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31.
聚苯硫醚酰胺的合成与表征 总被引:7,自引:1,他引:6
用4-氯苯甲酰4′-氯苯胺和硫化钠为原料在常压下合成了聚苯硫醚酰胺,并对其进行了表征。结果表明所合成的产物为结晶性聚合物,并且有较高的热稳定性。 相似文献
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This study provides experimental evidence for proton and hydrogen formation caused by the anodic electropolymerization of cyclohexyl benzene (CHB), which is a popular electrolyte additive for overcharge protection of lithium-ion batteries (LIBs). It is found that considerable H2 evolution is observed in overcharged LiCoO2/graphite cells, especially when CHB is included as an electrolyte additive. In order to confirm the proton generation during the CHB oxidation, Pt/Pt-rotating ring disc electrode (RRDE) measurements are performed in 1 M Li(C2F5SO2)2N ethylene carbonate/ethyl methyl carbonate (1/2, v/v) solutions with and without CHB. The cathodic ring current is intimately correlated to the anodic disc current, and the cathodic reaction at the ring is determined to be the reduction of the proton. The proton generation efficiency during the CHB oxidation is as high as 90%. Proton liberation is also observed during the anodic decomposition of the electrolyte solvents, although it occurs in a much less stoichiometric way compared with that during the CHB oxidation. 相似文献
34.
Michael Maiwald Hongping Li Thorsten Schnabel Kay Braun Hans Hasse 《The Journal of Supercritical Fluids》2007,43(2):267
On-line NMR spectroscopy can beneficially be applied to studies of supercritical and near-critical fluids as an alternative to optical spectroscopy. Up to now high pressure NMR experiments are predominantly accomplished using custom made NMR batch reactors. The authors present a novel high pressure cell with displacement plunger for on-line NMR experiments on compressible fluids which can be used in conjunction with commercially available SCF NMR flow probes. The on-line technique offers advantages compared to stopped flow techniques such as enhanced control of mixture composition and reaction parameters as well as the facility of engagement into the reaction. The new apparatus is used for NMR studies on hydrogen bonding of methanol in near critical and supercritical carbon dioxide up to 403 K and 35 MPa for which data on the chemical shift of the hydroxyl group and methyl group are reported and interpreted. 相似文献
35.
In order to increase the efficiency of waste utilization in thermal conversion processes, pre-treatment is advantageous. With the Herhof Stabilat® process, residual domestic waste is upgraded to waste-derived fuel by means of biological drying and mechanical separation of inerts and metals. The dried and homogenized waste-derived Stabilat® fuel has a relatively high calorific value and contains high volatile matter which makes it suitable for gasification. As a result of extensive mechanical treatment, the Stabilat® produced is of a fluffy appearance with a low density. A two-stage gasifier, based on a parallel-arranged bubbling fluidized bed and a fixed bed reactor, has been developed to convert Stabilat® into hydrogen-rich product gas. This paper focuses on the design and construction of the configured laboratory-scale gasifier and experience with its operation. The processing of low-density fluffy waste-derived fuel using small-scale equipment demands special technical solutions for the core components as well as for the peripheral equipment. These are discussed here. The operating results of Stabilat® gasification are also presented. 相似文献
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气体分馏装置原料液化石油气 (LPG)中有机硫化物形态复杂 ,考察分析工业装置精丙烯硫化物含量变化难度大。利用Hysys模拟 ,分析判断LPG中小分子有机硫化物在气体分馏产品的分布并提出了控制措施。考虑操作条件对精丙烯硫含量的影响 ,并对工业装置精丙烯总硫超标原因进行了分析。 相似文献
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介绍65t/h煤粉炉的基本概况和存在的问题,详细阐述了采用水平浓缩煤粉燃烧技术对原燃烧器的改造过程,对改造前后运行参数及经济效益进行了对比。 相似文献
40.
为探索山丘地区中小型泵站技术改造的经验,选定南康县四个小型泵站作为泵站改造的试点站,进行现场测试,根据测试成果,分析各站存在的问题及效率偏低的原因,并拟定各站技术改造的措施,经实施后取得了较好的效果,本文就南康县泵站改造的实际效果阐明泵站改造的必要性及其改造过程中值得注意的问题。 相似文献