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91.
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93.
PLZT ceramics with the composition of 9/62/38 (La/Zr/Ti) were fabricated from spraydried aqueous solution. Complete crystallization
of the spray-dried powder is achieved after 1 hr calcination at 650‡ C as compared to 800‡ C, 1 hr for conventional mixedoxide
method. Sintering environment plays an important role in the densification of PLZT ceramics. Densities of the atmosphere sintered
samples are much higher than those of normal sintered ones. PLZT ceramics derived from spray-dried powders have properties
comparable to those derived from sol-gel ones. The spray-dried method presents a less expensive and more effective approach
in the synthesis of PLZT ceramics. 相似文献
94.
The metal contact method of rapid freezing is greatly improved by irradiating the specimen with microwaves at 2.45 GHz for a short period of time (50 ms), while pushing the specimen onto the surface of the copper block cooled by liquid N2. The microwave irradiation, together with two technical improvements (a light-mass plunger and a recently developed β-gel shock absorber) for preventing bounce, produces a good freezing zone for squid retina, with high reproducibility for each experimental trial, extending from the contact surface to a depth of about 15 μm, which is comparable to the depth obtained by the metal contact method using liquid He in the absence of microwave irradiation. A good freezing zone was also experimentally demonstrated in specimens of rat liver and heart muscle. Microwave irradiation does not have appreciable effects on the ultrastructure of squid retina. The mechanism underlying the improvement in the rapid freezing under the microwave irradiation is discussed. 相似文献
95.
反应烧结法制备MgAlON的合成机理及烧结行为的研究 总被引:2,自引:1,他引:1
通过对以Al2 O3、MgO和AlN为起始原料 ,在氮气气氛中反应烧结合成MgAlON材料合成机理的研究发现 :在 12 0 0℃以前 ,MgO与Al2 O3反应生成镁铝尖晶石 ,此后 ,随着温度的升高 ,Al2O3不断向所形成的尖晶石中固溶 ;在 130 0℃以前 ,AlN基本上不参与反应 ,而在更高的温度下 ,AlN开始向尖晶石中固溶形成MgAlON ,约在 15 5 0℃时形成单一的MgAlON相。用热膨胀仪检测了试样的线变化率随温度和时间的变化 ,用最小二乘法回归分析了试样线变化率的实验数据 ,并根据烧结理论对MgAlON材料烧结初期的动力学进行了探讨。结果表明 ,MgAlON材料烧结初期的烧结机理以体积扩散为主 相似文献
96.
97.
98.
Calcium addition in straw gasification 总被引:1,自引:0,他引:1
The present work focuses on the influence of calcium addition in gasification. The inorganic-organic element interaction as well as the detailed inorganic-inorganic elements interaction has been studied. The effect of calcium addition as calcium sugar/molasses solutions to straw significantly affected the ash chemistry and the ash sintering tendency but much less the char reactivity. Thermo balance test are made and high-temperature X-ray diffraction measurements are performed, the experimental results indicate that with calcium addition major inorganic-inorganic reactions take place very late in the char conversion process. Comprehensive global equilibrium calculations predicted important characteristics of the inorganic ash residue. Equilibrium calculations predict the formation of liquid salt if sufficient amounts of Ca are added and according to experiments as well as calculations calcium binds silicon primarily as calcium silicates and less as potassium calcium silicates. 相似文献
99.
重点讨论了现代无线通信中关键元器件之一滤波器的发展进程,中、高频及微波滤波器的主要类型及性能特点。低损耗、高介电常数陶瓷在RF和IF滤波器中的应用,能够实现无线设备的微型化。对制备滤波器的介质陶瓷材料的要求是:在所使用的波段内,相对介电常数r要大,可缩小介质元件的尺寸;品质因数Q要高,可获得良好的滤波特性及通讯质量;谐振频率的温度系数f接近于零或可调节,以达到整机电子回路的要求。 相似文献
100.
The growth of carbide particles in TiC-XC-2 vol.% Ni and TiC-XC-30 vol.% Ni alloys, where X=Zr, Cr, W, Ta and Mo, was fitted
to an equation of the form d3-do
3=Kt. The grain growth behavior during liquid phase sintering at 1673K decreased markedly with the addition of Mo2C or WC, changed little for TaC, and increased with the addition of ZrC or Cr3C2. The grain contiguity decreased with increasing Ni content in the TiC−Mo2C−Ni alloy and was greater in the alloys with smaller growth rate constant. Consequently, the effect of carbide addition on
the grain growth of 2 vol.% Ni alloys was found to be similar to that of 30 vol.% Ni alloys. The grain growth mechanism could
be explained by the effect of contiguous carbide grain boundaries in restricting the overall grain growth, as well as the
area of the solid/liquid interfaces in the alloy by the usual solution/reprecipitation model. 相似文献