氮离子注入的Ti6Al4V表面分析

利用表面分析技术(AES,XPS,SIMS)研究了经氮离子注入的外科植入材料Ti6Al4V表面成分与键合态,用轮廓仪的测量结果计算了氮离子注入深度及注入氮离子的Ti6Al4V的刻蚀速率。考虑到该合金的基体效应,对AES的定量结果进行了修正。结果表明,注入到合金中的氮离子与合金中的Ti形成高硬度的TiN,N的分布近似为Gauss形式,注入总深度约为350nm,在距表面约140nm处氮量最大,N与Ti的浓度比可达1.1。     

Effect of substrate surface roughness on the adherence of NiCrAlY thermal spray coatings

The adherence of plasma sprayed NiCrAlY bond coats can be improved by an appropriate substrate surface finish. The interface fracture energy for crack propagation along the coating/substrate interface has been measured for different surface roughness by means of a specially designed four-point bending test. An increase of the interface fracture energy of about 15% was observed for a three times higher surface roughness. In addition, four-point bending tests with the coating on the side face of bending specimens were performed to analyze the fracture and spalling behavior of the coatings both under large tensile and compressive substrate deformations.     

铝合金表面纳米化处理及显微结构特征

采用高能喷丸技术在1420铝合金上制备出纳米晶结构表层,利用X射线衍射仪、透射电子显微镜及高分辨电子显微镜研究由表层沿厚度方向的结构变化特征,并对硬度沿厚度方向的变化进行分析.结果表明:经过表面高能喷丸处理,样品表面形成了厚度约为20μm的纳米晶层,平均晶粒尺寸由约20 nm逐渐增加到约100nm;距表层约20～50 μm为亚微细晶层;表面纳米化的程度与塑性变形量有关;表面纳米化是通过位错滑移的塑性变形方式实现的;与样品的内部相比,表面硬度显著提高.     

模具型腔的几种精整加工方法的对比分析

通过对模具型腔工作面的几种精整加工方法的对比分析，研究和探讨如何提高模具型腔工作面质量的方法，并提出精整加工的发展方向。     

超音速微粒高能轰击16MnR钢表面纳米化的研究

采用冷气动力超音速微粒高能轰击技术对16MnR低合金钢表面进行处理,利用扫描电镜、透射电镜和X衍射方法对基体表面的微观形貌和结构进行分析.试验结果表明:试样经过超音速微粒轰击处理后可以使表层晶粒细化至纳米量级,平均晶粒的尺寸为14.2 nm;处理后表层主要产生压应力;处理后表层的显微硬度增加.     

SURFACE MODIFICATION ON STEEL BY RARE EARTH AND LASER TREATMENT

ＳＵＲＦＡＣＥＭＯＤＩＦＩＣＡＴＩＯＮＯＮＳＴＥＥＬＢＹＲＡＲＥＥＡＲＴＨＡＮＤＬＡＳＥＲＴＲＥＡＴＭＥＮＴ①ＳｈｅｎＹｉｆｕ１，２，ＦｅｎｇＺｈｏｎｇｃｈａｏ１，ＣｈｅｎＪｉｚｈｉ１，ＬｉａｎｇＹｏｎｇ１１ＩｎｓｔｉｔｕｔｅｏｆＭｅｔａｌＲｅｓｅａ...     

不锈钢活性激光焊工艺研究

以不锈钢SUS304作为试验对象,分别研究了焊接速度、散焦离焦量、激光功率和保护气体等工艺参数以及活性剂和活性元素硫对不锈钢YAG激光焊焊缝成形的影响.试验结果表明,各焊缝表面成形良好,焊接速度和激光功率能明显影响焊缝成形,散焦离焦量和保护气体种类对YAG激光焊焊缝成形的影响较小.与硫含量较低的情况相比,活性剂和活性元素硫含量较高的情况下均能使得焊缝熔宽发生明显收缩,随着热输入量增加,活性剂增加熔深的效果也越明显,表明活性剂对熔深的影响效果与焊接过程的热输入量有密切联系.     

SMT建模仿真研究现状及发展

概述了SMT再流焊工艺过程、所用组装件以及形成的焊点3方面的仿真进展，充分展现了计算机模拟在再流焊研究中的重要作用。     

利用石墨化膨胀消除球铁皮下气孔的研究

对影响球墨铸铁件皮下气孔的各种因素分析表明,铁液中气体的产生有其必然性,通过减少气体的发生量以防止皮下气孔的方法并不是都能奏效.基于此,提出了利用石墨化膨胀将已经产生的气体排挤出铁液来消除皮下气孔,并用实验进行了验证.     

Effects of anodizing voltage on the anodized and hydrothermally treated titanium surface

Anodic oxidation is the process of creating a titanium oxide layer with various defects more dense and stable. In this study, a dense, stable and porous oxide layer was formed using anodic spark oxidation on pure titanium surface and hydroxyapatite crystals were formed on its surface via a hydrothermal treatment. A mixture of 0.02M−GP (Glycerolphosphate disodium salt) and 0.2M-CA (Calcium acetate) was used as an electrolyte. By increasing the anodizing voltage to 220, 260, 300, and 360 V, the effects of the anodizing voltage were examined by evaluating the film properties after anodization and a hydrothermal treatment. Breakdown occurred around 230 V. As the voltage increased after breakdown, the pore size increased. After the hydrothermal treatment, the amount of HA crystal precipitation was also increased as the voltage increased. The mean surface roughness (Ra) of the anodizing surface was also increased as the voltage increased. The Ra value was larger in the hydrothermally treated group compared with the group treated with anodization as a result of the HA crystals present on the surface after the hydrothermal treatment. Corrosion resistance of the surface modified by anodization was significantly increased in a saline solution compared to that for the non-treated group; this increased further after the hydrothermal treatment. These increases were most likely due to a thick stable oxide layer formed through anodization. Thus, it is believed that titanium with its surface modified through anodic spark oxidation would be a suitable biomaterial due to its corrosion resistance and biocompatibility.