（Ba1-xSrx）（Zn1/3Nb2/3）O3微波介质陶瓷温度系数的异常

研究了（Ba1-xSrx）（Zn1/3Nb2/3）O3微波介质陶瓷温度系数的非线性变化以及异常的原因。根据CM公式，随着系统中Sr（Zn1/3Nb2/3）O3的增多，τc的异常是由于氧八面体的畸变导致的相转变（对称性降低）所造成的（晶体结构由无序立方相向有序赝立方相的连续变化）。相转变的发生相应影响了极化以及极化模式，这是造成τc异常的根本原因。     

二厘米微波衰减标准装置不确定度的验证

采用传递比较法对二厘米微波衰减标准装置不确定度进行了验证。测量标准装置的重复性以组内实验标准偏差sn(A)定量表征，测量标准装置的稳定性用组间实验标准偏差sm定量表征。     

Copolymerization of bromophenylmaleimide with ethyl or butyl methacrylate

N‐p‐Bromophenylmaleimide (BrPMI) does not polymerize in solution by conventional free radical mechanism. However, it readily polymerized in bulk when mixed with a free radical initiator and heated in a microwave oven for 7–8 min. Copolymerization of ethyl methacrylate or butyl methacrylate with BrPMI was conducted in dioxane. The copolymers were characterized by IR and ¹H NMR spectroscopy and gel permeation chromatography. The monomer reactivity ratios were calculated by a non‐linear least‐square analysis. Thermal analysis indicated a great improvement in thermal stability of the copolymers compared with the methacrylate homopolymers. BrPMI was also polymerized in bulk in the DSC pan, which allowed the calculation of the activation energy of its polymerization. Copyright © 2003 Society of Chemical Industry     

Hydrothermal Synthesis and Low-Temperature Sintering of Zinc Gallate Spinel Fine Particles

Nanosized powders of single-phase zinc gallate (ZnGa₂O₄) spinel were hydrothermally synthesized from solutions in the presence of NaOH over the pH range of 1.9 to 7.0 and from solutions above pH 7.0, i.e., the very basic medium (pH of 13.85), by removing the residual ZnO phase by washing with aqueous H₂SO₄ from the precipitate mixtures of zinc gallate spinel particles and ZnO. A very wide compositional range (Zn/2Ga = 0.705–1.157) of zinc gallate spinel solid solutions could be hydrothermally synthesized in the form of nanosized particles from acid and very basic mediums (pH of 2.4–13.85) in the presence of NaOH. These hydrothermally synthesized spinel powders showed good sinterability and almost full densification at 1100°C for 1 h. Dense sintered bodies consisting of single-phase zinc gallate spinel were fabricated at 1100°C using zinc gallate spinel powders having almost stoichiometric composition formed from the solution at pH 9.95 in the presence of aqueous ammonia.     

微波消解-ICP-AES法测定菜油中P、S

采用微波加热,在高温高压下酸消解样品,运用电感耦合等离子体原子发射光谱法(ICP-AES)同时测定菜油中P、S。本法选用紫外区谱线P178.221nm、S180.669nm,避免了基体中存在的Fe、Zn、Al、Cu、Mn、Ca等元素的光谱干扰。实验通过用纯氮吹扫光谱仪光路的方法消减空气中氧对紫外线的吸收,获得了足够的灵敏度。该方法简便、快速,稳定可靠,P、S检出限分别为0.067、0.078μg/ml,RSD为1.35%～5.05%,回收率为89.0%～100.9%。     

非接触式半导体少子寿命测试方法——微波反射法

介绍了一种非接触式用于测量少子寿命的微波反射法，并与通常的光电导衰退法进行了比较。     

Ba（Mg1／3Ta2／3）O3微波陶瓷的损耗研究

本工作用ＸＲＤ，ＥＰＭＡ，ＳＥＭ等测试技术计算和示出了用不同活性粉料制备的Ｂａ（Ｍｇ１／３Ｔａ２／３）Ｏ３微波陶瓷晶格中Ｂ位离子有序度和元素的面分布情况，对它们在Ｘ面下的电行为作了探讨。实验结果表明，ＢＭＴ陶瓷的微波损耗主要与其密度有序度和微观结构的均一度有关。     

Fluorine analysis of nuclear waste glasses

A method for analyzing the fluorine content of glass using a microwave oven to digest the glass is presented. Analysis time and secondary waste generation are reduced using this method, without sacrificing accuracy.     

武钢四烧工程多目标优化方法烧结试验

采用二次回归正交设计进行烧结试验，获得了七个目标的数学模型，并验证了其可靠性，用多目标计算机选优法对四烧车间的工艺参数进行了选优。     

无源微波遥感用于地震预报的实验研究

对无源微波遥感用于地震预报在理论研究的基础上对不同岩性不同结构的岩石试件进行了加载实验，测量了岩石试件的微波辐射随载荷的变化．实验得出：岩石试件的微波辐射能量随岩石应力状态变化而显著变化；而且，不同的波段变化的幅度不同；同一波段不同极化方式的波随应力变化的变化量也不同；微波辐射能量的变化能够被卫星微波遥感探测器探测到．实验还发现，岩石试件临破裂前出现明显的微波辐射异常．