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In this paper, the author dipped surface vapor oxidized H13 steel specimens into 700℃ molten aluminum liquid for a certain period of time. Analyze the intermetallic phases formed on the H13 samples surface with optical microscope and X-ray diffraction method. The observation of immersion test sample's cross-section shows that Fe3O4 film will protect die substrate from molten aluminum erosion. The identification of the intermetallic phases reveals that they consist of 2parts, which is named as the composite layer and the compact layer. Further investigations are made in order to know the phase constituents of the 2 layers, they are Al8Fe2Si (outer composite layer), (AlCuMg) and Al5Fe2 (compact layer),respectively. The experimental results show that on the same specimen, a convex surface with bigger radius of curvature is more likely to be molten and the melting loss speed is also faster than a flat and smooth surface. The thickness of compact layer on a smooth surface is much bigger than that of the convex surface. Therefore, the author supposes the compact layer is favorable in stabilizing the die surface material from further melting loss, as their formation on the die surface, the melting loss speed will decrease. 相似文献
54.
Suppression of the development of pores during laser-induced surface dispersion of TiC into aluminium, by means of a static magnetic field 总被引:1,自引:0,他引:1
A static magnetic field having the strength of B=0.6 T has been used as an additional process parameter in order to suppress the establishment of pores while dispersing TiC particles in surface layers of aluminium alloys using a laser. The migration of hydrogen towards regions of high temperatures within the melting pool can lead to the creation of gas bubbles, therefore yielding pores after resolidification in the processed layer. This mechanism (known for instance in welding technologies of aluminium) could be suppressed by Lorentz-forces induced by an externally applied magnetic field. It could be shown experimentally that magnetic fields could assist laser surface treatment processes beneficially if higher beam powers were coupled in. This may be interesting if, for instance, thicker dispersed layers should be achieved. 相似文献
55.
A new electron beam control system was developed in a general vacuum electron beam machine by assembling with industrial control computer, programmable logic control (PLC), deflection coil, data acquisition card, power amplifier, etc. In this control system, scanning track and energy distribution of electron beam could be edited off-line, real-time adjusted and controlled on-line. Ti-Mo gradient material (GM) with high temperature resistant was fabricated using the technology of electron beam melting. The melting processes include three steps, such as preheating, melting, and homogenizing. The results show that the GM prepared by melting technology has fine appearance, and it has good integrated interface with the Ti alloy. Mo and Ti elements are gradually distributed in the inter.face of the gradient material. The microstructure close to the Ti alloy base metal is α + β basket-waver grain, and the microstructure close to the GM is a single phase of β solid solution. 相似文献
56.
注射成型塑化过程的可视化实验研究 总被引:1,自引:0,他引:1
利用自行开发的可视化实验装置对注射成型的塑化过程进行了系统的观察,着重讨论了不同的工艺条件对塑化性能的影响,同时借助示踪粒子对塑化过程的重要参数——固相速度进行了测量。实验所取得的数据为注射成型熔融模型的建立和对模型的验证提供了依据,同时也是注射螺杆优化设计的基础数据。 相似文献
57.
Multiple melting phenomena have been studied in blends of poly(vinylidene fluoride) (PVF2) with low molar mass isotactic poly(ethyl methacrylate) (it-PEMA). In all blends, as well as in pure PVF2, a transition (T1) was observed prior to the main melting point (T2). T1 is probably connected with the melting of secondarily-crystallized material. In addition to this, a high temperature melting endotherm (T3) was observed, which could be ascribed completely to recrystallization of PVF2. The highest transition (T4) was caused by melting of the σ form of PVF2. From Hoffman-Weeks plots—T2 vs. crystallization temperature, Tc — it could be concluded that no thermody amic depression of the melting point of PVF2 occurred in the blends. The stabilities of PVF2 crystallites in the various blends were derived from the slopes of Hoffman-Weeks plots and were in good agreement with lamellar thicknesses found from SAXS measurements. 相似文献
58.
PEN/PTT共混聚酯的熔融行为 总被引:1,自引:0,他引:1
利用差示扫描量热仪对不同配比的聚萘二甲酸乙二醇酯/聚对苯二甲酸丙二醇酯(PEN/PTT)共混体系的熔融行为进行了分析,发现在共混体系中两组分形成各自的晶体,PEN和PTT的熔点均随另一组分含量的增加而下降。根据Nishi-Wang方程,按300℃计算,由PEN/PTT共混体系中PEN熔点下降计算所得到的相互作用能密度为-0.214 2 J/cm~3,相互作用参数为-0.006 8,表明PEN/PTY共混体系在熔融态是热力学性质稳定的相容体系。 相似文献
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聚丙烯熔融特性与MDSC条件的相关性 总被引:1,自引:0,他引:1
用调制式差示扫描量热法研究了聚丙烯(PP)升温过程熔融特性与线性升温速率(β)、温度调制振幅(AT)和调制周期(p)的相关性。实验结果表明,在低β时,总热流部分PP熔融呈现双峰;β加快时,呈现单熔融峰。随β加快,不可逆热流部分熔融热(△H)增加;可逆热流部分出现明显的放热峰。随p延长,总热流部分和不可逆热流部分的熔融峰温(Tp)基本不变,起始熔融温度(Ton)降低;但△H前者不变,后者增加;可逆热流部分从吸热变成放热,放热峰温移向高温。总热流和不可逆热流部分的Tp和Ton不受AT的影响,但随AT增大△H前者不变,后者降低。 相似文献