一种基于网络应用特征串识别的局域网管理方案

鉴于网络应用的高速发展,局域网呈现出复杂化的趋势,为更好的完成局域网管理的工作,提出一种基于网络应用行为识别与统计分析的局域网管理方案。该方案以网络特征串识别网络应用行为为基础,以主动识别网络应用行为的方式,通过对网络应用的归类和统计分析实现对局域网网络的积极管理。该方案可以在局域网内有效实现对网络应用的主动监控,网络管理员可以自行设置网络管理方式,达到主动管理灵活监控的目标,优化局域网网络环境。     

动态法快速测定催化剂比表面

本文采用动态法原理测定催化剂的比表面，利用热导检测器测定催化剂微孔在液氮下的吸附及常温下的脱附面积。用外标法进行定量。该方法分析速度快．在l小时内同时测定3个样品的比表面。其准确度及精密度满足要求。     

SO4^2—／TiO2固体超强酸的比表面研究

用BET法研究了SO4^2-／TiO2在不同H2SO4溶液浓度、不同浸泡时间及不同焙烧温度时比表面的变化情况，并用指示剂测定了酸强度。     

石莼基微/中孔复合结构活性炭的制备及性能

以海洋海藻废弃物石莼为原料,通过热解预炭化,KOH活化制备活性炭。以碘吸附值和亚甲基蓝吸附值为吸附性能评价指标,探究了活化工艺对活性炭吸附性能的影响。结果表明,当KOH与石莼半焦质量比(碱炭比)为3.0∶1.0、活化时间为45 min、活化温度为800℃时,活性炭吸附性能最优,其碘吸附值和亚甲基蓝吸附值最大,分别为1824.19 mg/g、914.98 mg/g。FTIR测试表明,活性炭含有大量羟基等官能团。SEM测试表明,活性炭表面粗糙、存在大量孔结构。活性炭的BET比表面积为2616.3 m2/g,Langmuir比表面积高达4883.5 m2/g,平均孔径为2.73 nm。石莼基活性炭的孔结构为微/中孔复合结构,有作为储能、环保材料的潜质。     

硅灰石合成高比表面积二氧化硅的工艺研究

一系列硅灰石酸处理实验表明,产物物理性质与反应速度、反应时间、中和最终ｐＨ值等工艺条件有关。同时发现,如果工艺条件恰当,可以制得４００～６００ｍ＾２／ｇ的高比表面积二氧化硅。     

Interfacial area and volumetric mass transfer coefficient in a bubble reactor at elevated pressures

The present study deals with the pressure effects on mass transfer parameters within a bubble reactor operating at pressures up to . The gas-liquid systems are N₂/CO₂-aqueous solution of Na₂CO₃-NaHCO₃ and N₂/CO₂-aqueous solution of NaOH. A sintered powder plate is used as a gas distributor. Three parameters characterizing the mass transfer are identified and investigated with respect to pressure: the gas-liquid interfacial area a, the volumetric liquid side mass transfer coefficient k_La and the volumetric gas side mass transfer coefficient k_Ga. The gas-liquid absorption with chemical reaction is used and the mass transfer parameters are determined by using the model reaction between CO₂ and the aqueous solutions of Na₂CO₃-NaHCO₃ and NaOH. For a given gas mass flow rate, the interfacial area as well as the volumetric liquid mass transfer coefficient decrease with increasing operating pressure. However, for a given pressure, a and k_La increase with increasing gas mass flow rates. The mass transfer coefficient k_L is independent of pressure. Furthermore, the pressure increase results in a decrease of k_G and k_Ga for a given gas mass flow rate. The values of the interfacial area, which are obtained from both chemical systems are found to be different. These discrepancies are attributed to the choice of the liquid system in the absorption reaction model.     

Preparation of porous carbons from thermoplastic precursors and their performance for electric double layer capacitors

Porous carbons with high surface area were successfully prepared from thermoplastic precursors, such as poly(vinyl alcohol) (PVA), hydroxyl propyl cellulose and poly(ethylene terephthalate), by the carbonization of a mixture with MgO at 900 °C in an inert atmosphere. After carbonization the MgO was dissolved out using a diluted sulfuric acid and the carbons formed were isolated. The mixing of the PVA carbon precursor with the MgO precursors (reagent grade MgO, magnesium acetate or citrate) was done either in powder form or in an aqueous solution. The BET surface area of the carbons obtained via solution mixing could reach a very high value, such as 2000 m²/g, without any activation process. The pore structure of the resultant carbons was found to depend strongly on the mixing method; the carbons prepared via solution mixing were rich in mesopores, but those produced via powder mixing were rich in micropores. The size of mesopores was found to be almost the same as that of the MgO particles, suggesting a way of controlling the mesopore size in the resultant carbons. Measurement of capacitance was carried out in 1 mol/L H₂SO₄ electrolyte. The porous carbon with a BET surface area of 1900 m²/g prepared at 900 °C through solution mixing of Mg acetate with PVA showed a fairly high EDLC capacitance, about 250 F/g with a current density of 20 mA/g and 210 F/g with 1000 mA/g. The rate performance was closely related to the mesoporous surface area.     

Simultaneous measurement of flow pattern and mass transfer coefficient in bubble columns

Mass transfer studies were carried out in a bubble column using the chemical method. Catalytic oxidation of sodium sulfite was chosen for the studies and the corresponding specific rates of oxidation were obtained using a stirred cell. Laser Doppler anemometer (LDA) was used to measure the instantaneous velocities in the same stirred cell as well as in bubble columns (100 and i.d.). An efficient algorithm based on the multiresolution analysis of the velocity-time data using wavelets was used for the isolation of data belonging to the gas and liquid phases. Eddy isolation model was used for the characterization of the eddy motion including the estimation of the energy dissipation rate. Using the knowledge of eddy motion, a methodology was developed for the prediction of true mass transfer coefficient (k_L) in a stirred cell as well as in bubble columns. The predicted values of k_L have been compared with the experimental values obtained by the chemical method.     

On the importance of some surface and interface characteristics in the formation of the properties of adhesive joints

The importance of some relative surface characteristics which determines the strength of adhesive joints: specific surface of substrate , relative contact area β and specific contact area β in the adhesion interaction process were emphasised. Existing and potential methods of experimental evaluation of these characteristics were shortly analysed. The durability of the adhesive joints in water media significantly increases with growth of specific surface ^* of chemically treated substrate evaluated from the SEM micrographs. Specific surface calculated from the experimental data of hexane adsorption measurements for iron particles (particulate model of steel substrate) is more then ten times greater than respective ^* values. The relative contact area β of the Al₂O₃ particles (in wide range of ) with PE melt was in a roundabout way evaluated by experimental determination of the affect of on kinetic of peel strength formation of adhesive joints: Al₂O₃ filled PE-steel. The speculation was based on the ability of Al₂O₃ to adsorb low-molecular products of contact oxidation of PE which takes place in the process of formation of adhesive joints and determines their strength. The ability of sorption in its turn is proportional to efficient value of β. The availability of the Al₂O₃ surface was evaluated.     

基于高密度电阻率法的露天铁矿采空区探测的研究

露天铁矿开采区地下浅部大量采空区的存在,给矿山的人员及生产安全带来极大的威胁。为保证生产活动的顺利进行,必须对采空区进行精确探测。由于高密度电阻率法较常规电法具有信息丰富、精度高的特点,运用该法对露天铁矿采空区进行探测,结合数据反演断面图,在地下50m的范围内,共划定采空区四处,并精确划定采空区顶底板深度、水平范围和展布方向,为矿山的治理工作提供了可靠依据。并且在分析采集数据的基础上,总结出视电阻率识别模型及其主要特点,为地下采空区的划定提供了理论基础。