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81.
82.
几种常用捕收剂与红柱石作用机理的量子化学研究 总被引:1,自引:0,他引:1
运用量子化学中RHF(Hartree-Fock-Roothaan)方法,利用STO-3G基组,研究红柱石晶体中各离子电荷分布及4种捕收剂与红柱石作用的键级与能量变化。经对红柱石与捕收剂成键机理分析表明,十二烷基磺酸钠为化学吸附,十二胺为物理吸附,油酸钠和羟肟酸为物理吸附与化学吸附共存。4种捕收剂按捕收能力从强到弱的排序为:十二烷基磺酸钠〉十二胺〉羟肟酸〉油酸钠。该排序结果与浮选试验结果一致。 相似文献
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S. Yildirim R. G. Fuentes R. Evangelista Z. L. Nikoloy 《Journal of the American Oil Chemists' Society》2002,79(8):809-814
Two germ-separation methods, dry-milling and density separation by flotation, were evaluated for recovering recombinant β-glucuronidase
(rGUS) that accumulated primarily in the germ of transgenic corn. The dry-milling process consisted of (i) seed tempering,
(ii) degerming with a horizontal-drum degermer/dehuller, (iii) particle size fractionation with standard sieves, (iv) germ
and endosperm separation by roller milling and sifting, and (v) removal of hulls by aspiration. Sieves nos. 5, 6, and 7 retained
the majority of germ, and subfractions from these sieves were pooled as a germ-rich fraction. Mass balances showed that the
germ-rich fraction, which constituted 17% of the total dry-milled corn weight, contained 49% of rGUS activity and 64% of the
total recoverable oil. Germ fractionation by flotation was tested as a proof-of-concept method aimed at separating corn fractions
based on their difference in specific gravity (sp gr). The process consisted of impact-grinding of corn kernels followed by
density separation using 1.15 or 1.3 specific gravity sodium nitrate solution. The oil-containing germ fraction floated, whereas
the heavier endosperm fraction sedimented. The flotation method was simpler and resulted in higher enzyme recovery, that is,
the germ-rich fraction was 20% (w/w) of the initial corn weight, and accounted for 80% of rGUS activity and 77% of total oil.
The sodium nitrate solution did not have an adverse effect on the enzyme activity. 相似文献
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以十二烷基磺酸钠(SDS)和N-十二烷基-1,3-丙二胺(DN12)作为混合捕收剂,采用单矿浮选实验分离石英与长石,探究DN12和SDS对长石和石英浮选回收率的影响及其浮选分离的机理。结果表明,在p H为2.0,DN12浓度为4.739×10-4mol/L,SDS浓度为2.38×10-4mol/L时,长石和石英回收率的差值最大,达62.3%。紫外光谱的分析得出,SDS和DN12捕收剂在长石表面仅存在物理吸附,在石英表面不仅存在物理吸附,还存在化学吸附,表明该捕收剂对石英具有更强的捕收能力。 相似文献
88.
通过煤泥窄粒级浮选速率实验,以煤泥浮选一级动力学为基础,对煤泥浮选动力学的关键参数进行研究,包括最大可燃体回收率ε∞的计算、浮选级数n的确定、浮选速率常数K的变化.结果表明:浮选动力学模型中ε∞的经验解比模型解更符合实际;窄粒级煤泥的浮选动力学级数最符合一级动力学;窄粒级煤泥的浮选速率常数K是时间的函数,可用幂函数或经验公式表达,先求出ε∞的经验解,再求解K(t)函数,所得模型非常符合煤泥浮选特征的浮选动力学模型. 相似文献
89.
Effect of frothers in preventing bubble coalescence during flotation of minerals has long been investigated. To evaluate the performance of a frother, an apparatus to measure the bubble size is a basic necessity. McGill Bubble Size Analyzer (MBSA) or bubble viewer that has been developed and completed by McGill University's Mineral Processing Group during the last decade is a unique instrument to serve this purpose. Two parameters which are thought to influence the bubble size measurements by McGill bubble viewer include water quality and frother concentration in the chamber. Results show that there is no difference in Sauter mean (D32) when tap or de-ionized water was used instead of process water. However, the frother concentration, in this research DowFroth 250 (DF250), inside the chamber exhibited a pronounced effect on bubble size. Frother concentration below a certain point can not prevent coalescence inside the chamber and therefore caution must be taken in plant applications. It was also noted that the frother concentration which has been so far practiced in plant measurements (CCC75-CCC95) is high enough to prevent coalescence with the bubble viewer. 相似文献
90.
The size of bubbles created in the flotation process is of great importance to the efficiency of the mineral separation achieved. Meanwhile, it is believed that frother transport between phases is perhaps the most important reason for the interactive nature of the phenomena occurring in the bulk and froth phases in flotation, as frother adsorbed in the surface of rising bubbles is removed from the bulk phase and then released into the froth as a fraction of the bubbles burst. This causes the increased concentration in the froth compared to the bulk concentration, named as frother partitioning. Partitioning reflects the adsorption of frother on bubbles and how to influence bubble size is not known. There currently exists no such a topic aiming to link these two key parameters. To fill this vacancy, the correspondence between bubble size and frother partitioning was examined. Bubble size was measured by sampling-for-imaging (SFI) technique. Using total organic carbon (TOC) analysis to measure the frother partitioning between froth and bulk phases was determined. Measurements have shown, with no exceptions including four different frothers, higher frother concentration is in the bulk than in the froth. The results also show strong partitioning giving an increase in bubble size which implies there is a compelling relationship between these two, represented byCFroth/CBulk andD32. TheCFroth/CBulk andD32 curves show similar exponential decay relationships as a function of added frother in the system, strongly suggesting that the frother concentration gradient between the bulk solution and the bubble interface is the driving force contributing to bubble size reduction. 相似文献