Chemische Zusammensetzung und Mikrostruktur polymerabgeleiteter Gläser und Keramiken im System Si–C–O. Teil 2: Charakterisierung der Gefügeausbildung mittels hochauflösender Durchstrahlungselektronenmikroskopie und Feinbereichsbeugung

Chemical Composition and Microstructure of Polymer‐Derived Glasses and Ceramics in the Si–C–O System. Part 2: Characterization of microstructure formation by means of high‐resolution transmission electron microscopy and selected area diffraction Liquid or solid silicone resins represent the economically most interesting class of organic precursors for the pyrolytic production of glass and ceramics materials on silicon basis. As dense, dimensionally stable components can be cost‐effectively achieved by admixing reactive filler powders, chemical composition and microstructure development of the polymer‐derived residues must be exactly known during thermal decomposition. Thus, in the present work, glasses and ceramics produced by pyrolysis of the model precursor polymethylsiloxane at temperatures from 525 to 1550 °C are investigated. In part 1, by means of analytical electron microscopy, the bonding state of silicon was determined on a nanometre scale and the phase separation of the metastable Si–C–O matrix into SiO₂, C and SiC was proved. The in‐situ crystallization could be considerably accelerated by adding fine‐grained powder of inert fillers, such as Al₂O₃ or SiC, which permits effective process control. In part 2, the microstructure is characterized by high‐resolution transmission electron microscopy and selected area diffraction. Turbostratic carbon and cubic β‐SiC precipitate as crystallization products. Theses phases are embedded in an amorphous matrix. Inert fillers reduce the crystallization temperature by several hundred °C. In this case, the polymer‐derived Si–C–O material acts as a binding agent between the powder particles. Reaction layer formation does not occur. On the investigated pyrolysis conditions, no crystallization of SiO₂ was observed.     

光纤通信在市内接入网的应用

先说明市内接入网的单位用户和住家用户两大类使用通信和电视、交互型和分配型业务的要求不相同，相应地对光纤传输的应用须作不同的考虑，文中认为；光纤从市内交换局直连办公大楼是合乎现实需要的，而对于居民住家，宜选用光纤连至路边或光纤与同轴结合和适当利用无源光网络等方案，俟将来时机成熟才实行光纤连至每一家，文末有概括总结，说明接入网不同于长途网，接入网的光纤系统可以使用常规单模光纤，工作于波长1．3μm，而光放大器和波分多路系统不是普遍需要，但光电子集成在光端机中是必要的。     

SOPHO—S的结构分析与线路传输技术

ＳＯＰＨＯ－Ｓ系列数字程控交换机是由飞利蒲公司生产的。本文分析了该系列交换机的总体结构，并了它的线路传输技术。     

宽带自适应跳频控制器

本文叙述宽带自适应跳频控制器的原理及方案,频率集的配置、自适应跳频拒收门限及频点更新、跳频码序列及同步等。有效地组织宽带自适应跳频系统能避开大部分固定和半固定性质的单频连续波干扰,使得移动卫星通信系统中实现高可靠性的数据传输。     

DRB32在提高异种机互连传输中的应用

字结构不同的计算机互连，以往用软件转换字结构，增加了软件开销，导致传输效率降低。现介绍一种用硬件逻辑转换的方案，在数据传送过程中，使一台计算机的数据结构适应另一台计算机的要求。简捷、可靠、快速，大大地提高了异种机互连的传输率。     

井场信息系统建设体系结构

对井场钻井数据实时远程传输的研究和实践进行了总结,从数据远传作用、数据远传通信方式、数据通信网络体系结构、未来发展等几个方面对井场数据远程传输进行了探讨。     

Critical-point drying versus freeze drying for scanning electron microscopy: a quantitative and qualitative study on isolated hepatocytes

Critical-point drying and freeze drying were compared both quantitatively and qualitatively as preparative procedures for scanning electron microscopy. Isolated hepatocytes were used as model cells. Nomarski differential interference contrast microscopy was used for light microscopic measurements of the hepatocytes in the unfixed, the glutaraldehyde fixed, the glutaraldehyde + OsO₄ fixed, the critical-point dried and the freeze dried states. Critical-point dried hepatocytes were found to shrink to 38% of glutaraldehyde + OsO₄ fixed volume, whereas optimal freeze dried hepatocytes (frozen in water saturated with chloroform and freeze dried at 183 K for 84 h) were found to shrink to 51% of glutaraldehyde + OsO₄ fixed volume. Transmission and scanning electron micrographs of the critical-point dried cells showed well-preserved ultrastructure and surface structure. Micrographs of the freeze dried cells showed ultrastructure destroyed by internal ice crystals and surface structure destroyed by external ice crystals. Double-fixed isolated hepatocytes were shown to swell during storage in buffer and to shrink during storage after critical-point drying. For low magnification scanning electron microscopy (up to about 3000 times) both critical-point drying and freeze drying can be used. However, for high magnification scanning electron microscopy, critical-point drying is superior to freeze drying.     

用NILT导出的传输线瞬态分析模型

K Singhal与J Vlach的NILT(数值Laplace反变换) 技术是端接线性负载传输线分析的一种有效方法.本文利用这一NILT技术,导出了传输线的时域离散模型,由此可进行端接任意负载传输线的瞬态分析.这一模型毋须象通常的频域方法那样对传输线作有理逼近,因而不存在由此带来的数值问题,而计算量与它们相当.文中分别给出了均匀与非均匀传输线的处理,并用实例作了验证.     

分布式光纤喇曼放大技术及其在WDM系统中的应用

介绍了分布式光纤喇曼放大技术的原理、特点和应用 ,并从受此影响的 WDM传输系统的信噪比、噪声指数和品质因数三个方面讨论了光纤喇曼放大技术在提升光纤通信系统性能方面的重要作用。     

有耗传输线的TLM模型法

本文从传输线理论出发，介绍了一种解决传输线问题的新方法－－TLM法。