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61.
A. Zosel 《The Journal of Adhesion》1994,44(1):1-16
Correlations between shear resistance and the mechanical properties of pressure sensitive adhesives are studied by measuring the deformation behaviour in the static and the dynamic shear test and determining the dynamic shear modulus of the adhesive. For polymers with low or moderate viscosities, the shear strain vs. time characteristics in a static shear test and, accordingly, the static shear strength, can be evaluated from the master curves of the dynamic shear modulus or the dynamic viscosity. The dynamic shear strength also can be calculated. These exact calculations cannot be applied to highly viscous or slightly crosslinked polymers. On the basis of the model experiments, empirical correlations between shear strength and the dynamic shear modulus are established which seem to be generally valid. 相似文献
62.
63.
The present work aims to provide a better understanding of the effect of both the proportions and the characteristics of slaked lime on the microstructure of a lime-cement-sand mortar. Cement (CPA CEM I 52.5) has been replaced by various categories of slaked lime chosen for the diversity of their physico-chemical characteristics.Cement has been replaced by lime in proportions varying between 0 to 10% of the total binder mass. With very few exceptions, mortars were produced by maintaining the quantity of water constant.Experimental results show that it is necessary to have a high lime substitution percentage to influence the microstructure of the mortar, except in the case of a lime containing magnesium hydroxide or calcic lime featuring sizeable specific surface area.The influence of the nature of the substituted lime on the development of the microstructure in the matrix has been examined by SEM observations of the mortar micro porosity. 相似文献
64.
Collocation methods are developed for the solution of some differential equation models for transport phenomena problems in one-and two-dimensions in co-axial annuli of spherical and cylindrical shapes. General formulae are developed to obtain orthogonal polynomials over an arbitrary interval using two types of weighting functions. The convergence and accuracy of the methods are demonstrated using two test problems, i.e., calculation of effectiveness factors in (a) a spherical pellet with peripherally deposited catalyst and (b) a Raschig ring type cylindrical catalyst pellet. Comparisons of results obtained from the present methods with analytic solutions for the first-order reactions indicate good agreement. Numerical solutions are also obtained for the second-and the third-order reactions for which analytic solutions are not available. Results obtained in terms of a new Thiele modulus involving the ratio of volume of peripherally deposited part of catalyst to exterior surface area indicate that this normalization brings effectiveness factor versus Thiele modulus curves close together for co-axial spherical and long cylindrical pellets, as it does for these geometries without the inner co-axial portion. 相似文献
65.
To synthesize new functional poly(urethane‐imide) crosslinked networks, soluble polyimide from 2,2′‐bis(3,4‐dicarboxyphenyl) hexafluoropropane dianhydride, 4,4′‐oxydianiline, and maleic anhydride and polyurethane prepolymer from polycaprolactone diol, tolylene 2,4‐diisocyanate and hydroxyl ethyl acrylate were prepared. Poly(urethane‐imide) thin films were finally prepared by the reaction between maleimide end‐capped soluble polyimide (PI) and acrylate end‐capped polyurethane (PU). The effect of polyurethane content on dielectric constant, residual stress, morphology, thermal property, and mechanical property was studied by FTIR, prism coupler, Thin Film Stress Analyzer (TFSA), XRD, TGA, DMTA, and Nano‐indentation. Dielectric constant of poly(urethane‐imide) thin films (2.39–2.45) was lower than that of pure polyimide (2.46). Especially, poly(urethane‐imide) thin films with 50% of PU showed lower dielectric constant than other poly(urethane‐imide) thin films did. Lower residual stress and slope in cooling curve were achieved in higher PU content. Compared to typical polyurethane, poly(urethane‐imide) thin films exhibited better thermal stability due to the presence of the imide groups. The glass transition temperature, modulus, and hardness decreased with increase in the flexible PU content even though elongation and thermal expansion coefficient increased. Finally, poly(urethane‐imide) thin films with low residual stress and dielectric constant, which are strongly affected by the morphological structure, chain mobility, and modulus, can be suggested to apply for electronic devices by variation of PU. © 2006 Wiley Periodicals, Inc. J Appl Polym Sci 100: 113–123, 2006 相似文献
66.
A study was done of jute composite using a polymer matrix of epoxidized Novolac resin (ENR), diglycidyl ether of bisphenol A (DGEBA)–based epoxy, and their blends with different weight percentages of the resins. It was found that on blending ENR with DGEBA, the storage modulii at room temperature are enhanced by about 100% or more in the case of 30 and 40% ENR‐containing matrices, whereas the enhancement in the case of 20 and 12% ENR‐containing matrices is only 50% that of the pure matrix. It was also observed that the tan δ peak heights of the composites containing 30 and 40% ENR are closer to that of 20% ENR‐containing composite. The probable explanation drawn on the basis of experimental findings of DMA and mechanical analysis is that by blending ENR with DGEBA epoxy it is possible to manufacture jute composites with increased stiffness without sacrificing their ductility. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 85: 2800–2807, 2002 相似文献
67.
分析了PVC的拉伸过程,讨论了外力作用速度对PVC的影响.结果表明:PVC的拉伸屈服强度随外力作用速度的提高而提高,断裂伸长率却随之下降. 相似文献
68.
室内承载板法是测定土基回弹模量的标准试验方法。尺寸效应和约束条件的影响使得室内测定的回弹模量往往与现场不符,不能直接用于公路结构设计。以红黏土为研究对象,采用室内试验和数值模拟的方法研究了试样的尺寸效应和约束条件对土基回弹模量的影响。结果表明:试样的尺寸效应(试样直径和高度)对回弹模量的影响较大,随着试样直径的增大回弹模量增大,随着试样高度的增大回弹模量减小;无侧限条件下测定的回弹模量乘以约束条件系数1.2即得有侧限条件下回弹模量值。研究成果为室内合理测定土基回弹模量值提供参考依据。 相似文献
69.
掺加橡胶微粒可以明显改善混凝土的力学特性。采用橡胶微粒等体积取代细骨料的方法,通过不断调整配合比,反复试验配制出橡胶微粒体积掺量分别为0%、10%和15%的等强度(30 MPa)橡胶微粒混凝土,探讨橡胶微粒混凝土的抗压强度变化规律,以及在等强条件下不同橡胶微粒掺量对混凝土弹性模量的影响。结果表明:掺入橡胶后,混凝土的前期强度(3 d和7 d)发展较基准混凝土变缓,7 d以及14 d后强度出现较大幅度的增长,28 d后各个配比混凝土立方体抗压强度增幅不大;掺入一定量的橡胶后,混凝土的抗裂性能得到了一定程度的改善,橡胶微粒体积掺量越大,试件受压破坏后的完整性越好;掺入橡胶后,混凝土的弹性模量呈现出近乎线性的大幅下降趋势。 相似文献
70.
J. K. Krü ger W. Possart R. Bactavachalou U. Mü ller T. Britz R. Sanctuary P. Alnot 《The Journal of Adhesion》2004,80(7):585-599
The newly developed Brillouin microscopy is used for the first time to measure in situ the longitudinal elastic stiffness coefficient in the GHz-range inside of glass-epoxy-metal joints as a function of distance from the substrates. Interphases with a local variation of mechanical properties are quantitatively characterized. These interphases possess unexpected widths of tens to hundreds of microns. Inside the interphases, the spatial variation of the longitudinal stiffness coefficient depends on the type of substrate, on the curing conditions for the epoxy and probably on the distribution of internal stresses. The obtained spatial mechanical profiles provide valuable insight into the morphology-driven mechanics of the interphase, but additional information is needed for a full understanding of their physical and chemical origin. The presented results prove the sensitivity of the Brillouin microscopy; the elastic stiffness coefficients are detected with an accuracy in the subpercentage range. The spatial resolution is better than 10 µm. 相似文献