溶剂对助焊剂性能的影响

选用四种不同的醚与单一醇复配作为溶剂配制出四种助焊剂。通过扩展试验、润湿力试验和表面绝缘电阻测试,评价各种助焊剂的性能。结果表明,溶剂种类对焊料的平均扩展率、润湿性能和表面绝缘电阻均有影响;沸点与焊料熔点相近的溶剂所配助焊剂使焊料具有75.4%的平均扩展率;对活化剂有最好溶解能力的溶剂可提高润湿速率约12.5%。     

GaN蓝光LED电极接触电阻的优化

通过分析LED的工作电压和晶圆上两相邻N电极间电阻来讨论快速退火(RTA)和表面处理对GaN基蓝光LED接触电极的影响.研究了p-GaN表面处理对Ni/Au与p-GaN接触电阻的影响.结果表明,用KOH清洗p-GaN表面比用HCl清洗更能有效地改善Ni/Au与p-GaN的接触电阻.讨论了在氧和氮混合气氛下两种退火温度对P电极接触电阻的影响,当退火温度从570 ℃升到620 ℃时接触电阻升高.研究了氮气氛下不同退火温度和时间对LED电极接触的影响,发现在480 ℃下连续退火对N接触有利,但却使P接触变差,而450 ℃、10 min的氮气氛退火能同时得到较好P接触和N接触.     

丁二酸改性电子墨水用球形SiO2颗粒的FTIR及XPS分析

采用丁二酸对球状亚微米级SiO2颗粒进行表面改性,以提高SiO2颗粒于四氯乙烯溶剂中的电泳性能,制备适于电子墨水用的白色电泳颗粒。利用傅立叶红外光谱(FTIR)、X射线光电子谱(XPS)和Zeta电位粒度仪,研究了丁二酸改性SiO2颗粒的表面键合情况及其在四氯乙烯溶剂中的Zeta电位变化情况。研究发现,丁二酸仅有一端的羧基与SiO2颗粒表面的羟基发生酯化反应,而且当丁二酸的用量为3g(50mL乙腈中)时,接枝于SiO2颗粒表面的丁二酸的量达到最大值,此时C1s(O—CO)/Si(原子比)有最大值为5.77×10-2。Zeta电位测试结果表明,丁二酸改性后的SiO2颗粒在四氯乙烯中的Zeta电位比改性前的SiO2颗粒提高了约5.5倍。     

n-GaN上Ti/Al电极的表面处理与退火

实验研究了不同表面处理方法和不同退火条件对GaN上的Ti/Al电极的影响,用CH3CSNH2/NH4OH处理后的GaN材料的荧光光谱强度最高,在该材料上制作的Ti/Al电极的欧姆接触电阻率最小.通过欧姆接触电阻率,I-V曲线,X射线衍射等手段,分析了GaN与Ti/Al 电极接触表面在退火过程中的固相反应,提出了二次退火的方法.     

激光诱导放电毛化技术中放电坑的表面形貌研究

利用高重频YAG激光作用在固体表面所产生的等离子体使工件和电极之间在电压远低于击穿阈值的条件下产生放电。实验结果显示 ,放电坑基本上呈火山坑形 ,既有单坑结构 ,也有多坑结构 ,其形貌受到放电波形、电源极性、放电介质等因素的影响。放电坑表面形貌的规律是 :①除了涂油时的阳极放电坑是单坑结构以外 ,其他条件下的放电坑都是复合多坑结构 ;②单坑结构呈火山坑形 ,坑底为圆弧形 ,熔凝物堆积在坑的边缘 ,多坑结构则是一个大的放电坑中有多个凸起尖峰     

Characterization of surface roughness anisotropy on mismatched InAIAs/lnP heterostructures

We have studied surface roughness on mismatched In_0.65Al_0.35As epilayers of various thicknesses on (001) InP. The sample set spans the entire range from coherently strained to completely relaxed epilayers. As characterization tools, we have used atomic force microscopy (AFM), laser light scattering (LLS), and variable azimuthal angle ellipsometry (VAAE). AFM reveals that the surfaces are covered by densely packed ellipsoidal islands elongated along the [1-10] direction. The island size increases with layer thickness. Island anisotropy and the root mean square of the surface roughness increase with increasing thickness but decrease upon full lattice relaxation. LLS intensity displays a prominent azimuthal dependence that correlates well with the two-dimensional power spectrum of the surface topography, as predicted by theory. VAAE reveals a sinusoidal dependence of the ellipsometric parameter Δ on azimuthal angle. The amplitude of A correlates well with the short wavelength anisotropy of the surface power spectrum. Our work suggests that LLS and VAAE are fast, nondestructive, sensitive techniques for characterization of surface roughness in mismatched III-V heterostructures.     

扫描近场光学显微镜及其在生物微结构探测上的应用

扫描近场光学显微镜（ＳＮＯＭ）可探测生物体亚波长水平的光学特性，以接近分子水平的分辨率在生物微结构成象、探测和修饰等多方面有巨大的潜力。本文对ＳＮＯＭ的技术方法及其近期的的生物学应用进行了介绍。     

Low cost surface passivation for p-type mc-Si based on pseudobinary alloys (Al2O3)x(TiO2)1−x

The conventional process for back side passivation with full face Al screen printing layer is not suitable for very thin multicrystalline (mc-Si) solar cells and approaches to new technological processes are searched for. More investigations have been concentrated on local aluminum contacts and passivation coatings with different layers on mc-Si wafers. The aim of this work is to prove that (Al₂O₃)_x(TiO₂)_1−x is one promising candidate to be applied as passivation layer on multicrystalline Si. Investigations were performed on dielectric films of pseudobinary alloy (PBA) (Al₂O₃)_x(TiO₂)_1−x, prepared by chemical solution deposition known initially as sol–gel method. It was determined that their optical, dielectric and electrophysical properties are suitable for applications of these layers as back side surface passivation for thin multicrystalline silicon cells.     

晶粒超细化方法在降低材料表面能过程中的作用

利用分子动力学的原理计算了几种超细金属晶粒的表面能。研究表明:在超细化的晶粒尺寸范围内,材料表面能随晶粒尺寸的进一步减小急剧降低,而当晶粒长大到约20 nm后,材料的表面能则很快升至一个稳定的极限值——宏观尺寸材料的表面能值。对材料表面进行晶粒的超细化处理可使材料具有极低的表面能特性,这一特性可以应用于高黏度流体的减阻输送等领域。     

Shape optimization of inclined ribs as heat transfer augmentation device

This work presents numerical optimization techniques for the design of a rectangular channel with inclined ribs toenhance turbulent heat transfer.The response surface method with Reynolds-averaged Navier-Stokes analysis isused for optimization.Shear stress transport turbulence model is used as a turbulence closure.Computational re-sults for local heat transfer rate show a reasonable agreement with the experimental data.Width-to-rib height ratioand attack angle of the rib are chosen as design variables.The objective function is defined as a linear combina-tion of heat-transfer and friction-loss related terms with the weighting factor.Full-factorial experimental designmethod is used to determine the data points.Optimum shapes of the channel have been obtained in a range of theweighting factor.