自升式钻井平台DCS集成配置的研究

自升式钻井平台DCS（集散系统）是平台自动化控制的核心,该系统可以实现对整个平台及其重要设备的状态监测、控制、报警、记录等功能。本文对现有部分自升式钻井平台的DCS配置情况进行分析,致力于形成一种功能相对完善,配置相对合理的集成配套形式,可为自升式钻井平台项目DCS的搭建提供一个有益参考。     

火力发电厂仪用压缩空气带水带油探究

采用系统分析、数学及物理计算的方法,对火电厂仪用压缩空气带水带油的原因进行论证,找出最主要原因,并有针对性地采取了预防和改造措施,对改造效果进行了分析与总结。     

略论对外汉语同义语汇

在汉语词汇学界,同义词一直是汉语词汇学研究争论的焦点,对同义词的研究也极为详尽和全面,但在对外汉语教学领域中的同义词教学还需要探索,本文从对外汉语教学角度出发,提出了对外汉语同义语汇的概念,它比汉语学界的同义词要宽泛,并探讨了它的收词范围和辨析方法。     

长株潭城市群郊野山区旅游开发的理论思考与实证分析

文章以长株潭城市群"两型社会"为目标引领,以城乡统筹理论为实践指导,系统分析了长株潭城市群郊野山区发展旅游休闲的可行性与必要性。在此基础上,以金龙天池民族生态乐园旅游开发为实际案例,详细探讨了长株潭城市群郊野山区旅游休闲开发应遵循的原则与应注意的问题。     

基于小波分析和遗传神经网络的模拟电路故障诊断方法*

针对BP网络极易收敛于局部极小点与过拟合等缺点,在构建小波神经网络的基础上,提出用遗传算法优化BP神经网络的模拟电路故障诊断方法.该方法使用小波作为预处理工具,经PCA分析和归一化后提取输出信号的能量信息作为特征向量,用遗传BP神经网络作为故障识别器,对模拟电路故障进行诊断.与传统BP神经网络相比较,结果表明,该方法可明显改善神经网络结构、提高故障诊断的精度和速度.     

Water as a Promoter of the Complete Oxidation of Volatile Organic Compounds over Uranium Oxide Catalysts

The effect of water addition on the complete oxidation of benzene and propane VOCs by uranium oxide catalysts has been investigated. Benzene oxidation was studied using a silica supported U₃O₈ catalyst. Complete oxidation is promoted by the addition of 2.6% water compared with the reactivity when no water is added to the reactant feed. Increasing the water concentration to 12.1% resulted in a suppression of oxidation activity. Investigation of propane oxidation using U₃O₈ shows a dramatic promotion of activity. Propane conversion was ca. 50% at 600 °C without added water, whilst it increased to 100% at 400 °C with the addition of 2.6% water. A comparison of oxidation activity has been made with Mn₂O₃, an oxide recognised for complete oxidation. In contrast to the U₃O₈ catalysts the addition of 2.6% water suppresses the activity of Mn₂O₃. In situ powder X-ray diffraction studies showed that the bulk U₃O₈ structure was stable under all the reaction conditions. The origin of the increased activity is not clear but may be due to modification of the catalyst surface and the contribution from new reaction pathways such as steam reforming.     

Two new aluminophosphates, IST-1 and IST-2: First examples of a dual templating role of water and methylamine in generating microporous structures

This study is aimed at exploring the ability of very small sized N-bearing molecules to generate and stabilize microporous aluminophosphates. Two new AlPO₄-n materials, called IST-1 and IST-2, have been obtained in aqueous media using, as main template, methylamine (MA), directly added, or generated in situ from methylformamide (MF) degradation. While IST-1 topology proved to be novel, IST-2 appears structurally related to AlPO₄-53(A). The obtained materials were characterized by powder XRD, TG/DSC, SEM and solid-state NMR. Tetraalkylammonium (TEA) cations were used as potential co-templates but only MA and water were found incorporated in the pore volumes of both structures, which argues for their true templating role. In IST-1, ¹³C solid-state NMR studies showed that half of MA species, presumably protonated, is H-bonded to framework oxygens while the other half surprisingly bonds directly to framework Al atoms. ¹³C NMR showed that only protonated MA occurs in IST-2 channels. TEA⁺ cations definitely do not play any specific template role. They indirectly favor the crystallization of IST-1 or IST-2 devoid from other crystalline or amorphous side phases, by interacting with part of the Al and P in solution and forming soluble [AlPO₄(OH)]–[TEA,HMA] complexes, substantially modifying the compositions of gels precursors to each phase during nucleation and/or growth steps. While both IST-1 and IST-2 crystallize from gels of similar initial compositions, it was demonstrated that the new MA/T ratio (T = Al or P) obtained after in situ complexation was the key parameter that specifically governs the crystallization of each phase.     

Loss of Curing Agent During Thin Film (Droplet) Curing of Thermoset Material

Recently, it has been reported by our group and others^1.2 that loss of curing agent is encountered during the curing of small droplets or thin films of amine cured epoxies. In our earlier study³ results were reported on loss of curing agent in small droplets used in conducting the rnicrobond, single fiber test for determination of interfacial shear strength (ISS). It was reported that use of a volatile curing agent (meta-phenylene diamine (m-PDA) with DGEBA resin) resulted in increasing amounts of curing agent being lost (as measured by T₈ of the cured droplets) with decreasing droplet size during the processing procedure. Droplets smaller than 150 micrometers were seen to lose up to 40% of the curing agent leading to alteration of the mechanical properties of the droplet and, therefore, causing measured values of ISS to be exceedingly low. Use of a less volatile curing agent (Jeffamine 700, a polyether diamine, Texaco Specialty Chemicals) in combination with DGEBA resin produced results which indicated that loss of curing agent was not occuring. This study was undertaken to show the relationships between film (or droplet) size and the amount of curing agent lost (during the processing) for three different aminecured epoxy systems.     

A synthetical development approach for rehabilitation assistive smart product–service systems: A case study

Digital transformation (DT), the combination of information, computing, communication and connectivity technologies, which has triggered an effective upgrade of different aspects of market strategy, customer experience etc. Nowadays, rehabilitation assistive devices (RADs) are evolving to be more digital, intelligent and personalized. Digitalization and servitization have fostered to an emerging business model—the smart product–service system (Smart PSS). Therefore, DT of the RADs’ industry advocates not only the design of products and functions, the more important is the management of service processes and resource integration. With the increase in the elderly and disabled population, the requirement for RADs is becoming more urgent. However, research on Smart PSS for RAD is still limited. The rehabilitation assistive smart product–service systems (RASPSS) was introduced into the development of RADs based on the “Design and Management of DT” strategy through the service design of assistive devices and user requirements analysis. Further, an integrated design of RAD and Smart PSS has been created, a development method of RASPSS proposed, the theoretical model of the Smart PSS based on RADs built. To specify the service framework, this case study discusses the development of a home rehabilitation assistive system for femoral stem fracture patients. This paper evaluates the usability of the system, the results of which prove usability and effectiveness of the RASPSS development method. The RASPSS development model is designed to meet needs of stakeholders, improve the user rehabilitation experience, promote the service innovation of Smart PSS, bring certain market benefits of rehabilitation aids and create social value.     

Er-doped SiO2–Al2O3 thin films prepared by the sol–gel route

The synthesis of homogeneous and pure silica–alumina binary glasses doped with rare-earth (RE) ions such as Er³⁺ is currently a key challenge for the development of integrated optics devices such as lasers, optical amplifiers or waveguides. In this study Er³⁺-doped SiO₂–Al₂O₃ films were prepared by the sol–gel route. Aluminium sec-butoxide, Al(O-sec-C₄H₉)₃ (ASB), and tetraethoxysilane, Si(OC₂H₅)₄ (TEOS), were used as glass oxide precursors, whereas erbium was introduced as Er(NO₃)₃. The alumina content in the silica matrix was 10 at.%, while erbium doping ranged between 200 and 5000 ppm. The preparation of the starting sol–gel solution and the layer deposition by a dip-coating procedure were performed in dry-box under nitrogen atmosphere. The obtained films were subsequently annealed in air between 300 and 1000 °C. After treatment at 500 °C, layers 200 nm thick were obtained. The composition, microstructure and surface morphology of the films were investigated by X-ray photoelectron spectroscopy (XPS), secondary-ion mass spectrometry (SIMS), glancing incidence X-ray diffraction (GIXRD) and atomic force microscopy (AFM). Crack-free, transparent, high purity films were obtained, characterised by compositional and microstructural homogeneity.