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71.
研究了加料顺序,陈化方式,陈化条件,对Fe(naph)_2—Al(i—Bu)_3——CH_2=CHCl体系催化丁二烯聚合活性的影响。结果发现按Bd+Fe+Cl+Al的加料顺序配制的催化剂的活性高于其它加料顺序;陈化方法不能提高催化剂的活性。 相似文献
72.
考察了所配制的70#和90#两种彩色道路沥青在老化过程中正戊烷沥青质的变化;并依据老化过程中正戊烷沥青质的变化,进行了彩色沥青老化动力学研究,得出了有关动力学参数,得到了两种彩色沥青老化动力学方程,其理论计算值与实际试验数据基本吻合,表明彩色道路沥青老化属于一级动力学反应。结果表明,70#彩色沥青反应活化能(Ea=4.483×104J·mol-1)比90#彩色沥青反应活化能(Ea=4.322×104J·mol-1)高,反应速度常数较小,具有较低的老化速率和较好的抗老化性能。 相似文献
73.
制备了 5种牌号的重交通道路沥青 ,并通过薄膜烘箱 (16 3℃ ,5h)实验前后正戊烷沥青质含量的变化及胶体不稳定指数和老化指数比较了它们的抗老化性能 ,同时建立了辽曙一区原油的切割温度及调和剂用量与使用性能关系的回归方程。实验结果表明 :所建立的切割温度与针入度、软化点关系及调和剂用量与针入度、软化点关系的回归方程对沥青工业生产和使用具有一定的指导意义。沥青老化后针入度明显降低、软化点升高、延度变差。沥青质含量变化最快的道路沥青抗老化性能最差 ;胶体不稳定指数越小 ,胶体结构越稳定 ,抗老化性能越好 ;老化指数越大的沥青 ,抗老化性能越差 相似文献
75.
Age-dependent MRI-detected lesions at early stages of transient global ischemia in rat brain 总被引:2,自引:0,他引:2
Canese R Lorenzini P Fortuna S Volpe MT Giannini M Podo F Michalek H 《Magma (New York, N.Y.)》2004,17(3-6):109-116
Although ischemic stroke has higher incidence and severity in aged than in young humans, the age factor is generally neglected in ischemia animal models. This study was aimed at comparing age-dependent effects at early stages of transient global cerebral ischemia (TGCI) in rats. TGCI was induced in two groups of rats (3–6 and 20–24 months old, respectively) by exposure to 15% oxygen and 15 min occlusion of the two common carotid arteries. Brains were analysed in vivo by MRI–apparent diffusion coefficient (ADC) and T2 maps–at 1–3 h post-TGCI and in vitro by histochemical examination of triphenyltetrazolium chloride (TTC)-stained slices. At 1–3 h post-TGCI, a higher incidence of lesions was found in aged than in young rats especially in the hippocampus and cortex (occipital plus parietal) but not in the thalamus. The lesioned regions showed lower ADC values in aged than in younger rats. The most substantial ADC decreases were associated with enhanced spin-spin relaxation and lower TTC staining. The different responses of the two age groups support the use of aged animals for investigations on different ischemia models. Our model of brain ischemia appears appropriate for further studies including drug effects. 相似文献
76.
Beatriz?I.?Vázquez Luis?Carreira Carlos?Franco Cristina?Fente Alberto?Cepeda Jorge?Barros-VelázquezEmail author 《European Food Research and Technology》2004,218(2):118-122
Vacuum skin packaging (VSP) is a new and promising technology that includes the instantaneous heating of the upper packaging film immediately before its descent over the meat surface. In the present paper we evaluated this technology for the packaging of a wide variety of beef retail cuts and compared this with traditional vacuum packaging (TVP) performed in parallel. Shelf-life and quality evolution was estimated by analysing three spoilage bacterial groups, an ubiquitous psychrotrophic food pathogen, and three biochemical and physico-chemical attributes throughout 40 days of storage at 4 °C. Statistically-significant lower microbial counts were obtained for all microbial parameters and meat types. The VSP lot exhibited lower pH. This, however, involved a lower water holding capacity and a higher degree of firmness, the latter indicating a limited tenderisation process in the VSP batch. Extended aging times in the carcasses were studied to improving the tenderness of VSP samples. The extension of the aging process prior to VSP may be useful for improving the tenderness of certain meat types and to improve the sensory quality of meat cuts processed under this system. 相似文献
77.
The objective of this study was to investigate the influence of Eudragit® NE 30 D blended with Eudragit® L 30 D-55 on the release of phenylpropanolamine hydrochloride (PPA·HCl) from coated pellets. The miscibility of Eudragit NE 30 D/L 30 D-55 blends at different ratios was studied by using differential scanning calorimetry. The release of PPA·HCl from pellets coated with Eudragit NE 30 D alone and a Eudragit NE 30 D/L 30 D-55 blend, when stored at 40°C and 60°C, was determined by UV spectroscopy. Eudragit NE 30 D and Eudragit L 30 D-55 were miscible in ratios greater than 4:1. The curing time that was required to reach an equilibrium state decreased with the addition of Eudragit L 30 D-55. The presence of Eudragit L 30 D-55 also produced a film coating that was less tacky, and a dispersion of Eudragit NE 30 D containing Eudragit L 30 D-55 (5:1) was shown to prevent agglomeration of the pellets during coating and storage. 相似文献
78.
Petroleum-based transformer oil performs the dual roles of insulator and electrolyte depending on charges in the oil. The availability of charges for conduction influences the level of voltage breakdown in the mineral oil and depends on the intensity of physicochemical processes such as redox action, hydrolysis, photodegradation, sludge/particle development, and gas formation arising from thermal, mechanical, chemical, and electrical stresses in the oil. Previous investigators have focused mostly on single oil aging indicators to build models for estimation of the aging rates of transformer oils, within a time frame that is too short relative to the operational service life of transformers. In this research, the interdependence of oil voltage breakdown and changes in oil physicochemical characteristics was investigated experimentally using T24 and T14 oils. Tests were performed with a DTS-100D oil tester for voltage breakdown and a HKV 4000 series high kinematic viscosity bath. The calculated activation energies are 26.2?KJm?3 for T24 and 25.4?KJm?3 for T24 transformer oils, respectively. Neglecting catastrophic failure from environmental hazards, the estimated service lives of T14 and T24 transformers that are herein analyzed are 40 and 43 years, respectively. Their degradation constants were experimentally determined to be 7.38×10?12 and 6.98×10?12?L?1?S?1, respectively. 相似文献
79.
Li Ying Shi Jian Qiang Wang Ling Gao Li Huang Jianhua Zhu Ying Wang Xiaoxing Fan Tao Yu Mei Zhu Zhaosheng Li Zhigang Zou 《Materials and Manufacturing Processes》2007,22(6):705-709
Mesostructured lamellar zirconia was synthesized in the hydrothermal systems using Cetyltrimethyl Ammonium Bromide (CTAB) as a template and zirconyl chloride as zirconium precursor. The as-prepared composites were characterized by X-ray diffraction (XRD), TG-DTA, and DR-UV techniques. The influences of hydrothermal aging time, total concentration of solution, different mole ratio of zirconyl chloride/surfactant, and post treatment on the structure of mesostructured lamellar zirconia were discussed in this article. 相似文献
80.
Analytical approaches for modeling aging viscoelastic behavior of concrete include the time–shift approach (analogous to time-temperature
superposition), the solidification theory, and the dissolution–precipitation approach. The aging viscoelastic properties of
concrete are generally attributed solely to the cement paste phase since the aggregates are typically linear elastic. In this
study, the aging viscoelastic behavior of four different cement pastes has been measured and modeled according to both the
time–shift approach and the solidification theory. The inability of each individual model to fully characterize the aging
viscoelastic response of the materials provides insight into the mechanisms for aging of the viscoelastic properties of cement
paste and concrete. A model that considers aging due to solidification in combination with inherent aging of the cement paste
gel (modeled using the time–shift approach) more accurately predicted the aging viscoelastic behavior of portland cement paste
than either the solidification or time–shift approaches independently. The results provide evidence that solidification and
other intrinsic gel aging mechanisms are concurrently active in the aging process of cementitious materials. 相似文献