UV法测定聚甲基丙烯酸酯纳米粒中胰岛素的包封率

建立一种简便易行的测定聚甲基丙烯酸酯胰岛素纳米粒中游离胰岛素含量方法.用Nanosep OD100C33超滤膜分离纳米粒和游离药物,在276 nm处测定药物的吸光度,建立胰岛素含量测定方法,并对线性、回收率、精密度等指标进行考察,最后测定各种胰岛素和载体比例混合的纳米粒的包封率.结果发现,该超滤膜能较好地分离纳米粒和游离的药物,在0.11～1.10 u/mL范围内,药物在276 nm的吸光度和浓度存在良好的线性关系(r=0.999 8),线性方程为A=0.868 8C-0.001 6,高、中、低3种浓度的回收率和精密度良好.该方法操作简单、结果可靠,可用于胰岛素纳米粒中药物包封率的测定.     

提高加热炉热效率措施的探讨

对本厂常减压装置提高加热炉热效率采取的措施进行了分析和总结     

Kinetics of DyNi2 film growth by electrochemical implantation

Electrochemical implantation was performed at Ni electrodes to form DyNi₂ films at 0.55 V (vs. Li⁺/Li), 0.62 V, and 0.70 V for 0.5-5.0 h in a molten LiCl-KCl-DyCl₃ (0.50 mol%) system at 700 K. It was found that the DyNi₂ films grew linearly with time with coulomb efficiency of about 100%. The obtained growth rates were higher at more negative potentials, i.e., 0.47 μm min⁻¹ at 0.55 V, 0.32 μm min⁻¹ at 0.62 V, and 0.14 μm min⁻¹ at 0.70 V. On the analogy of the metal oxide growth, the observed rapid and linear growth of DyNi₂ films may be explained by the existence of the outer and inner DyNi₂ layers.     

大庆油田三类油层聚合物驱注入速度研究

注入速度是影响聚合物驱开发效果的重要指标,而由于假设条件的局限性,数值模拟方法无法体现聚合物溶液弹性对注入速度的影响。为了确定大庆油田三类油层合理注入速度,通过不同注入速度条件下的天然岩心驱油试验,对水驱和聚合物驱驱油效率进行了研究,结果表明,聚合物驱驱油效率提高值随驱替速度的变化可由二次多项式来表示。依据此关系式,由势的叠加理论得到的流体在油层中的渗流速度的基础上,建立了该类油层合理注入速度模型,并给出大庆油田三类油层在100 m注采井距下的合理注入速度为0.288 PV年/,该方法对现场开发方案编制有重要指导意义。     

Improvement of emission efficiency in polymer light-emitting devices based on phosphorescent polymers

We report improvement of emission efficiency in polymer light-emitting devices (PLEDs) employing phosphorescent polymers. A hole-blocking layer was inserted between the emissive layer and the cathode to enhance recombination efficiency for the injected holes and electrons. Aluminum(III)bis(2-methyl-8-quinolinato)4-phenylphenolato (BAlq) was used for the hole-blocking layer. The resultant PLEDs exhibited significant improvement of emission efficiency. The respective external quantum efficiencies for red, green and blue PLEDs were 6.6, 11 and 6.9%. These values are very high compared with those based on conventional fluorescent polymers.     

建(构)筑物机械拆除方法综述

介绍了几种常用的建(构)筑物机械拆除方法,对其工作原理、特点、应用条件及局限性加以分析和说明。     

焦化加热炉空气预热器腐蚀结垢与预防

空气预热器运行的好坏直接影响到加热炉的热效率 ,文章结合焦化装置加热炉空气预热器的使用、维修、改进等 ,论述了预热器存在的露点腐蚀问题。同时提出从设计、操作、设备等方面采取有效措施 ,保障预热器的长周期高效运行。     

Numerical Modeling of Silicon Photodiodes for High-Accuracy Applications Part I. Simulation Programs

The suitability of the semiconductor-device modeling program PC-1D for high-accuracy simulation of silicon photodiodes is discussed. A set of user interface programs optimized to support high-accuracy batch-mode operation of PC-1D for modeling the internal quantum efficiency of photodiodes is also described. The optimization includes correction for the dark current under reverse- and forward-bias conditions before calculating the quantum efficiency, and easy access to the highest numerical accuracy available from PC-1D, neither of which is conveniently available with PC-1D’s standard user interface.     

矿用立式旋风水膜除尘器除尘性能的试验研究

本文通过对立式旋风水膜除尘器除尘性能的模型试验,揭示了几个主要参数对其除尘性能的影响,确定了合理的取值范围,对该种除尘器的设计和应用提供了依据。     

酸性盐水及其配套装置的应用与运行

介绍了对进槽盐水由酸碱性改为微酸性的技术改造，减少了副反应的发生，从而提高了电解槽的电流效率。