Flattening and solidification of thermally sprayed particles

In this article, molybdenum particles were plasma sprayed on copper, zirconia, and glass substrates. The impact of the molten particles was monitored using a fast two-color optical fiber pyrometer focused on a small spot on the substrate surface. The apparent duration of the flattening process and the cooling speed, both determined from the pyrometer signals, were found to depend on the substrate conditions and to vary with coating thickness. The substrate material and its roughness were also found to influence the texture in the sprayed coatings. Furthermore, a transient thermal flow numerical model was used to compute reliable thermal histories of the impinging particles and the underlying lamellae, the interfacial thermal resistance being determined by comparison of experimental thermograms with computed ones.     

Borides at interfacial zone of IC6 TLP bonded joints

1　INTRODUCTIONTransientliquidphase (TLP)bondingtechniquehasbeensuccessfullyusedinjoiningheatresistantal loys ,likeHastelloyX ,Inconel713C ,In10 0 ,Udimet5 0 0 ,70 0 ,MarM 2 0 0 ,0 0 7,2 4 7,30 2 ,Rene′80 ,TD NiCr ,MA75 4,6 0 0 0 ,PWA14 2 2 ,CSMX 2etc ,whicharesusceptibletohotcrackingor post weldheat treatmentcrackingproblemsduringfusionweld ing[14 ] .Inaddition ,therewerereportsofjoiningNiAlandTiAlintermetallicsbyTLPbondingmethod[510 ] .Forexample ,Galehadinvestigatedthemic…     

Current transients of passive iron observed during micro-indentation in pH 8.4 borate buffer solution

Micro-indentation test of passive iron electrode in deaerated pH 8.4 borate buffer solution was carried out to investigate the rupture and repair of passive film. During driving a conical diamond micro-indenter with a load of 0.1 N order downward to the electrode and driving upward from the electrode, a couple of anodic current peaks were observed. The first current peak spiked during loading was responsible for partial exposure of iron substrate to the solution due to rupture of the passive film when the indenter tip contacted. The second peak emerged during unloading when elastic deformation recovered, which was ascribed to repair at the ruptured sites. The second peak current was larger than the first one. Both peaks were sensitively influenced by electrode potential or concentration of sulfate ions containing in solution. The model for a series of rupture and repair processes of the passive film by micro-indentation was proposed to discuss the current transients.     

在VPO催化剂上丁烷选择氧化的质谱研究

The selective oxidation of n-butane to maleic anhydride(MA) on a vanadium-phosphorus oxide (VPO) catalyst was studied using on-line gas-chromatography combined with mass spectrometry(GC-MS) and transient response technique.The reaction intermediates,butene and furan,were found in the reaction effuent under near industrial feed condition (3% butane 15% O2),while dihydrofuran was detected at high butane concentration (12% butane,5%O2).Some intermediates of MA decomposition were also identified.Detection of these intermediates shows that the vanadium phosphorus oxides are able to dehydrogenate butane to butene,and butene further to form MA.Based on these observations,a modified scheme of reaction network is proposed.The transient experiments show that butane in the gas phase may directly react with oxygen both on the surface and from the metal oxide lattice,without a proceeding adsorption step.Gas phase oxygen can be adsorbed and transformed to surface lattice oxygen but it can not participate in selective oxidation.Adsorbed oxygen leads to deep oxidation,while lattice oxygen leads to selective oxidation.     

Dynamic compensation by fusing a high-speed actuator and high-speed visual feedback with its application to fast peg-and-hole alignment

This paper presents a dynamic compensation concept to grapple with the dynamic defects of a traditional robot arm, especially while performing high-speed endpoint regulations. The proposed high-speed dynamic compensation concept offers a new point of view for cooperating with a traditional manipulator to realize highly dexterous performance of manipulations. The concept is realized through adoption of a high-speed light-weight actuator as well as endpoint closed loop configured high-speed cameras. The dynamic compensation is analyzed experimentally with 1000 Hz visual feedback and a high-speed finger for a robot arm in the case of one degree of freedom. The advantage of the proposed approach is that the modeling for the robot system’s dynamics is not needed, whereas it is necessary and trivial in order to realize high-speed regulations by traditional approaches. Thus, the control issue becomes easier with the proposed approach. As an application for this concept, fast peg-and-hole alignment with large position and attitude uncertainty is studied. The alignment algorithm is based on a visual compliance strategy. Alignment experiments show that with the proposed concept of dynamic compensation as well as visual compliant motion control, robust and fast convergence was realized for most cases.     

基于局部自适应先验MRF模型的快速BP图像分割算法

针对常规MRF分割模型不能有效描述图像的局部特征、常导致图像的过分割现象,提出了一种局部自适应先验的MRF模型。该模型利用图像的邻接区域信息建立了一种局部自适应特征MRF模型。基于提出的模型,建立了一种具有快速收敛策略的区域BP算法对MRF模型的区域消息进行传递,有效解决了区域BP算法的计算量大的问题。实验结果表明,与常规区域BP算法相比,提出的分割方法具有更快的分割速度和精度。     

NH3-NO/NO2 SCR for diesel exhausts after treatment: mechanism and modelling of a catalytic converter

We review herein the key mechanistic and kinetic features of the reactions involved in the NH₃-NO/NO₂ SCR system investigated by dynamic reactive experiments over a V-based commercial powdered catalyst, eventually leading to the proposal of an original redox scheme which accounts for stoichiometry, selectivity and intrinsic kinetics of the global SCR process.     

基于单轴速率转台的角速度传感器标定方法

针对传统的标定方法标定成本高且对北向基准的要求严格等问题,提出了一种用单轴速率转台作为标定设备的光纤陀螺捷联航姿系统标定方法。对光纤陀螺组合的误差进行建模,将光纤陀螺捷联航姿系统安装于单轴速率转台上,使光纤陀螺捷联航姿系统的3个陀螺轴向分别朝下进行标定实验,由此标定出3只光纤陀螺的零偏、标度因数和安装失准角共12个误差参数。通过对标定精度进行分析,验证了该方法的可行性,其标定成本低且不需要北向基准,具有一定的工程应用价值。     

Calmodulin Supports TRPA1 Channel Association with Opioid Receptors and Glutamate NMDA Receptors in the Nervous Tissue

Transient receptor potential ankyrin member 1 (TRPA1) belongs to the family of thermo TRP cation channels that detect harmful temperatures, acids and numerous chemical pollutants. TRPA1 is expressed in nervous tissue, where it participates in the genesis of nociceptive signals in response to noxious stimuli and mediates mechanical hyperalgesia and allodynia associated with different neuropathies. The glutamate N-methyl-d-aspartate receptor (NMDAR), which plays a relevant role in allodynia to mechanical stimuli, is connected via histidine triad nucleotide-binding protein 1 (HINT1) and type 1 sigma receptor (σ1R) to mu-opioid receptors (MORs), which mediate the most potent pain relief. Notably, neuropathic pain causes a reduction in MOR antinociceptive efficacy, which can be reversed by blocking spinal NMDARs and TRPA1 channels. Thus, we studied whether TRPA1 channels form complexes with MORs and NMDARs that may be implicated in the aforementioned nociceptive signals. Our data suggest that TRPA1 channels functionally associate with MORs, delta opioid receptors and NMDARs in the dorsal root ganglia, the spinal cord and brain areas. These associations were altered in response to pharmacological interventions and the induction of inflammatory and also neuropathic pain. The MOR-TRPA1 and NMDAR-TRPA1 associations do not require HINT1 or σ1R but appear to be mediated by calcium-activated calmodulin. Thus, TRPA1 channels may associate with NMDARs to promote ascending acute and chronic pain signals and to control MOR antinociception.     

基于FFT的陀螺寻北仪误差补偿

传统提高陀螺寻北仪精度的方法主要是选用高精度陀螺、提高转位精度、增加转位数、通过数字滤波消除外界干扰等,这些方法大多针对寻北仪的某方面误差因素进行改进,而对寻北仪整体的误差特性研究较少。通过对陀螺寻北仪综合误差特性的分析,提出了基于快速傅立叶变换(FFT)的寻北仪误差补偿方法。该方法首先测量出寻北仪的整周误差,然后通过求取FFT系数完成对寻北仪的系统级误差补偿,该方法尤其对寻北仪制造过程中的结构误差和测量元件的常值漂移残差具有良好的补偿效果。经产品验证可以在保持现有陀螺和转位精度不变的情况下,提高寻北精度3倍以上,具有良好的工程实用价值。