Dielectric Resonators for the Measurement of Superconductor Thin Films Surface Impedance in Magnetic Fields at High Microwave Frequencies

We present the design and realization of cylindrical dielectric resonators operating in the 40–60 GHz frequency range, designed for the measurement of the surface resistance and of the surface reactance shift in High-T _c Superconductors (HTS) thin films in a dc magnetic field. The resonators are single tone, based on the TE ₀₁₁ mode, and multiple tone, the latter allowing in principle to exploit the simultaneous determination of the surface impedance at different frequencies. As an application example, we report the temperature and field dependencies of the effective surface impedance of some cuprate superconductors thin films. The results are compared with those obtained through the use of a standard metal cavity with a similar Q-factor and operating in the same frequency range. The comparison highlights a superior stability and a higher sensitivity, resulting in an increase of about two orders of magnitude in the resolution of the surface impedance measurement. By contrast, the dissipative part of the superconducting transition (above T/T _c = 0.97) is better studied with the metal cavity. We also present measurements in the vortex state in YBaCa₂Cu₃O_7−δ and Tl₂Ba₂CaCu₂O_8+x that show significantly different physics. PACS: 74.25 Nf.     

催化裂化原位降硫助剂的制备及其性能研究

采用溶胶-凝胶法制备具有介孔结构的降硫基质材料，选择具有降硫选择性的活性元素对合成的基质材料进行改性处理，考察不同的改性方法对制得的催化裂化原位降硫助剂性能的影响，并对基质材料和降硫助剂的结构进行表征。采用美国进口的ACE-R小型催化裂化评价装置将降硫助剂与催化裂化催化剂匹配进行性能评价，在不改变原催化裂化产品分布和产品性质的同时，降低原料的总硫含量，总硫降低可达40％以上。     

Imaging the domain pattern of the canted magnetization state in Co/Pt multilayer films

The exact magnetization pattern of magnetic films close to a spin-reorientation transition is difficult to analyze due to the intrinsically three-dimensional (3d) variation of the orientation of the local magnetization. We present a technique how this can be performed, based on the analysis of high quality 2d polarization maps from a single scanning electron microscope with polarization analysis (SEMPA) measurement with tilted sample. The key tool is the statistical distribution of all occurring polarization doublets, visualized in a 2d histogram plot. From the shape of the distribution the type of transition—canted-phase, or coexisting phases—can be inferred. For the canted-phase state, the canting angle can be accurately determined from geometrical considerations. With help of the histogram the image data can be analyzed and the three components of the magnetization can be calculated for most points of the image. For a Co/Pt multilayer film we found a cone state. The magnetization forms a complex pattern consisting of out-of-plane domains while the in-plane magnetization shows a maze pattern.     

Facile synthesis of nanocrystalline zinc ferrite via a self-propagating combustion method

Macroporous nanocrystalline zinc ferrite with single spinel-phase was prepared by a facile self-propagating combustion method using zinc nitrate, iron nitrate and glycine. The as-prepared ZnFe₂O₄ were characterized by X-ray diffraction (XRD) analysis, N₂ adsorption, scanning electron microscopy (SEM), high-resolution transmission electron microscopy (HRTEM), selected area electron diffraction (SAED) and energy dispersive X-ray spectrum (EDS). The magnetic properties of the prepared ZnFe₂O₄ were also studied.     

汽轮机轴承烧瓦与轴颈的渗巴氏合金现象

简述轴承工作性质，巴氏合金应用与相组成的基本情况。论述汽轮机转子在两个电厂长期运行后，由于轴颈发生的不正常摩擦损伤，在大修改造中由无损检查、机械加工揭示出轴颈存在严重的渗巴氏合金现象，低熔点金属Sn、Sb与Cu向转子材料晶界的深层渗入最终导致了3根大型在投转子的严重开裂与报废。图11表2     

一种抗干扰能力极强的计算机通信接口电路

设计了一种结构简单，抗干扰能力极强的计算机通信接口电路。该电路利用模拟开关实现了全数字二态电平（1，0）与三态电平(1，0，-1)之间的相互转换；利用模拟开关导通电阻的动态效应以及MOS晶体管开启电压Vτ的衬偏效应，提高了接收电路的抗干扰能力，提出了一种与共模干扰无关的模拟数字混合接收电路。     

非平面对称磁场的空间展开及样条函数表述

为了研究带电粒子光学系统的光学特性,需要知道系统中磁场的空间分布。实际磁场往往不具有严格的平面对称性质,一些作者曾就这类磁场的空间展开做过不少工作。但他们的工作是在柱坐标系统中进行的,适用于诸如回旋加速器、双向聚焦磁分析器、环形磁β谱仪等一类装置的磁场分析。对于大型同位素电磁分离器(calutron)那样一类装置,其磁场分布需要     

Design of a robust controller for a supersonic aircraft using H∞ approach

In this paper an H_∞ optimal, robust flight control system design for a supersonic aircraft has been described. Separate controllers are designed for longitudinal and lateral motions. A general two-degrees-of-freedom controller is proposed, where feedback control is designed for robust performance augmentation, while a series compensator is used to ensure that requisite handling qualities. Three alternative methods to achieve performance robustness have been discussed. The results obtained are very encouraging. It is hoped that this will equip the flight control engineers with an alternative to the conventional methods.     

二(二甲苯基)丙烷合成工艺的研究

二氯丙烷(DCP)与二甲苯在混合金属氯化物催化剂(HD90)作用下合成二(二甲苯基)丙烷,生产过程简单,产品收率高。在60—80℃的温度下,二甲苯与二氯丙烷摩尔比为6∶1,HD用量50克/摩尔DCP的条件下反应5—6小时,二(二甲苯基)丙烷的收率可达88％以上。