45号钢二次枝晶臂间距与冷却速度的关系

本文利用可控平均冷却速度的单向凝固实验炉测定了４５号钢在不同平均冷却速度下的冷却曲线，由此得到其在凝固期间的平均冷却速度Ｒ，相应地测量了不同平均冷却速度下试样的二次枝晶臂间距Ｓ２，通过回归，得到了如下关系式：Ｓ２＝７２７Ｒ－０．４１，并将引式成功地应用于实际生产中。     

生物降解型聚碳酸顺丁烯二酸亚乙酯 1、合成和表征

用CO_2、环氧乙烷、顺丁烯二酸酐进行三元共聚首次得到聚碳酸顺丁烯二酸亚乙酯(PECM),并用IR、~1H NMR、DSC等进行了表征,共聚物链中CO_2和MA单元随机分布,不饱和单元可在0～0.5mol分数之间调节。共聚过程不发生双键交联和构型转化。环氧乙烷的转化率可高达到93％。控制PECM链上的双键含量并使之发生自由基加成反应,得到对热较稳定的可溶性产物。     

A theory for the formation of tetrahedral amorphous carbon including deposition rate effects

A theoretical model is presented to describe the effect of ion beam bombardment rate on the formation of tetrahedral amorphous carbon (ta-C) films. The critical ion energy, E_c, corresponding to a 50% sp³ content in the films, is found to be dependent on both the effective thermal resistance and the ion beam bombardment rate. In the model, the ‘window’ width in the ion energy scale for the formation of ta-C material increases with decreasing deposition rate and with a reduction in the effective thermal resistance, until limited by lower and upper boundary thresholds. Experimental data are reproduced by the model. The plasmon energy, which correlates with sp³ fraction, is found experimentally of be higher for lower deposition rate and smaller effective thermal resistance. Data points for high sp³ content ta-C films deposited on silicon substrates at room temperature occupy a region in the ion energy-deposition rate (E-r) diagram similar to that predicated from the theory.     

低速爆轰管对黑火药的点传火性能研究

文章采用中心点火管结构的实验装置研究了黑火药的点传火性能。用低速爆轰 (L VD)中心点火管来点燃黑火药时 ,1# ～ 3# 大粒黑药的传火速度为 70 0 m· s-1～ 80 0 m· s-1数量级 ,燃烧波宽度在 3.1ms～ 3.5 ms,最大压力峰值 :1# 为 36 .4 MPa,2 # 为 2 4 .0 MPa,3# 为 38.0 MPa。用普通中心点火管点燃黑火药时 ,2 # 、3# 和钝化 2 # 大粒黑的传火速度分别为 6 1.2 m· s-1、6 8.2 m·s-1和 4 0 .1m· s-1,最大燃烧波宽度分别为 9.2 ms、6 .3ms和 9.5 ms。燃烧波表明 ,L VD中心传火管与普通中心传火管相比较 ,在传火管的不同位置处 ,前者的 P- t曲线一致性远高于后者。     

Evolution of BET internal surface area in glassy carbon powder during thermal oxidation

It is demonstrated that glassy carbon powder can be thermochemically activated. During activation, a film with open pores is created on the glassy carbon particles. This film has a large internal surface area, which is accessible to liquids and gases. A simple model for the evolution of the internal surface area in glassy carbon powder during thermochemical gas-phase oxidation is also presented and compared with experimental data. Experimental results are in qualitative agreement with the model. We found that a sharp particle size distribution is desirable with regard to potential technical applications.     

高水固结尾砂充填采矿充填体合理配比的研究

高水固结尾砂充填采矿是一种新型充填采矿法。试验测定了高水固结尾矿充填体的强度和变形特征；研究分析了影响充填体强度的主要因素、高水充填工艺的特殊要求，以及上向，下向进路开采对充填体强度和稳定性的要求，提出了满足支护强度，工艺及经济需求的充填材料的合理配比范围。     

片式多层电容电阻复合元件的研制

采用低温共烧陶瓷(LTCC)技术将电容、电阻元件集成在多层陶瓷基板里,构成了一种新型的片式多层复合元件,并研究了其制造工艺性能和频率特性。结果表明,片式多层电容电阻复合元件制造工艺适合批量化生产,并为片式多层LC滤波器、LTCC基板及器件的研发提供了极好的参考价值。     

喷锚结合水泥搅拌桩在基坑支护中的应用

结合紫金苑工程实例,分析喷锚结合水泥搅拌桩在基坑支护中的应用并总结施工、监测经验。     

Contemporary approaches to certification of measurement provision software

Contemporary approaches to the certification of measurement provision software are considered in domestic and overseas publications. Normative documentation is analyzed and a scheme is proposed for certification that takes account of the features of programs used for metrological purposes. __________ Translated from Izmeritel’naya Tekhnika, No. 5, pp. 65–68, May, 2007.