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31.
32.
A finite element formulation and the solution of a set of nonlinear coupled heat and mass transfer equations for a two-phase system with a moving evaporation interface is presented. The interface condition takes into account the moisture transfer balance at the moving boundary. The finite element results were compared with existing results for a single phase system for model validation. In the two-phase system, the movement of evaporation front has an appreciable effect on the temperature and moisture distribution inside the porous medium during drying. The effect of the nondimensional heat of vapourization parameter γ on the evaporation front, temperature and moisture distribution in porous medium was studied. The higher the value of γ, the slower is the movement of the evaporation front. The temperature decreased and the moisture content increased as the nondimensional vapourization parameter γ increased. This model has potential applications in studying the heat and mass transfer characteristics in food and biomaterials. 相似文献
33.
本文介绍核孔膜生产线,重点描述了膜微孔制备工艺的实验研究。对于PC和PES膜,已得到32种工况下的扩孔公式,其形式为D=A+Bt,其中D——孔径,t——扩孔时间,A,B为特定工艺参数下的常数值.通过实验。得到了膜孔密度N与300~#核反应堆功率P、热柱辐照位置L的经验公式,即N=6.97×10~5×10~3×101~(1.18L).在本生产线上可生产最大幅面为3 140mm×240mm,孔径为0.04~10 μm的多系列多规格的核孔膜产品。 相似文献
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35.
氧化锌压敏陶瓷烧结致密化过程的研究 总被引:6,自引:0,他引:6
本文研究了氧化锌压敏陶瓷的致密化过程,结果发现只有当烧结温度升高到一定值时,试样中的ZnO粉粒产生聚集,致密化过程才开始.致密化是瓷体获得稳定电性能的基础.低熔点添加剂B2O3可以降低致密化的起始温度,而致密化过程中的等温烧结对ZnO压敏陶瓷的最大密度几乎没有影响. 相似文献
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37.
The production of porous polymeric particles is attractive for a large number of applications and can be achieved by various techniques. Although numerous production schemes exist for glassy polymers, difficulties arise for soft, rubbery materials that need a chemical crosslinking step, such as elastomers. This is particularly true for poly(dimethylsiloxane) (PDMS), which shows the lowest glass‐transition temperature among the polymers. Recent studies suggest in situ hydrogen bubble formation or vacuum drying of water droplets dispersed in the polymer matrix in order to generate porous PDMS structures. In this work we report early results based on the chemical crosslinking of water in PDMS emulsion droplets in a mechanically stirred thermostated water vessel. This approach is shown to lead to high porosity PDMS beads (ca. 10?3 m particle diameter) with an open structure whose properties (diameter and porosity) are strongly influenced by the starting composition (solvent, surfactant, and polymer types and ratios), as well as the operating parameters (agitation and temperature). The possible uses of these derived beads are discussed. © 2002 Wiley Periodicals, Inc. J Appl Polym Sci 83: 967–971, 2002 相似文献
38.
P. Bocchetta C. Sunseri A. Bottino G. Capannelli G. Chiavarotti S. Piazza F. Di Quarto 《Journal of Applied Electrochemistry》2002,32(9):977-985
Alumina membranes were fabricated by anodizing aluminium metal in 0.15 M oxalic acid. The growth kinetics of the porous layer were investigated in the temperature range –1 to 16 °C using linear potential scans up to 70 V. The faradaic efficiencies of metal oxidation and of porous layer formation, determined by applying Faraday's law, were found to be independent of both temperature and electrical charge. SEM analysis of the metal-side and solution-side surfaces revealed different morphologies. After dissolution of the barrier layer in phosphoric acid, the metal-side surface showed circular pores whose size of about 90 nm was found to be uniform and independent of temperature. The pore population was also practically independent of temperature and a value of about 4 × 1013 pores m–2 was determined. On the solution-side surface the presence of a deposit partially occluding the mouths of pores was observed. This coating could be removed by chemical etching in NaOH or thermal treatment at 870 °C, where decomposition of oxalate occurs. This supports the hypothesis that the deposit consists of an aluminium salt containing oxalate anions precipitated from the solution. The results show that it is possible to control the morphological characteristics of the anodic alumina membranes by careful choice of experimental conditions. 相似文献
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40.
A. Stein 《Advanced materials (Deerfield Beach, Fla.)》2003,15(10):763-775
This report highlights developments in the fields of microporous and mesoporous materials that were published mostly during the year 2002. Selected examples are provided to illustrate new zeolite structures, porous coordination materials, mesoporous solids with new compositions, controlled morphologies, and increased hydrothermal and thermal stabilities, as well as porous solids with tunable pore openings or other structural features that can be dynamically modified. A number of applications are discussed, including stabilization of reactive guests, separations, electronic materials, and sensors. 相似文献