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现行标准GB5231-GB5235-85中共有88个合金牌号要求测定铜量,其含铜量从53%到99.97%以上。本文就ISO、GB和主要铜材生产企业分析规程中铜量测定方法,结合本人的实践经验进行综述。 相似文献
53.
热处理对制备纳米氧化铟锡(ITO)粉末的影响 总被引:9,自引:0,他引:9
以共沸蒸馏工艺辅助的共沉淀法制备了纳米氧化铟-氧化锡(ITO)粉体,研究了不同热处理温度对制备粉体的影响,结果表明,随着热处理温度的提高,粉体发生从四方结构向体心立方结构转变,晶粒出现长大现象,比表面积变化明显,化学组分保持高纯状态,综合比较,在700~800℃进行热处理可以得到尺寸均匀,晶形完整的纳米级粉体。 相似文献
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Effects of blending on surface characteristics of copper corrosion products in drinking water distribution systems 总被引:1,自引:0,他引:1
Copper scales formed over 6-months during exposure to ground, surface and saline waters were characterized by EDS, XRD and XPS. Scale color and hardness were light red-brown-black/hard for high alkalinity and blue-green/soft for high SO4 or Cl waters. Cl was present in surface or saline copper scales. The Cu/Cu2O ratio decreased with time indicating an e transfer copper corrosion mechanism. Cu2O, CuO, and Cu(OH)2 dominated the top 0.5-1 A° scale indicating continuous corrosion. Cu2O oxidation to CuO increased with alkalinity, and depended on time and pH. Total copper release was predicted using a Cu(OH)2 model. 相似文献
56.
用动电位伏安法,动电位光电流测量,表面膜的阴极还原和XRD分析等手段研究了铜在含或不含人血清白蛋白的模拟宫腔液(pH=7)中的电化学和光电化学行为,在不含白蛋白的模拟宫腔液中,铜电极表面生成的Cu2O呈n型光响应;一定量白蛋白存在时使Cu2O的光响应从n型转为p型,Cu2O在模拟宫腔液中呈n型光响应可归因于氯离子对Cu2O的掺杂,白蛋白排斥氯离子对Cu2O的掺杂,使其光响应从n型转为p型。 相似文献
57.
潘锦华 《特种铸造及有色合金》2005,25(11):689-691
介绍了五台山铜塔铸造工艺,由于其结构特殊,故采用了3种工艺分别铸造而成:细砂湿模造型、树脂砂毁模贴皮造型和熔模铸造.介绍了铜塔表面化学着色技术.铜塔铸造工艺对其他相似艺术铸品具有一定的借鉴价值. 相似文献
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We present a comprehensive computational analysis of the deformation of ultrafine crystalline pure Cu with nanoscale growth twins. This physically motivated model benefits from our experimental studies of the effects of the density of coherent nanotwins on the plastic deformation characteristics of Cu, and from post-deformation transmission electron microscopy investigations of dislocation structures in the twinned metal. The analysis accounts for high plastic anisotropy and rate sensitivity anisotropy by treating the twin boundary as an internal interface and allowing special slip geometry arrangements that involve soft and hard modes of deformation. This model correctly predicts the experimentally observed trends of the effects of twin density on flow strength, rate sensitivity of plastic flow and ductility, in addition to matching many of the quantitative details of plastic deformation reasonably well. The computational simulations also provide critical mechanistic insights into why the metal with nanoscale twins can provide the same level of yield strength, hardness and strain rate sensitivity as a nanostructured counterpart without twins (but of grain size comparable to the twin spacing of the twinned Cu). The analysis also offers some useful understanding of why the nanotwinned Cu with high strength does not lead to diminished ductility with structural refinement involving twins, whereas nanostructured Cu normally causes the ductility to be compromised at the expense of strength upon grain refinement. 相似文献
60.
A. Santos P. Yustos A. Quintanilla G. Ruiz F. Garcia-Ochoa 《Applied catalysis. B, Environmental》2005,61(3-4):323-333
Catalytic wet oxidation of phenol as a model pollutant has been performed in a three phase fixed-bed reactor (FBR) by using a commercial catalyst based on copper oxide in order to analyze the variables affecting significantly the copper leaching. It has been found that temperature has an almost negligible influence in the range studied (70–160 °C). On the contrary, an important effect of the pH value was noticed. The copper leaching reduces when the pH of the solution fed to the reactor increases, being almost negligible at pH ≥ 5. Moreover, the composition of the reaction media also influences the leaching. Higher copper concentrations than those expected by the effect of the acid aqueous media have been measured in the reactor effluent when phenol, catechol, hydroquinone, p-benzoquinone and maleic acid are present in the reaction media. On the contrary, oxalic acid has a negative influence on the leaching, since it captures the copper in solution to form copper oxalate which precipitates on the catalyst surface. For a previously acidified medium, the acetic and formic acids do not have any other effect on the copper leaching. It has been also demonstrated that as copper in solution decreases, so does phenol conversion, because the homogeneous catalysis contributes significantly to the oxidation reactions even in fixed-bed reactors. 相似文献