酸溶性钛渣酸解工艺研究

针对攀枝花钛铁矿冶炼钛渣的物化性质，对影响钛渣酸解率和钛液指标的各个因素进行了全面系统的实验室研究，并在年产2000t钛白生产线上进行了工业验证和优化试验，酸解率稳定在93％以上，三价钛控制在1－3g/L，钛液浓度较钛矿酸解提高了40－50g/L，其它钛液指标达到了后续水解工艺的要求。     

One‐step production of 2,3‐butanediol from starch by secretory over‐expression of amylase in Klebsiella pneumoniae

BACKGROUND: 2,3‐Butanediol (2,3‐BD) is a valuable chemical that can be biosynthesized from many kinds of substrates. For commercial biological production of 2,3‐BD, it is desirable to use cheap substrate without pretreatment, such as starch. However, there have been few reports on the production of 2,3‐BD directly from starch. RESULTS: In this work, gene malS coding for α‐amylase (EC 3.2.1.1) precursor was inserted into plasmid pUC18K, and secretory over‐expression of α‐amylase was achieved by engineered Klebsiella pneumoniae. The extracellular recombinant amylase accelerated the hydrolyzation of starch, and one‐step production of 2,3‐BD from starch was carried out by engineered K. pneumoniae. A 2,3‐BD concentration of 3.8 g L^?1 and yield of 0.19 g 2,3‐BD g^?1 starch were obtained after 24 h fermentation. CONCLUSION: The one‐step production of 2,3‐BD from starch was achieved by secretory over‐expression of amylase in K. pneumoniae. This would simplify the process and reduce the production cost considerably by enabling use of starch with minimal pretreatment. Copyright © 2008 Society of Chemical Industry     

Material removal and surface damage in EDM of Ti3SiC2 ceramic

Material removal and surface damage of Ti₃SiC₂ ceramic during electrical discharge machining (EDM) were investigated. Melting and decomposition were found to be the main material removal mechanisms during the machining process. Material removal rate was enhanced acceleratively with increasing discharge current, i_e, working voltage, u_i, but increased deceleratively with pulse duration, t_e. Microcracks in the surface and loose grains in the subsurface resulted from thermal shock were confirmed, and the surface damage in Ti₃SiC₂ ceramic led to a degradation of both strength and reliability.     

纳秒级上升时间的高压脉冲群电源

按照IEC 61000-4-4/GB 17626.4—1998的要求，首先应用PSPICE仿真确定电路中各元件的参数值，然后基于拉普拉斯变换用MATLAB求解二阶电路验证各元件参数。在此基础上研制了一台以开关电源作为高压直流电源、以氢闸流管作为主控开关的脉冲群电源。该电源体积小、重量轻、效率高、成本低廉。试验结果表明，其输出信号符合标准要求，可用于快速瞬变脉冲群抗扰度试验。     

二元复合驱阶段见效特征

针对孤东油田油藏条件，通过室内试验研究，确定了以胜利石油磺酸盐为活性剂主剂和聚合物的二元复合驱油体系，通过两者之间的协同效应，增加水驱波及体积和洗油效率。该体系在孤东油田七区西馆上54—61层进行试验，取得了较好的阶段性降水增油效果。本文分析了复合驱见效特征和影响见效因素，为下步跟踪分析调整具有指导意义。     

4-氨基-3-肼基-5-巯基-1,2,4-三唑的合成及其对醛的检验

以硫脲和水合肼合成了可用于检验醛的试剂——4-氨基-3-肼基-5-巯基-1，2，4-三唑(别名：紫醛)，其结构通过红外光谱、核磁进行了确定。试验表明，紫醛对醛的检验敏感、专一、快速、操作简单。     

一种廉价实用的双积分A/D转换器

介绍用51单片机和通用分立器件构成的双积分A／D转换器，文中给出了详细的源程序清单。     

控制W9Cr3Mo4V低倍碳化物剥落的工艺改进

针对W9Cr3M04V轧制成品材低倍碳化物剥落的形成原因分析，得出一次碳化物颗粒粗大、在1／4D至中心区域聚集是导致低倍热酸浸试验碳化物剥落的主因；由此进行冶炼过程中注速（锭形）、浇注温度选择对比工艺试验，得出在原有冶炼＋轧制的工艺基础上选用2．2t锭、降低浇注温度（1489℃）能有效改善一次碳化物颗粒大小和聚集程度，进而有效降低低倍碳化物剥落倾向。     

汽车排放控制系统中的氧传感器现状及展望

介绍了浓差型(Nernst型)、极限电流型和半导体电阻型等汽车排放控制系统中的氧传感器原理及结构。在综合该领域国内外研究现状的基础上,对氧传感器的发展进行了展望。     

水调信息发布系统的设计与实现

在分析水电厂水调信息体系结构和应用需求的基础上,探讨采用现代信息技术构建基于交互式Web、自报/查询短消息、自动收发邮件及自动应答语音等的水调信息发布系统,从而实现多途径水调信息的发布、查询和管理,以解决水电厂单一模式的水调信息发布方式,提升水调信息多途径传递方式,以及信息传递的实时性和可靠性.