Cu2O-CuAlO2-Cu基金属陶瓷导电性能研究

通过热压技术制备Cu2O-10CuAlO2-xCu金属陶瓷材料，并对其导电性能进行了研究。结果表明，Cu2O-10CuAlO2-xCu在Cu含量超过15wt．％后呈金属导电性。材料的微观结构观察及物理性能测试表明，金属陶瓷材料的电导率不仅取决于材料的金属相含量，还取决于金属相颗粒尺寸和孔隙率的大小。材料中金属相的颗粒尺寸取决于热压工艺参数，随着热压温度的升高而增大，但随热压压力的升高而减小。     

Fat-simulating and accelerating solvents for polyolefins and MWD of solvent extracts of polyethylenes

Migration kinetics of straight-chain oligomers and antioxidants from several polyolefins at different temperatures into various solvents have been studied by radioactive tracer techniques. Anhydrous ethanol appears to be a well suited food-oil or liquid-fat simulant for extracting different types of migrants from polyolefins. Pure and mixed triglycerides are also good oil or fat simulants, but the triglycerides offer no simpler analytical procedures than the use of oil or fat themselves. n-Octanol may also be considered as a reasonable oil or fat simulant; however, its action depends somewhat on the choice of migrants. The accelerating action of n-heptane over that of oil or simulants is quantitatively demonstrated. The accelerating effects are greater for migration systems with lower diffusion coefficients. The diffusion coefficients for migration into n-heptane are about 20 times greater than the diffusion coefficients into ethanol or oil for otherwise identical migration systems yielding diffusion coefficients of about 10^?7 cm²s^?1 into oil or ethanol. For systems yielding diffusion coefficients into oil or ethanol of about 10^?12 cm²s^?1, the corresponding diffusion coefficients into n-heptane are about 1000 times greater. The molecular weight distributions (MWDs) of the n-heptane and ethanol extracts of polyolefins have been analysed. n-Heptane can not only accelerate the migration of the individual migrant but also remove oligomer species that are slightly soluble or present at low levels in the oil or simulant extracts.     

Pickup (critical) velocity of particles

This work presents experimental results on pickup velocity (critical velocity) measurements for a variety of particulate solids. The present experiments together with previously published experiments of a number of researchers encompass about 100 measurements of 24 materials for a wide range of particle sizes, shapes and densities. Based on the experimental results, three zones are defined by establishing simple relationships between the Reynolds and Archimedes numbers. The empirical relationships were further modified by taking into account the pipe diameter and particle shape (sphericity). The three-zone model was shown to reasonably correlate to Geldart's classification groups.     

A survey on nature-inspired optimization algorithms with fuzzy logic for dynamic parameter adaptation

Metaheuristic optimization algorithms have become a popular choice for solving complex problems which are otherwise difficult to solve by traditional methods. However, these methods have the problem of the parameter adaptation and many researchers have proposed modifications using fuzzy logic to solve this problem and obtain better results than the original methods. In this study a comprehensive review is made of the optimization techniques in which fuzzy logic is used to dynamically adapt some important parameters in these methods. In this paper, the survey mainly covers the optimization methods of Particle Swarm Optimization (PSO), Gravitational Search Algorithm (GSA), and Ant Colony Optimization (ACO), which in the last years have been used with fuzzy logic to improve the performance of the optimization methods.     

无机物——聚醋酸乙烯复合乳液粒子结构及主要性能

本文对均聚醋酸乙烯乳液及其与无机物的混合物,无机物——聚醋酸乙烯复合乳液的粒子结构进行了比较,阐述了复合乳液的主要性能。     

IMAGING OF PARTICLE MOTION IN FLUID-SOLID SYSTEMS USING A GAMMA CAMERA

A new approach is presented for the characterization of particle motion in fluid-solid systems based on dynamic imaging with a gamma scintillation camera. A two-dimensional spouted bed of 200-500 micron diameter anion exchange resin beads was used as a test system. One or several beads were radiolabeled with the 140 keV gamma emitting radionuclide 99m-Tc pertechnetate, and particle velocity, panicle path, the spatial distribution of particle residence times, and local bed density were determined from the measured temporal and spatial distributions of particle activity. While care must be exercised in the interpretation of data when the scale for changes in the spatial distribution of activity approaches the limits of camera resolution, the method is quantitative, non-invasive, and well suited to the study of systems having symmetry in one spatial dimension.     

Measurement of the size, shape and orientation of convex bodies

Different types of solid bodies (particles) with specific shape and size are needed for industrial processes. For spherical particles, ‘sizer’ measurements are usually reported as sphere diameters. For non-spherical particles, particle shape and especially orientation must be taken into account. Particles of a specific shape will present different views when looked at from different directions.We have employed a Camsizer^® instrument to measure the distribution of projected area under different physical conditions for solid cylindrical particles:

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Under ‘ideal’ conditions, corresponding to a uniform distribution of particle orientation, measurements agreed with predictions. The celebrated theorem of Cauchy applies only to this case.

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For two other situations, measured and predicted results differed. However, from the experimental data it was possible to infer the particle orientations and hence theoretically predict the projected area distribution. Excellent agreement between theory and practice was then restored.

     

磁盘阵列环境下的取证目标系统重构

封存原始硬盘与业务系统服务的连续性是计算机取证中面临的一对矛盾。在独立硬盘环境中,问题的解决并不困难,但在磁盘阵列(RAID)环境下,目前还缺乏有效的解决办法。为此,为RAID环境下的取证目标系统的重构提出一套解决方案,并设计实现其中关键任务的处理软件。实验表明,该方法可适用于不同RAID等级、不同操作系统下的系统重构,使得用户感受不到重构得到的系统与原系统有任何差异。与数据同步方法相比,该方法可以有效地减少重构的时间开销,且不会破坏原始证据硬盘上的数据。     

THE EFFECT OF PRECIPITATION PARAMETERS ON PREPARATION OF LITHIUM FLUORIDE (LIF) NANO-POWDER

Lithium fluoride powder (LiF) is a white powder with a density of 2.64 gr/cm³ and a melting point of 848°C. This powder has several applications such as flux, glaze, soldering, and aluminum melting process, but one of the most important uses of this powder is its application in dosimetry. The commercial powders currently used for this purpose have average sizes of 5 to 10 micrometers; the objective of this research is to produce LiF powder with nano-metric particle size. In this study, the reaction of LiOH + HF → LiF + H₂O has been selected from among several reactions that were able to produce LiF powder, and some precipitation parameters such as temperature, time, agitation type, and supersaturation degree have been controlled. The morphology, phase analysis, and particle size distribution of the resulting powders were analyzed by SEM, XRD, and LPSA. Finally, lithium fluoride nano-powder was synthesized at a temperature of 25°C, pH about 2-3, reaction time less than 1 s, and agitation by ultrasonic bath.     

Optimising the dewatering behaviour of clay tailings through interfacial chemistry, orthokinetic flocculation and controlled shear

The effect of shear on dewatering behaviour and particle interactions of Na-exchanged smectite and kaolinite clay dispersions has been investigated at pH 7.5, using hydrolysable Ca(II) and Mn(II) ions as coagulants and high molecular weight anionic and non-ionic polyacrylamide (PAM A and PAM N, respectively) and polyethylene oxide (PEO) flocculants. Metal ion addition enhanced the flocculation performance by dramatically reducing the magnitude of the particle zeta potential and, in the case of smectite pulp, suppressing osmotic swelling. Under optimum orthokinetic flocculation conditions of controlled agitation rate and duration, PAM A and PEO-based flocs settled faster than those of PAM N whilst kaolinite pulps produced higher sedimentation rates than smectite pulps. The settling rates are nearly an order of magnitude greater than those observed under standard flocculant-pulp mixing/flocculation methods of inversion and plunging. The difference in the flocculant behaviour is attributed to the more expanded conformation of PAM A and PEO polymer chains in contrast to PAM N, whilst the lower yield stresses, reflecting inter-particle bridging and floc network structure strength that are conducive to faster clarification, were displayed by kaolinite pulps. Following shear, similar consolidation enhancement of ≈ 5-7 wt.% solid for both pulps was achieved at an optimum agitation range of 100-200 rpm. This was accompanied by decreased yield stress in the case of PAM A-based pulps, indicating non-reversible disruption of polymer mediated particle and floc network structure. In contrast, the yield stresses of PAM N and PEO flocculated dispersions indicated similar and stronger particle interactions, respectively, upon consolidation following shear. The findings show clear links between effect of shear, interfacial chemistry and polymer structure on pulp particle interactions and dewaterability.