Early detection of ageing in solder joints through laser probe thermal analysis of the peltier effect

We have recently developed an optical contactless method for testing the quality of solder joints during accelerated thermal cycling ageing processes.¹ The method was based upon the measurement of the dynamic thermal behaviour of the joint to short bursts of Joule heating. It has proved to be efficient in revealing the formation of cracks at the lead-solder interface. We present a method to evaluate ageing at a much earlier stage in the cycling process. We have observed in earlier work,¹ that before cracks appear, structural changes occur in the solder at the lead-solder interface. The thermal response of the solder joint is recorded over time to a Peltier heat perturbation produced by flowing a current pulse through the interface where structural changes occur. The key point in this method is to discriminate the Peltier effect from the Joule thermal response because both effects generate heat. The variation of the early Peltier response in the thermal cycling ageing tests is seen as a quantitative signature of the structural changes in the lead-solder interface.     

三辊穿孔和轧管所产生的钢管壁厚极差和波浪形内螺纹

定量描述了实际生产过程中三辊斜轧穿孔所产生的钢管壁厚极差和波浪形内螺纹，初步探讨了三辊轧管机对钢管壁厚极差和波浪形内螺纹的影响。     

Preparation of core–shell type nanoparticles of diblock copolymers of poly(L‐lactide)/poly(ethylene glycol) and their characterization in vitro

Core–shell type nanoparticles of poly(L ‐lactide)/poly(ethylene glycol) (LE) diblock copolymer were prepared by a dialysis technique. Their size was confirmed as 40–70 nm using photon correlation spectroscopy. The ¹H‐NMR analysis confirmed the formation of core–shell type nanoparticles and drug loading. The particle size, drug loading, and drug release rate of the LE nanoparticles were slightly changed by the initial solvents that were used. The drug release behavior of LE core–shell type nanoparticles showed an initial burst during the first 12 h and then a sustained release until 100 h. The degradation behavior of LE block copolymer nanoparticles was divided into three phases: the initial rapid degradation phase, the stationary phase, and the rapid degradation phase until complete degradation. It was suggested that lidocaine release kinetics were predominantly governed by the diffusion mechanism in the initial burst phase and after that by both of the diffusion and degradation mechanisms. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 85: 2625–2634, 2002     

补充型润滑油添加剂分析

补充型润滑油添加剂对改善和提高油品使用性能具有重要意义，有较大的发展应用潜力。本文对补充型添加剂及有关问题进行了分析和分析，认为补充型添加剂不是万能的，使用时须认真考虑与润滑油的协和性，要加强对它的质量监控。     

异形柱柱头混凝土连续托梁分次置换技术

通过某工程异形柱头混凝土置换实例,介绍了连续托梁分次置换技术的设计计算、施工方法和技术措施等。     

微波热液法制备光催化TiO2功能材料

采用微波加热法，研究了钛配离子热分解水解反应的规律。结果表明，水解产物在大气气氛和300℃下煅烧2h，所得产物为锐钛型TiO2粉末。在紫外线照射下，乙酸经Ti02光催化反应12h后，残余量小于初始量的20％。     

门式脚手架在已建高层建筑外装修中的应用

介绍门式脚手架在已建高层建筑外排栅中的整体搭设和应用实例。     

户式中央空调发展方向的探讨

本文描述了我国户式中央空调的发展现状，分析了三种户式中央空调各自的特点，提出了把风管式机组作为我国户式中央空调的发展方向。     

钻杆防磨技术的现状和发展

在深井超深井勘探过程中，由于径向力、涡动、横向振动等因素的存在，随着钻井时间的增长，钻柱作用于套管内壁的侧向力增大，导致套管磨损的问题越来越严重。介绍了近年来钻杆防磨技术的发展，主要从钻杆接头表面处理和钻杆保护器2方面来研究防磨减磨措施的现状和发展。     

挠性抗回旋PDC钻头的有限元分析

回旋是导致PDC钻头早期失效的主要原因，介绍了一种基于挠性钻头的构想设计的抗回旋PDC钻头，阐述了其结构和抗回旋原理。对挠性钻头的公、母接头进行了有限元应力分析，说明了模型建立、网格划分以及约束和载荷施加过程中所采用的方法和关键技术。有限元分析结果表明挠性钻头的强度满足要求。