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81.
82.
The realization and applicability of a new dynamic hydrogen reference electrode (DHRE) within an electrochemical microcell for sensor applications is reported. The electrodes are fabricated in thin-film technology and fixed within a flow-through device. An experimental setup for accurate electrochemical potential measurements is described. Smooth platinum, platinized platinum and pHEMA coated electrodes are investigated with regard to their initialization behavior, stability, reproducibility and interference with electrolytes. It is found that platinized platinum DHREs show excellent stability and reproducibility. For uncoated electrodes, the electrochemical potential is established within seconds. The potential is independent of the pH value within the range of pH 4–10. Interference with sulfate and phosphate is observed. Thus, the platinized platinum DHRE is well suited for bioanalytical sensor applications, where the pH value is buffered and the concentrations of the disturbing anions are constant or very low. 相似文献
83.
采用Delphi实现三层客户/服务器数据库应用程序 总被引:17,自引:1,他引:16
讨论了三层客户/服务器结构应用程序的思想,并给出了采用Delphi实现的方法。 相似文献
84.
85.
统计分析认为,影响八面河油田面138区薄层稠油油藏热采效果的主要因数是油层厚度和油层渗透率。根据数值模拟的结果,对面138区薄层稠油油藏蒸汽吞吐工艺参数进行优化后,热采效果得到明显改善,单井注汽量减少,单井产量、周期油汽比和回采水率均得到提高。 相似文献
86.
复合尼龙附耳薄壁圆筒件超声波焊接破裂分析与解决 总被引:2,自引:0,他引:2
介绍了尼龙玻纤复合材料带饶性的薄壁圆筒件超声波焊接时,出现的破裂情况.并对其原因进行了分析.采取有效措施解决了焊接破裂问题,使焊接零件完全合格. 相似文献
87.
Nils C. Broedling Alexander Hartmaier Huajian Gao 《International Journal of Fracture》2006,140(1-4):169-181
The collective dislocation behavior near a crack tip in a ductile layer sandwiched between two brittle solids is analyzed
via two-dimensional dislocation dynamics (DD) simulations that incorporate a cohesive zone (CZ) model. The cohesive crack
tip is treated as part of a much larger finite crack confined in the ductile layer. The underlying boundary value problem
is formulated with a set of boundary integral equations and numerically evaluated with a collocation method. The fracture
energy of the layered composite material is shown to be strongly correlated with the layer thickness and is directly influenced
by the cohesive strength of the ductile layer (Hsia KJ et al. (1994) J Mech Phys Solids 6 877–896). 相似文献
88.
Characterization and microstructure of highly preferred oriented lead barium titanate thin films on MgO (100) by sol-gel process 总被引:1,自引:0,他引:1
Highly preferred oriented lead barium titanate (Pb1−x,Bax)TiO3 thin film, with particular emphasis on (Pb0.5,Ba0.5)TiO3, can be obtained by spin-coating on MgO (100) substrate by using the precursor sol, which was synthesized from acetylacetone chelating with titanium isopropoxide and ethylene glycol as a solvent, in the sol-gel process. Film thickness, pyrolysis temperature and heating rate were studied systemically to investigate their influences on the formation of preferred oriented thin films. The highly preferred (001)/(100) oriented thin film could be obtained by the pyrolysis of wet film at 500 °C and annealing at 600 °C at a slow heating rate of 5 °C/min. It is confirmed that the tetragonal perovskite structure of the titanate ceramic decreases with an increase of Ba content in (Pb1−x,Bax)TiO3. The (001)/(100) oriented films were synthesized from all compositions between x = 0.2 and x = 0.8, at a crystallization temperature of 600 °C. In particular, for the Ba content in the range of x = 0.50.6, highly preferred (001)/(100) planes were observed. 相似文献
89.
J.Y. Cheng C.A. Ross H.I. Smith E.L. Thomas 《Advanced materials (Deerfield Beach, Fla.)》2006,18(19):2505-2521
One of the key challenges in nanotechnology is to control a self‐assembling system to create a specific structure. Self‐organizing block copolymers offer a rich variety of periodic nanoscale patterns, and researchers have succeeded in finding conditions that lead to very long range order of the domains. However, the array of microdomains typically still contains some uncontrolled defects and lacks global registration and orientation. Recent efforts in templated self‐assembly of block copolymers have demonstrated a promising route to control bottom‐up self‐organization processes through top‐down lithographic templates. The orientation and placement of block‐copolymer domains can be directed by topographically or chemically patterned templates. This templated self‐assembly method provides a path towards the rational design of hierarchical device structures with periodic features that cover several length scales. 相似文献
90.