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71.
The interaction of different metal oxides such as Co3O4, NiO, Al2O3, Cr2O3, Fe2O3 and SiO2 with Na2SO4 at a temperature of 1100 and 1200 K in flowing oxygen has been studied. The thermogravimetric studies for each system were
carried out as a function of Na2SO4 in the mixture. The presence of different constituents in the reaction products were identified by X-ray diffraction analysis
and the morphologies of the reaction products were characterized using metallography and scanning electron microscopy (SEM).
The formation of products was also investigated by thermodynamic computation of free energies of the reactions and the study
of relevant equilibrium phase diagrams. The soluble species in the aqueous solutions of the reaction products were determined
quantitatively using atomic absorption spectrophotometry.
The high temperature interaction products usually contain a 3-phase structure namely, Na2O·M2O
x
, M2O
x
and metal sulphide and/or metal sulphate. The formation of Na2O·M2O
x
depends upon the solid state solubility of metal oxide in the molten salt at high temperatures. Under limited solubility
conditions Na2O·M2O
x
is invariably formed, but as soon as this condition is relaxed the oxide. M2O
x
, precipitates and forms a separate phase. 相似文献
72.
从理论上探讨了磁阻率效应,叙述了精密角位移传感器的工作原理及结构设计。传感器的分辨率已达0.01°,通过可靠性寿命试验,传感器的失效率λ(t)<1×10-7/h。 相似文献
73.
Directional solidification studies of gelatinized corn starch-water mixtures were undertaken in order to examine, in situ, the freezing behavior of this food model. The solidification rate was controlled by varying sample cell velocity as it moved from a 25°C hot stage to a -25°C cold stage. While freezing at cell velocities ≤7.5 μm/sec, starch granules were alternately pushed or entrapped by the advancing solid-liquid interface producing a segregated structure consisting of alternating high-starch and low-starch bands. At a cell velocity of 10 μm/sec, the frozen product was homogeneous. The relationship between the solid-liquid interface velocity and segregation behavior was quantified and compared to an existing model of particle-interface interactions. 相似文献
74.
根据转炉炼钢的物理化学反应机理,从质量平衡和能量平衡的计算出发,通过小参数变动,导出了增量式静态模型中矿石方程和供氧方程的系数。所得结论与新日铁资料基本相符。同时,还进行了炉料和产物的计算,分析了改变废钢比对生产的影响。 相似文献
75.
Quasi-static and dynamic crushing behaviors of aluminum and steel tubes with a cutout 总被引:3,自引:0,他引:3
Tubular members are commonly used as an energy absorber in engineering structures and many such members have a cutout. In this study, the crushing behaviors of tubes with a cutout are characterized and the effects of cutout on the energy absorption capabilities of these tubes are quantified. Systematic parametric studies were carried out to study the effect of material properties, including yield and ultimate strength of material, strain rate effect, location of cutout, tube length and impact speed on the crushing behaviors and energy absorption capacity of aluminum and steel tubes. First, a numerical model was constructed with a commercial explicit finite element code. It will be first proven that the numerical simulation can produce sufficiently accurate results in an economic manner. Subsequently, the crushing behavior of aluminum and steel tubes with a cutout was experimentally characterized and their energy absorption capacity was evaluated in terms of mean crushing force, peak crushing force and specific energy absorption (SEA). Tubes of various lengths with a cutout located at different locations, subject to both quasi-static and dynamic impact loadings were considered. For steel tubes, the numerical simulation investigated the influence of the strain rate effect and variation in strain hardening ratio of the material. Empirical equations describing the mean and peak crushing forces of aluminum and steel tubes with a cutout were developed using linear and nonlinear regression methods applied to the results obtained from the numerical and experimental studies. 相似文献
76.
Results of metal testing in impact tension–compression and indentation are analyzed. As the analysis of these data demonstrates, the strength of metals increases greatly with strain rates and at moderate indentation rates. At high indentation rates, a decrease in the specific energy (per unit volume of a displaced material) necessary for the formation of a conical cavity was observed. The account of the effects of viscosity, temperature increase upon plastic deformation and its localization can be used to explain the above phenomena. 相似文献
77.
References: 《中国炼油与石油化工》2007,(3):35-42
The proton nuclear magnetic resonance spectroscopy (1H-NMR), the synchronous fluorescence spectrometry (SFS) and the ruthenium ions catalyzed oxidation (RICO) method were used to determine the chemical structure of polyaromatic nucleus in Oman residue fractions. The results of 1H-NMR analyses showed that the average numbers of aromatic rings in the aromatics, resins and asphaltenes units were 3.2, 5.6 and 8.2, respectively. SFS was used to investigate the distribution of aromatic rings in residue fractions, the main distribution range of aromatic rings in aromatics, resins and asphaltenes were 3 4 rings, 3--5 rings and more than 5 rings, respectively. The aromatic network in residue fractions was oxidized to produce numerous carboxylic acids. The types and content of benzenepolycarboxylic acids, such as phthalic acid, benzenetricarboxylic acids, benzenetetracarboxylic acids, benzenepentacarboxylic acid and benzenehexacarboxylic acid disclosed the condensed types of aromatic nuclei in the core. The biphenyl fraction (BIPH), the cata-condensed fraction (CATA), the peri-condensed fraction (PERI) and the condensed index (BCI) were calculated based on the benzenepolycarboxylic acids formed. The results implied that there was less biphenyl type structures in all residue fractions. The aromatics fraction was almost composed of the cata-condensed type system, and the asphaltenes fraction was wholly composed of the peri-condensed type system, while in the resins fraction co-existed the two types, herein the peri-con- densed type was predominant over the cata-condensed type. Based on the analytical results obtained in the study, the components --aromatics, resins and asphaltenes -- were given the likely structural models. 相似文献
78.
79.
80.