7A55合金均匀化处理

采用光学显微镜、扫描电镜、能谱分析、透射电镜和X射线衍射分析等研究了7A55合金铸态与均匀化显微组织演化与成分分布,确定了该合金的均匀化处理温度与过烧温度,研究了铸锭均匀化动力学过程,利用菲克定理导出了均匀化动力学方程,利用动力学方程对均匀化过程中合金元素的扩散、Al3Zr的析出、难熔相的聚集和球化现象进行了解释。根据实验及计算结果,得出合理均匀化处理工艺为470℃均匀化24 h。     

7A55铝基表面微区等离子烧结复合 陶瓷涂层的工艺与机理

目的 通过优化电解液配方和电参数输出模式,得到改性微弧氧化新工艺,制备出综合性能优良的SiO2-Al2O3复合陶瓷涂层。方法 采用碱性硅酸盐体系电解液为诱发起弧剂,加入80~150 mL/L的碱性硅溶胶溶液和60~80 g/L蔗糖等成分为辅助添加剂,同时在电参数中加入负电参数,在7A55铝合金基体表面完成了SiO2-Al2O3复合陶瓷涂层的制备。采用SEM和EDS等测试方法分析了复合陶瓷的微观形貌和组成元素,并与制备单一Al2O3陶瓷涂层的微弧氧化工艺进行对比,分析新工艺的成膜机理。结果 改性新工艺能够在7A55铝合金基体表面制备出SiO2-Al2O3复合陶瓷涂层,厚度达到100 μm以上,其制备效率相比微弧氧化制备单一Al2O3陶瓷涂层提高了2~3倍。复合陶瓷涂层由表及里,Al2O3含量增加,SiO2含量减少,表面呈致密的球形颗粒状,没有单一Al2O3陶瓷涂层的微裂纹和大量烧蚀孔洞。新工艺除了微区放电形成微区等离子弧烧结,得到Al2O3陶瓷涂层外,还有SiO2的吸附沉积,为吸附与烧结综合作用过程。结论 加入含纳米SiO2的碱性硅溶胶等成分改性电解液,有利于改善陶瓷涂层结构,提高致密性。     

Q235上电弧喷涂Zn55Al涂层在3.5wt%溶液中的腐蚀行为研究

本文使用电弧喷涂通过包套挤压+拉拔的方法制备的Zn55Al伪合金丝材成功的在Q235钢上喷涂出了Zn55Al涂层。通过扫描电镜和微区XRD研究了Zn55Al 伪合金丝材的显微结构。通过浸泡腐蚀实验和电化学方法研究了Zn55Al涂层、Zn15Al涂层和 Al涂层的腐蚀行为,并对比了三种涂层之间的差异。结果表明Zn55Al伪合金丝材由纯锌和纯铝组成,在整个成型过程中没有产生合金化。Zn55Al涂层由层片状的富锌相和富铝相组成。经过20天的浸泡实验,Zn55Al涂层形成了一层致密的钝化膜,比其他两种涂层有更好的耐腐蚀性。Zn55Al涂层的自腐蚀电位大约是-1.25v,高于Zn15Al涂层低于纯Al涂层和Q235基体.电偶腐蚀实验表明,Zn55Al涂层比Zn15Al涂层具有更好的点虎穴保护作用。这些结果说明Zn55Al涂层具有更好的耐腐蚀性和可以给Q235基体提供更强的电化学保护.本文也讨论了Zn55Al涂层的的腐蚀机理。     

55NiCrMOV7钢回火组织特征与回火温度和时间的关系

采用X射线衍射(XRD)技术,研究了55NiCrMoV7热作工具钢回火过程组织的演化规律.结果表明,随回火温度增加,残余奥氏体逐渐分解,回火碳化物为M3C和少量VC;X射线衍射马氏体(211)峰半高宽随回火温度线性下降,随回火时间呈幂指数下降关系.并建立了回火组织特征马氏体(211)峰物理半高宽与回火温度、回火时间服从B=B0·e-(Dt)m定量关系的单一模型和分段模型.     

基于修正JC模型和BP-ANN算法预测HNi55-7-4-2合金高温流变行为的对比

采用Gleeble-3500型热模拟试验机,分别在变形温度为873,923,973,1023,1073 K,应变速率为0.01,0.1,1,10 s-1条件下对HNi55-7-4-2合金进行等温热压缩试验,研究了该合金的高温流变行为;基于试验数据,分别采用修正Johnson-Cook(M-JC)模型和反向传播人工神经网...     

Ti—55M高温Ti合金焊缝塑性的改善

考察了Ti-55M高温Ti合金焊接接头力学性能,结果显示焊缝在明显的室脆性,探讨了Ti-55M焊缝室温塑性的各种影响因素,尝试使用调整焊缝化学成分的方法改善Ti-55M焊缝的塑性,选择ELI级Ti-5Al-2.5Sn焊丝、配合脉冲氩弧焊工艺和适当的焊后热处理制度、获得的焊缝塑性接近母材的塑性,接头的室温和高温强度以及高温持久等重要性能能够满足母材技术指标要求。     

基于CANopen协议的扭矩传感器数据采集测试系统

介绍了一种高精度的力矩数据采集测试系统,重点阐述了CANopen协议的通信对象以及基于该协议的扭矩传感器配套使用的放大器MP55,系统中上位机VB控制程序通过访问MP55对象字典(重点是SDO和PDO)从而对传感器采集和数据传输各项参数进行设置.系统实现了对传感器测试数据高精度和较高速等时间间隔的采集和传输.     

Production and quality analysis of Pr55gag particles produced in baculovirus-infected insect cells

In this work Sf-9 cells previously adapted to SF900II and EXCELL 401 serum-free media (SFM) were grown and infected at different agitation rates in order to study the effects of power input upon cell growth, infection and production of Pr55gag particles in both SFM. Maximum cell concentration increased from 3×10⁶ to 6×10⁶ cells cm⁻³ and 6·5×10⁶ cells cm⁻³ when the agitation increased from 80 to 250 rpm or sparged aeration (0·01 vvm at 170 rpm) is used, clearly indicating that cell growth is limited by gas transfer. The specific productivity increased 3·5-fold when the agitation rate was increased from 80 to 170 rpm, indicating that in SFM cell infection is also limited by gas transfer. The highest product concentration was obtained in SF900II at 120 h post-infection (hpi). The product quality analysis showed that SF900II is the best medium for production of Pr55gag particles and that a careful optimisation of the harvest time is required. The maximum product titre was obtained at 120 hpi, 48 h after the achievement of the highest quality. © 1998 SCI     

DIMPLE FORMATION ON FRACTURE SURFACE OF STEEL 55SiMnMo

The fracture surface of the normalized steel 55SiMnMo was observed,under tensile device at-tached on the SEM,to be of ductile dimple feature on the bainite which is composed of lathferrite and austenite platelet.The dimple is essentially nucleated in the ferrite.Because theaustenitic plastic deformation is remarkable during fracturing,the tear ridge of dimple is verysharp.     

Acceptance of technology related to healthcare among older Korean adults in rural areas: A mixed-method study

Many older adults find it difficult to accept new forms of information and communication technology (ICT), despite its advantages such as convenience and efficiency. It is necessary to identify the reasons for low ICT use among older people—even among those with positive attitudes toward ICT—to help older adults cope with social changes and bridge the digital divide. This study explored technology acceptance and related factors among older Korean adults living in rural areas. Based on an existing model (the senior technology acceptance model), a new conceptual framework for technology acceptance was proposed, and the framework was tested using pathway analysis. Semi-structured interviews were conducted in three focus groups (n = 15), and a survey questionnaire was administered to older Korean adults living in a rural area (n = 233) from 17 January 2021 to 18 February 2021. Qualitative data were analyzed using directed content analysis, and quantitative data were analyzed using pathway analysis. Four categories, 11 subcategories, and 18 codes were identified, and a new conceptual framework was proposed based on the qualitative findings. The results of the model revealed significant positive direct paths from external controls (β = 0.45, p < .001), attitudinal beliefs (β = 0.33, p < .001), and cognitive health (β = 0.10, p = .040) to internal abilities. It is necessary to develop and apply a targeted and tailored ICT education program to improve self-efficacy and reduce anxiety regarding technology use among older Korean adults living in rural areas.