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51.
Tsan-Yue Yang George E. Klinzing Shiao-Hung Chiang Fernando J. Aguirre 《Chemical Engineering Communications》1988,64(1):1-11
In the study of mass transfer between partially miscible liquids, temperature perturbations have been found to have an important effect in the generation of interfacial activity. Micro- and macro-generated interfacial convection usually occurs in combination with one another even in fairly simple heat or mass transfer events. These combinations are responsible for the enhancement of mass transfer rates. In an effort to acquire a better understanding of the heat transfer effects in ternary liquid-liquid systems, temperature difference profiles were measured when contacting two partially miscible phases. A vertical and a rotational transfer cell were designed to contact the partially miscible phases without inducing external disturbances. Five thermocouples were immersed in the bottom liquid phase at predetermined positions below the interface. In order to understand the influence of the convection generated, the vertical cell was designed to hinder convection in one phase, while the rotational cell permits convection in both phases. The experimental results showed larger temperature differences in the rotational cell after the contact of the phases. Also, systems which were initially unsaturated presented larger heat effects than those in which the partially miscible solvents were initially saturated. Several parameters indicating the importance of heat effects in the ternary systems studied are reported. 相似文献
52.
In this paper we describe an apparatus for reproducibly measuring thermal shock resistance of thick polymer layers bonded to metals. The thermal shock behavior is discussed in terms of epoxy samples bonded to an aluminum substrate. It was found that both high resin toughness and low resin thermal expansion coefficient improved thermal shock resistance of thick coatings, but only a sample containing 60wt. % glass beads did not develop a failure crack. Effects of sample thickness, temperature gradient, and resin composition on thermal shock behavior are discussed. 相似文献
53.
54.
The secure operation of autonomous vehicle networks in the presence of adversarial observation is examined, in the context of a canonical double-integrator-network (DIN) model. Specifically, we study the ability of a sentient adversary to estimate the full network’s state, from noisy local measurements of vehicle motions. Algebraic, spectral, and graphical characterizations are provided, which indicate the critical role of the inter-vehicle communication topology and control scheme in achieving security. 相似文献
55.
56.
David A. Woodford Donald R. VanSteele Mohammed J. Hyder 《Journal of the American Ceramic Society》1991,74(12):3142-3144
The development of a tensile testing methodology for ceramics which enables a stress vs strain-rate response to be measured at high temperature is described. The test involves a carefully controled stress relaxation test at constant total strain using an experimental procedure and phenomenological analysis previously developed for metallic materials. It is demonstrated here with preliminary tests on alumina at 1050° and 1150°C. This offers, with further development, the possibility of establishing design stresses associated with low strain-rate behavior for structural applications. The results demonstrate that data covering four decades of strain rate may be generated in tests lasting a few hours. The inelastic strain consists of substantial anelastic recoverable strain in addition to a permanent creep strain. 相似文献
57.
浅析SRT-Ⅳ裂解炉炉管弯曲及断裂原因 总被引:1,自引:0,他引:1
主要分析计算了裂解炉炉管受力情况,进而得出结论:裂解炉自身结构的相互约束力和炉管渗碳是导致炉管弯曲、断裂的主要原因,并提出了相应的解决措施。 相似文献
58.
本文介绍了冷却器盘管破裂泄漏的情况,分析了失效破坏的原因,并提出防止冷却器盘管破裂泄漏的措施。 相似文献
59.
MgO/Ni系梯度功能材料的设计与制备 总被引:11,自引:0,他引:11
对MgO/Ni系梯度功能材料(FGM),分别用实验和微观力学模型测定和计算了用于热应力缓和设计的各物性参数。讨论了两种结果之间存在差异的原因。用有限元方法模拟了制备过程中FGM的热应力,得到MgO/Ni系FGM的综合设计准则。按设计结果进一步调整粉末工艺性质,成功地烧制出MgO/Ni系FGM。 相似文献
60.
污泥中总磷测定方法的探讨 总被引:1,自引:0,他引:1
污泥样品与氢氧化钠熔融,使污泥中含磷有机化合物全部转化为可溶性的正磷酸盐,然后测定污泥中的总磷含量.此方法方便易行,平行性好,准确度高,可作为测定污泥中总磷的标准方法. 相似文献