沥青油毡瓦国内外标准对比分析

从范围、原材料要求、组分要求、物理力学性能等方面对比分析了我国现行油毡瓦标准与欧美标准的区别,提出了我国制订沥青油毡瓦国家标准的的原则。     

测井新技术在四川油气勘探开发中的应用

综述随着四川盆地油气勘探深入所面临的油气领域复杂和困难的技术问题，介绍应用测井新技术为四川油气开发解决了大量的技术难题，特别是在复杂缝，洞型储层的评价，井旁地质构造形态精细分析和地质，测井，地震多学科结合储层横向预测等3个方面所取得的良好应用效果。     

标准物质在分析测试中的重要地位及发展前景

标准物质在分析测试领域中无论在定值，方法的研究，误差确定等方面都有着重要地位。标准物质的质量保证及正确使用也应引起我们重视。随着科学技术迅速发展标准物质有着广阔发展前景。     

用硫酸铁铵容量法测定钛精矿中二氧化钛含量

样品在过氧化钠熔融、水浸取及盐酸酸化后，在盐酸和硫酸介质中，隔绝空气，用金属铝将钛(Ⅳ)还原至钛(Ⅲ)，以硫氰酸盐为指示剂，用硫酸铁铵标准溶液滴定。     

碳素材料超声检测的信号处理方法

针对碳素材料超声无损检测存在信噪比较低的问题,从自相关性出发分析了典型超声检测信号的组成成分,提出了在自相关分析的基础上的小波去噪思想,探讨了自相关分析和小波分析相结合的信号处理方法。利用此方法进行实际超声信号分析效果良好。     

同位素中子源活化瞬发分析装置

一、基本原理自六十年代中期以来,中子活化瞬发γ射线元素分析技术(PNAA)得到人们广泛重视。与通常的中子活化分析(NAA)技术相比,它分析的是样品中的主要成分,若用同位素中子源,还可进行实时在线连续测定及现场分析。PNAA技术是用热中子与待测元素发生中子俘获反应,处于激发态的产物核在瞬间     

Physico-chemical properties of ceramic pigments for high-temperature application

Heat resistant coatings are required primarily for stacks, exhaust pipes, reactors, space crafts and similar equipments that are permanently or occasionally exposed to elevated temperatures. High-temperature coatings are generally based on silicone resin with ceramic and metallic pigments. In this study, iron oxide, cobalt oxide (thermo chromic compound) and aluminum oxide are used for the preparation of four new types of coloured pigments. The thermal resistant characteristics of these ceramic pigments were studied by differential thermal analysis, thermo gravimetric analysis and differential scanning calorimetric analysis. These ceramic pigments are found to be thermally stable up to 400 °C.     

Introduction of a nonlinearity measure for principal component models

Although principal component analysis (PCA) is an important tool in standard multivariate data analysis, little interest has been devoted to assessing whether the underlying relationship within a given variable set can be described by a linear PCA model or whether nonlinear PCA must be utilized. This paper addresses this deficiency by introducing a nonlinearity measure for principal component models. The measure is based on the following two principles: (i) the range of recorded process operation is divided into smaller regions; and (ii) accuracy bounds are determined for the sum of the discarded eigenvalues. If this sum is within the accuracy bounds for each region, the process is assumed to be linear and vice versa. This procedure is automated through the use of cross-validation. Finally, the paper shows the utility of the new nonlinearity measure using two simulation studies and with data from an industrial melter process.     

Feasibility analysis of membrane reactors – discovery of reactive arheotropes

A feasibility analysis methodology adopted from reactive distillation is applied to membrane reactors. A model is formulated to depict the reactive liquid phase composition on the retentate side of a continuous type membrane reactor. The effects of both the chemical reaction kinetics and the membrane mass transfer kinetics on the feasible products are elucidated by means of retentate phase diagrams and bifurcation analysis. The proposed method can be applied to various membrane processes, independent of the specific structure of the membrane. Two quaternary reaction systems are considered to illustrate the methodology. In the first hypothetical system, it is shown how selective membranes can influence the sequence of effective volatilities which in turn affects the feasible products of the system. In the second example of practical importance, i.e. the heterogeneously catalysed synthesis of propyl acetate coupled with permeation through a porous polycarbonate membrane, the dusty gas model is applied to describe the component fluxes through the membrane. For the latter reaction system, the existence of reactive arheotrope is demonstrated. Arheotropes represent mass transfer controlled feasible products of membrane separation process.     

甘三酯立体专一分析的研究：（Ⅱ）甘三酯立体专一分析方法初探

在第一部分综合讨论的基础上对甘三酯立体专一分析方法作了初步探讨。以液体油(菜油)及固体脂(猪脂)为基质,系统地研究了这一分析方法,取得了经验并补充了一些具体验证方法。分析液体油的结果与文献数据相一致,分析猪脂的结果欠佳,还存在一些问题需待进一步研究。