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63.
Miroslav Pastorek 《Materials and Manufacturing Processes》2018,33(15):1674-1680
Thermal annealing as an additional polymer processing step or post-treatment processing step enables the structural changes of amorphous parts into crystalline parts. This paper investigates the feasibility of thermal annealing at 100°C up to 90?min used as an additional processing step to modify the crystalline structure and the thermo-mechanical stability of poly(lactic acid) (PLA). Moreover, the crystallization ability of PLA has been amended by the addition of 3?wt% of wood flour and kaolin. The values of the degree of crystallinity and lamellar thickness determined by wide-angle-X-ray scattering showed that the thermal annealing of PLA samples modified with nucleating agents was an efficient processing step to increase the final crystallinity of PLA. Moreover, altered crystalline structure helped to improve the thermomechanical stability of PLA. 相似文献
64.
Nucleation Crystallography of Ni Grains on CrFeNb Inoculants Investigated by Edge‐to‐Edge Matching Model in an IN718 Superalloy 下载免费PDF全文
Wenchao Yang Pengfei Qu Lin Liu Ziqi Jie Taiwen Huang Feng Wang Jun Zhang 《Advanced Engineering Materials》2018,20(2)
65.
分子动力学模拟测得熔融(RbCl)108离子簇在300K至600K温度时凝固的成核速率大于10^35m^-3s^-1,用均相成核的经典理论加以分析,估算得氯化铷离子簇的固液界面自由能σalT^1.4,用Grunasy提出的扩散界面理论加以分析,估算得扩展界面厚度约为0.195nm,σalT^0.97,2个理论在实验温度范围内没有明显判别,且均能较好地分子动力学模型的结果,但预测的较高温度下的成核速率有比较显著区别,因此进一步地研究将有助于鉴别它们。 相似文献
66.
This work is the first part of an overall project the aim of which is the development of general mix design rules for concrete containing different kinds of mineral admixtures. The separation of the different physical effects responsible for the modification of cement hydration, when chemically inert quartz powders are used in mortars, is presented. The phenomenological approach, based on semi-adiabatic calorimetry, is only associated with first-order phenomena, and the study excludes the complex physicochemical details involved in the chemistry of cement. The results, obtained for a wide range of fineness (between 180 and 2000 m2/kg) and replacement rates (up to 75%), show that short-term degrees of hydration in mortars containing a chemically inert mineral admixture (quartz) are always higher than for a reference mortar. This study confirms that cement hydration is enhanced by inert mineral admixtures. The two main physical effects responsible for the modification of the hydration of cement are identified as the dilution effect and heterogeneous nucleation. The dilution effect of the cement is highlighted with a coarse mineral admixture. The heterogeneous nucleation effect, although it increases with fineness of mineral admixtures, presents an optimum depending on the replacement rate. In the following part of this work, these results will be used for the development of an empirical model allowing us to quantify both physical effects. 相似文献
67.
G. J. Gruber 《Journal of Nondestructive Evaluation》1980,1(4):263-276
Shape and size are the most important defect characteristics that need to be determined for the reliable prediction of the remaining service lifetime of a defective structure or part. The analytical and supporting experimental results presented in this paper concern a general, pattern recognition-based, ultrasonic defect identification and sizing method. The satellite-pulse technique (SPT) is based on the interpretation, in terms of defect types (shapes) and dimensions, of the separation in time of arrival between the readily detected specularly reflected pulse and its generally ignored tip-diffracted or tangentially scattered satellite contained in the received waveform. Calibration procedures were also developed that enable the ultrasonic examiner to read the time scale of the oscilloscope for equivalent crack depth or void diameter as appropriate. 相似文献
68.
A high-Ti 6061 alloy was rolled with strains up to 0.8-2.0 and at 350-550 ℃. Microstructures that developed during deformation and subsequent solution heat treatment (SHT) were observed by using optical and transmission electron microscopy. Microstructure evolution during SHT depends mainly on the initial rolling temperature, and it was found that the higher this temperature is, the coarser the grains are. After rolling at 400 ℃, well-defined cells and subgrains were formed, which induced further sites for recrystallization nucleation during subsequent SHT. The recrystallization mechanism was found to be subgrain rotation, with a final grain size smaller than 200 μm. Increasing the rolling temperature to 500 ℃ results in a low density of dislocations distributed uniformly in the deformed matrix and fewer nucleation sites during subsequent SHT. The recrystallization mechanism is grain boundary bulging, while the final grain size approaches several millimeters. Finally, a hot forming process of high-Ti 6061 alloy for inhibiting grain coarsening was proposed, and verified by experiments. 相似文献
69.
M.E. Biancolini C. Brutti G. Paparo A. Zanini 《International Journal of Fatigue》2006,28(12):1820-1825
In this paper, a new acoustic emission (AE) diagnostic technique, for the study of fatigue cracks nucleation and propagation on steel, was investigated. Using the fractal analysis, and the box-counting method (BCM) in particular, it is possible to characterize the spatial distribution of the prime AE sources through the fractal dimension (D) that evolve with the number of fatigue cycles (N) of the specimen. D–N curves were found useful to identify the condition of incipient collapse due to the nucleation and propagation of fatigue cracks on steel. It is possible to use the fractal dimension as a damage parameter. In all tested specimens, the crisis occurs within the same range of values of fractal dimension. The results suggest that it is possible to anticipate the detection of crack beginning relating to the other theoretical or experimental techniques. 相似文献
70.
Fretting is associated with small amplitude oscillatory movements between two surfaces in contact. One possible consequence of fretting is the formation and subsequent growth of cracks at the edges of the contact. This paper presents an experimental investigation of the cracking behaviour under fretting loading of two different aluminium alloys: 2024-T351 and 7075-T651. Systematic and controlled experiments with a cylinder-flat contact under partial slip fretting conditions were carried out. A model which combines both crack nucleation and propagation processes is used to predict the crack extension throughout the life of the component. The direction of crack propagation experimentally observed was taken into account by the model. Furthermore, an analytical prediction of crack nucleation based on the process volume approach is made. The predictions of both crack extension and nucleation are compared with the experimental results, and show good agreement. 相似文献