石墨炉原子吸收测定化探样品中痕量金的研究

采用以王水分解样品,泡沫塑料富集,硫脲解脱,石墨炉原子吸收分光光度计测定微量金。研究了测定时干燥温度和时间的选择,原子化温度和时间的选择,灰化温度和时间的选择,以及王水体积分数对吸附效果等条件对测定结果的影响。该方法检出限为0.2×10-9,经国家一级分析标准样品验证,结果与标准值相符。     

低能X射线吸收法测量泡沫材料密度

文章介绍为适应惯性约束聚变(ICF)靶材料研究而发展的一种密度测量方法。通过测量X射线经靶材料吸收前后的强度变化,可较为精确地计算出待测样品的密度。用于泡沫材料密度测量的X射线源是特制的激发源。     

由中间相沥青制备泡沫炭:Fe(NO3)3的影响

以中间相沥青为前驱体制备高性能泡沫炭，在考察中间相沥青、Fe（NO3）3及其混合物热分解行为的基础上，着重研究了Fe（NO3）3对制备中间相沥青基泡沫炭的影响，揭示了Fe（NO3）3对泡沫炭孔泡结构的影响规律及其作用机制，初步研究了在泡沫炭炭化过程中形成的Fe／C之物相结构及其石墨化行为。结果表明，在不同的炭化温度下，Fe在泡沫炭中的存在形态各异；Fe物种的存在有利于提高泡沫炭的石墨化程度。     

Fracture and microstructure of open cell aluminum foam

SEM and EDS measurements were used to scrutinize the microstructure of Duocel open cell 6101 aluminum foam in relation to its fracture properties. In-situ SEM tensile tests on the open cell aluminum foam were performed to investigate the different fracture modes of struts and Aramis/Digital Image Correlation software was used to map the strain in individual struts. Observations during tensile tests showed that the microstructure of the struts has a great influence on the fracture behaviour of the foam. In particular AlFeSi-precipitates, which are due to the casting of the 6101 aluminum alloy, and the morphology of the foam alters the fracture mode of the struts in the foam from transgranular to intergranular. Less energy is needed for intergranular fracture of struts and the strain to failure of the foam is decreased due to weak individual struts.     

Compression-after-Impact Strength of Sandwich Panels with Core Crushing Damage

Compression-after-impact (CAI) strength of foam-cored sandwich panels with composite face sheets is investigated experimentally. The low-velocity impact by a semi-spherical (blunt) projectile is considered, producing a damage mainly in a form of core crushing accompanied by a permanent indentation (residual dent) in the face sheet. Instrumentation of the panels by strain gauges and digital speckle photography analysis are used to study the effect of damage on failure mechanisms in the panel. Residual dent growth inwards toward the mid-plane of a sandwich panel followed by a complete separation of the face sheet is identified as the failure mode. CAI strength of sandwich panels is shown to decrease with increasing impact damage size. Destructive sectioning of sandwich panels is used to characterise damage parameters and morphology for implementation in a finite element model. The finite element model that accounts for relevant details of impact damage morphology is developed and proposed for failure analysis and CAI strength predictions of damaged panels demonstrating a good correlation with experimental results.     

低腐蚀酚醛泡沫及其改性研究

合成了可发性酚醛树脂，确定了酚醛泡沫用低腐蚀性混合酸固化体系的配方及其发泡工艺参数，并采用聚乙二醇、氢氧化铝对其进行了改性，研究了聚乙二醇及氢氧化铝加入量对泡沫压缩强度、阻燃性及发泡工艺等的影响。     

硬质聚氨酯泡沫塑料用于冷库保温工程施工中应注意的问题

阐述了冷库现场喷涂聚氨酯施工作业中对原材料、施工队伍、施工工艺等方面的要求和建议。     

泡沫铝制备过程中增粘剂的选择

研究了铝熔体中添加不同种类增粘剂后的增粘效果,并通过对制备泡沫体的宏观观测和微观检测,研究了铝熔体增粘方式对泡沫体结构的影响及各种增粘剂的增粘机理. 结果表明:铝熔体中加入金属钙、镁、氧化铝和粉煤灰后,其物相组成发生改变,增粘剂存在形式和增粘机理不同,得到的泡沫体在结构上差别也很大.     

SiCP增强泡沫铝基复合材料制备工艺及润湿性研究

对采用熔体发泡法直接制备碳化硅颗粒增强泡沫铝基复合材料进行了探索，讨论了制备过程中SiCp与铝液间的润湿性、发泡工艺参数与温度控制等对制备工艺的影喻。表明该工艺简单，易于操作，不需任何增粘措施，处理后的SiCp浸润性好且分布均匀，孔洞分布均匀。     

CaCO3发泡剂制备泡沫铝工艺研究

用CaCO3作发泡剂，用熔体发泡法制备泡沫铝，即Al—Si12在熔融状态下，加入活性剂Mg粉，再与SiC颗粒混合均匀，然后加入发泡剂(CaCO3)搅拌，进行保温发泡，最后冷却。结果表明，对于Al—Si12的合金，用CaCO3作为发泡剂，制备出孔隙结构均匀，平均孔隙率最大、结构均匀的泡沫铝的最优条件是：CaCO3含量1．2％～1．8％，加热温度680～700℃之间，保温时间4～8min之间。