骤与程序。这为约束理论在设备管理中的进一步应用提供一个参考。 相似文献
994.
本文自行设计和制作了1.30μmDFB激光器组件的讨论了光隔离和光耦合原理。由于采用的激光器-光隔离器-光纤的一体化结构,大大增加了该组件的可用性。在实验中得到高达55%的耦合效率。 相似文献
995.
Chaosuan Kanchanomai Yukio Miyashita Yoshiharu Mutoh 《Journal of Electronic Materials》2002,31(5):456-465
Low-cycle fatigue (LCF) tests on as-cast Sn-3.5Ag, Sn-3Ag-0.5Cu, Sn-3Ag-0.5Cu-1Bi, and Sn-3Ag-0.5Cu-3Bi solders was carried
out using a noncontact strain-controlled system at 20°C with a constant frequency of 0.1 Hz. The addition of Cu does not significantly
affect the fatigue life of eutectic Sn-Ag solder. However, the fatigue life was significantly reduced with the addition of
Bi. The LCF behavior of all solders followed the Coffin-Manson relationship. The fatigue life of the present solders is dominated
by the fracture ductility and can be described by the ductility-modified Coffin-Manson’s relationship. Steps at the boundaries
of dendrite phases were the initiation sites for microcracks for Sn-3.5Ag, Sn-3Ag-0.5Cu, and Sn-3Ag-0.5Cu-1Bi solders, while
for Sn-3Ag-0.5Cu-3Bi solder, cracks initiated along both the dendrite boundaries and subgrain boundaries in the dendrite phases.
The linking of these cracks and the propagation of cracks inside the specimen occurred both transgranularly through eutectic
phases and intergranularly along dendrite boundaries or subgrain boundaries. 相似文献
996.
杨畅 《导弹与航天运载技术》1998,(5):21-29
提高惯性平台使用精度的途径之一是和计算机实时补偿平台误差的系统分量。首先介绍了仪表和平台误差模型,重点讨论如何从3个含有测量误差,安装误差和基准漂移误差的加速度计输出信号中,分离出载体飞行加速沿制导坐标系三轴的分量。对由于惯性基准的漂移而上起的载体姿态角的测量误差也进行了分析。 相似文献
997.
The gasification reaction of fir charcoal with CO2 was studied by isothermal thermogravimetric analysis under kinetic control. The derived reaction rate (r=dX/dt) as a function of the converted carbon mass (X) was compared with random pore model predictions and found to be much higher at elevated conversion levels than predicted by theory. Similar enhanced reaction rate behaviour was evidenced after removing the natural alkali catalyst from the charcoal by acid washing, suggesting that with untreated charcoal the late reaction rate contribution stems from both, catalytic and additional structure effects. Literature attributes the unpredicted late reaction rate behaviour to the disintegration of the porous char particle into small fragments, which, in line with percolation theory predictions, seems to occur only after a critical conversion level has been reached. However, our gasification data reveal a gradual rise in the charcoal reactivity thereafter, suggesting a breaking up (embrittlement) of the solid phase accompanied by the exposure of fresh surface area from fracturing. The original random pore model derivation given by Bhatia and Perlmutter is extended to account also for these peculiarities and the resulting kinetic relation described our reaction rate data well over the entire conversion range. 相似文献
998.
999.
Ioannis D. Moscholios Michael D. Logothetis 《International Journal of Communication Systems》2006,19(1):67-93
We consider a single link loss system of quasi‐random input, described by the Engset multirate loss model (EnMLM). Blocked calls may once reattempt to be connected to the system requiring less bandwidth; then the system is described by the single retry model for finite sources (f‐SRM). The EnMLM and the f‐SRM are extended with the single threshold finite source model (f‐STM), where calls may attempt to be connected to the system with less bandwidth requirements, according to the link occupancy, before blocking occurs. We focus on CBP equalization in the EnMLM, f‐SRM and f‐STM, under the bandwidth reservation (BR) policy. For this analysis, we apply two approximate methods, the Roberts' method and the method of reverse transition rates (RTR), which lead to a recursive CBP calculation. We evaluate the accuracy of the above models under the BR policy by comparing the analytical with simulation CBP results, based on the relative approximation errors (RAE). The results are highly satisfactory because they show that the proposed models (formulas) lead to small RAE. Copyright © 2005 John Wiley & Sons, Ltd. 相似文献
1000.