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21.
The effect of rare earth oxides Y203 or Ce02 on sintering properties of Si3N4 ceramics was studied and the mechanism of assisting action during sintering was analyzed. The results in dicate that the best sintering properties appear in Si3N4 ceramics with 5% Y203 or 8% CeO2. Secondary crystallites are formed at grain boundaries after heat treatment,which decreases the amount of glass phase and contributes to the improvement of high-temperature mechanical properties of silicon nitride. 相似文献
22.
VK Tzitzios V Georgakilas TN Angelidis 《Journal of chemical technology and biotechnology (Oxford, Oxfordshire : 1986)》2005,80(6):699-704
A study of nitrous oxide (N2O) reduction with methane (CH4) and propene (C3H6) in the presence of oxygen (5%) over Ag/Al2O3, Rh/Al2O3 and Ag–Rh/Al2O3 catalysts, with Ag and Rh loadings of 5 wt% and 0.05 wt% respectively, has been performed. From the results, it was observed that the Ag–Rh bimetallic catalyst was the most active for both nitrous oxide removal (more than 95%) and hydrocarbon oxidation. This high activity seems to be connected with a synergistic effect between Ag and Rh. The findings from X‐ray diffraction and X‐ray photoelectron spectroscopy studies showed also, that there were no strong interactions (eg alloying) between Ag and Rh. Copyright © 2005 Society of Chemical Industry 相似文献
23.
设{Z,(W)}是定义在概率空间上的独立的随机变量序列,Z(W)具有方差为期望E(Zn)=0.本文证明了对任意算数序列{bn}及任意的存在充分大的整数N>0使当N'>N″>N时.有此不等式在随机级数研究中有重要作用. 相似文献
24.
Preparation and Properties of Sintering Additives Coated Si3N4 from Heterogeneous Nucleation Processing 总被引:1,自引:0,他引:1
The sintering additives such as Al2O3 and /or Y2O3 were coated on the surfaces of Si3N4 particles via heterogeneous nucleation processing using a buffered pH solution as the precipitation reagent .They nucleated and grew only on the surfaces of Si3N4 and did not form sol particles in solution by TEM observation .The isoelectric point(IEP) of coated Si3N4 was different from that of as-received Si3N4.The IEP of Al(OH)3-coated Si3N4 occurred at pH8.4, which is close to that of alumina .When Al(OH)3-coated Si3N4 particles were coated with Y(OH)3,the IEP of coated Si3N4 powder shifted from pH8.4 to pH9.2 ,similar to that of yttria.In addition ,the rheological data showed that Al2O3 and /or Y2O3 coated Si3N4 suspension is nearly Newtonian and that added Si3N4 suspension shows a shear rate thinning behavior. 相似文献
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Received September 14, 2000; revised September 25, 2001 相似文献
27.
J.-P. Croisille 《Computing》2006,78(4):329-353
We introduce a new box-scheme, called ``hermitian box-scheme' on the model of the one-dimensional Poisson problem. The scheme
combines features of the box-scheme of Keller, [20], [13], with the hermitian approximation of the gradient on a compact stencil,
which is characteristic of compact schemes, [9], [21]. The resulting scheme is proved to be 4th order accurate for the primitive
unknown u and its gradient p. The proved convergence rate is 1.5 for (u,p) in the discrete L
2 norm. The connection with a non standard mixed finite element method is given. Finally, numerical results are displayed on
pertinent 1-D elliptic problems with high contrasts in the ellipticity, showing in practice convergence rates ranging from
1 to 2.5 in the discrete H
1 norm.
This work has been performed with the support of the GDR MOMAS, (ANDRA, CEA, EDF, BRGM and CNRS): Modélisation pour le stockage des déchets radioactifs. The author thanks especially A. Bourgeat for his encouragements and his interest in this work. 相似文献
28.
L. Pibida M. Unterweger L. R. Karam 《Journal of research of the National Institute of Standards and Technology》2004,109(4):451-456
Characterization of commercially available instruments for measurement and identification of unknown radionuclides was carried out in support of the development and testing of the American National Standards Institute (ANSI) standard, N42.34, “Performance Criteria for Hand-held Instruments for the Detection and Identification of Radionuclides.” Measurements were based on the performance of the devices, i.e., the capability of the detectors to ensure a correct radionuclide identification in a given time interval for various radioactive sources. 相似文献
29.
N‐p‐Bromophenylmaleimide (BrPMI) does not polymerize in solution by conventional free radical mechanism. However, it readily polymerized in bulk when mixed with a free radical initiator and heated in a microwave oven for 7–8 min. Copolymerization of ethyl methacrylate or butyl methacrylate with BrPMI was conducted in dioxane. The copolymers were characterized by IR and 1H NMR spectroscopy and gel permeation chromatography. The monomer reactivity ratios were calculated by a non‐linear least‐square analysis. Thermal analysis indicated a great improvement in thermal stability of the copolymers compared with the methacrylate homopolymers. BrPMI was also polymerized in bulk in the DSC pan, which allowed the calculation of the activation energy of its polymerization. Copyright © 2003 Society of Chemical Industry 相似文献
30.