Corrosion of Three Commercial Steels Under ZnCl2 –KCl Deposits in a Reducing Atmosphere Containing HCl and H2S at 400–500°C

The corrosion of three commercial steels in a reducing atmosphere containing HCl plus H₂S in the presence of ZnCl₂–KCl deposits has been investigated at 400–500°C and compared with the corrosion of the same materials in a similar gas mixture free from H₂S. The presence of H₂S in the gas accelerated the corrosion of the three commercial steels beneath ZnCl₂–KCl deposits. All materials suffered from severe corrosion with partial detachment and spalling of the external scales. Degradation of the steels resulted from the penetration of chlorine-containing species through the scale formed initially down to the metal matrix, because chorine-rich species were detected close to the alloy/scale interface. Although the corrosion resistance generally increased with increasing Cr content, even the high-Cr stainless steel SS304 is still unable to provide good corrosion resistance against the ZnCl₂–KCl deposits in the presence of H₂S due to the bad adherence of the scales to the alloy. The mechanisms of attack are discussed on the basis of thermodynamic considerations and of the active-oxidation model.     

Surface nanocrystallization of commercial pure titanium by shot peening

The surface nanostructures of commercial pure titanium was realized by the modified shot peening equipment commonly used in industry through the special treatment process. The results show that high-energy-shot-peening(HESP) commonly used to prepare nanostructured surface layers can be achieved by the increase of pill size, pill speed, and treatment time in the commercial shot peening equipment. XRD, SEM and TEM were used to characterize the surface layer microstructure of treated specimens. The analytic results show that the main deformation mode of commercial pure Ti is twinning. At the beginning of deformation, the dislocations are formed and twins occur within or on plane, then twins in intersection plane appear, and at last the twin characteristics disappear in the surface layer after longer treatment time. The deformation layer depth increases with treatment time in a certain period when the pill size and speed are unchanged. And in the severe plastic deformation (SPD) layer in which the twins are not identified easily by using SEM, the nanocrystalline microstructures are found under TEM. The finest grain size in the surface layer is about 40 nm, and the depth of nanostructured layers is over 60 μm. The microhardness of the nanostructured surface layers is enhanced significantly after shot peening compared with that of the initial simple.     

工业纯铝高温流变行为的实验研究

为了深入了解连续铸轧这一融合了“铸造”和“轧制”两个工艺过程条件下的流变行为与简单铸造+热加工(热轧)组合条件下流变行为的差异,在Gleeble-1500热模拟机上对铸造工业纯铝高温压缩流变行为及其影响因素进行了系列的模拟实验研究,得到了不同变形条件下铸造工业纯铝高温压缩成形过程中的流变曲线;通过多元线性回归分析得到了其应力-应变本构方程;并与铸轧过程物理模拟实验研究的结果进行了对比分析,结果表明:在相同变形条件下铸造工业纯铝高温压缩变形流变应力小于铸轧过程的流变应力,且随着应变速率的增大,它们之间的差值更大。     

对中小商业银行等级保护咨询服务探讨与研究

本文力求全面剖析中小商业银行的等级保护咨询服务项目,帮助将要开展信息安全等级保护的咨询方和银行信息安全管理者明确等级保护的咨询服务所涵盖的内容及所能达到的目标。     

数字式大气波导测试仪设计

由于常规大气结构探测设备的误差较大,根据开口微波谐振腔的谐振频率随流过腔内介质不同而变化的原理,设计了一种数字式大气波导测试仪。实验证明：大气波导测试仪能够探测出气象仪器所无法获得的精细大气波导结构,具有精度高、响应速度快等特点。该仪器可为舰船雷达、通信系统实现超视距传播奠定基础。     

大气湍流图像像素偏差机理分析

对大气湍流导致图像畸变和像素偏差的因素进行了深入分析,对大气湍流状态下激光发射远距离光束的光束漂移均方值进行仿真,分析光束漂移均方值曲线,为后续对图像畸变、像素偏差校正及克服湍流影响提供有效的理论依据。     

商业银行安全保障体系设计

随着计算机及网络通信等新技术在银行业的广泛应用,金融电子化、网上银行、现金支付系统等新的业务系统为客户提供方便快捷服务的同时,给银行自身带来了众多安全隐患,还由此引发了诸多金融风险。基于现代信息安全理论,采取信息技术和管理相结合,静态设计与动态管理相结合,应用系统工程的观点和方法,分析网络的安全措施,按照突出重点、讲求实效、加强管理、保证安全的原则,构筑商业银行信息系统网络和信息安全保障体系。     

一种可溶性双酮酐型共聚酰亚胺的合成及性能

以均苯四甲酸二酐(PMDA)和4,4’-对苯二甲酰二邻苯二甲酸酐(TDPA)为二酐单体,4,4’-(3-氨基苯氧基)二苯甲酮(BABP)为二胺单体,采用两步法低温溶液缩聚合成了系列双酮酐型共聚酰亚胺。采用红外光谱、X射线衍射、差示扫描量热分析、热重分析、拉伸测试和溶解性能测试对聚合物的结构与性能进行了表征,考察了TDPA/PMDA不同摩尔比对共聚酰亚胺溶解性、耐热性和力学性能的影响。结果表明,双酮酐型聚酰亚胺的玻璃化转变温度随TDPA摩尔含量的增加逐渐下降,溶解性能则逐渐提高,当TDPA/PMDA摩尔比为7/3时,共聚酰亚胺具有优良的耐热性能及力学性能,可溶于N,N-二甲基甲酰胺(DMF)等极性溶剂。     

视觉文化语境下手绘插画与商业包装的交融

目的研究视觉文化时代下的手绘插画。方法从手绘插画和商业包装设计艺术形式的角度出发探讨手绘插画与商业包装的交融性。结论手绘插画具有独特的艺术魅力和浓厚的文化底蕴,可以有效传播品牌文化、塑造品牌形象。与商业包装相融的手绘插画能丰富商业包装的视觉语言、承载人们情感,使包装更具亲和力与艺术魅力。     

商业诽谤犯罪中网络服务提供者行为的技术与法律分析

在本案中,刑法及其司法解释完全从商业诽谤犯罪实行行为的角度进行解释,没有重视网络信息服务提供者的行为特点,实际上导致难以根据刑法以及司法解释分析网络服务提供者在网络商业诽谤违法犯罪中的责任。在商业诽谤刑事案件中,网络服务提供者不仅有义务向侦查机关提供有关资料,而且由于其在信息监管责任缺位,必须对其设置责任追究的机制,从而推动其履行商业诽谤信息审查义务。