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11.
Debasmita Das Purabi Rani Samaddar Pratik Kumar Sen Kaushik Das 《Journal of Applied Electrochemistry》2008,38(6):743-749
Galvanostatic steady state current potential measurements were carried out for oxidation of a series of aliphatic alcohols
having varying number of hydroxyl groups. The anodically deposited layer of MnO2 on platinum was used as the electrode material. The deposit was characterised by scanning electron microscopy (SEM), energy
dispersive X-ray analysis (EDAX) and electrode potential measurements. The catalytic role of MnO2 in the electro-oxidation of alcohols was indicated by the chronopotentiograms and the cyclic voltammograms. An analysis of
the electrochemical data indicated a catalytic EC mechanism in which Mn (V) is generated electrochemically and consumed chemically
in succession. Based on this and the hydrogen bonding interaction between alcoholic hydroxyl groups and MnO2 layer, a mechanism was proposed which accounts for the variation in the observed electrochemical reaction orders. Tafel behaviour
was found to be followed only approximately. Current efficiency of the electrochemical oxidation of polyols was studied. Replacement
of platinum by carbon as current collector was found to leave the electrocatalytic activity of the MnO2 deposit practically unaltered. 相似文献
12.
Teresa Łuczak 《Journal of Applied Electrochemistry》2008,38(4):469-476
The electrooxidation of phenylethanolamine (2-amino-1-phenylethanol) at a gold electrode in alkaline electrolyte has been
studied. Measurement of the differential capacitance of the electric double layer versus the electrode potential has shown
that the adsorption of phenylethanolamine at the gold-solution interface plays a significant role in the oxidation mechanism.
The effect of amine concentration, electrolyte pH and potential scan rate on the electrooxidation is analysed. 相似文献
13.
14.
S. Zisekas G. Karagiannakis C. Kokkofitis M. Stoukides 《Journal of Applied Electrochemistry》2008,38(8):1143-1149
The reaction of NH3 decomposition was studied on Ag in a proton conducting double chamber cell-reactor. The proton conductor was a strontia-ceria-ytterbia
(SCY) perovskite of the form SrCe0.95Yb0.05O3−α. The reaction was studied at 350–700 °C and atmospheric total pressure. The proton transference number (PTN) was calculated
by simultaneous measurement of the imposed current and the proton flux and it was found to vary between 0.5 and 0.7. The effects
of imposed current, temperature and inlet gas composition on the reaction rate and the PTN, were examined. Although the faradaic
efficiency (Λ) remained near unity in all experiments, reaction rate enhancements (ρ) as high as 57 were achieved. An up to
90% decrease in the activation energy of the reaction was observed when protons were electrochemically “pumped” away from
the catalyst. 相似文献
15.
16.
吴静 《中国材料科技与设备》2007,4(3):22-25
在近几年的InAs/GaAs自组织量子点的研究中,如何荻得1.3~1.55μm。长波长量子点材料是一个很热门的课题。本文综述了各种延长自组织InAs/GaAs量子点发光波长的方法,并提出了实用化的最佳途径。 相似文献
17.
We report here a non-enzymatic detecting electrode strip for fast monitoring of uric acid in human whole blood. A single-use amperometric uric acid sensor strip, incorporating a three-electrode configuration, has been fabricated on a polypropylene substrate using low cost screen-printing (thick-film) technology. Both the working and counter electrodes were prepared by screen-printing commercial carbon ink. The integration on the same support of pseudo-reference electrode was obtained by screen-printing a commercial silver ink and subsequent electrochemical pretreatment. Simply by placing a 20 μl human whole blood drop on the strip is enough for uric acid analysis by square-wave voltammetry. Real human whole blood samples were analyzed by this method and compared to the phosphotungstic acid clinical test procedure with satisfactory results. 相似文献
18.
Yoo‐Seong Kim Woong‐Sik Kim Hak‐Nyun Choi Tae‐Geum Koh Yong‐Seog Kim 《Journal of the Society for Information Display》2007,15(3):199-204
Abstract— Among various barrier‐rib manufacturing processes, the mold‐pattern‐transfer method has potential to reduce processing cost as well as the manufacture of high‐resolution pixels. In this study, the effects of major processing variables of the mold‐pattern‐transfer process on the formation of air‐trapped pores within barrier ribs were examined. The results indicated that with an optimum combination of the processing variables, barrier ribs without trapped defects can be produced, demonstrating the possibility of reducing the number of processing steps and costs of barrier ribs. 相似文献
19.
采用微波高压制样技术,快速提取饲料中的氟元素,结合氟离子选择性电极标准添加和电位极差测试方法,能够快速、准确地测试饲料中的含氟量 相似文献
20.
Jian‐Peng Cui Feng Zhou Chengqun Song Quan‐Min Zhong Qiong‐Hua Wang 《Journal of the Society for Information Display》2012,20(6):347-350
Abstract— A low‐voltage (~10 Vrms) and high‐transmittance (~90%) polymer‐stabilized blue‐phase liquid‐crystal (BPLC) device with a slanted‐electrodes structure is proposed. Unlike the vertical‐field‐switching (VFS) mode in which oblique incident light and a vertical field are employed, the proposed device utilizes normal incident light and an oblique field. The slanted electrodes generate a strong and uniform oblique electric field, which contributes in obtaining low voltage and high transmittance. Moreover, no couple films or prism sheets are needed, which helps to enhance the optical efficiency and simplify of the device structure. This device has great potential application for emerging BPLC displays and photonic devices. 相似文献