Aeroelastic stability of heated functionally graded cylindrical shells containing fluid

The article is concerned with the analysis of panel flutter of heated circular clamped cylindrical shells made of functionally graded (FG) material, which are subject to a simultaneous action of the external supersonic gas flow and the internal flow of ideal compressible fluid. The effective properties of the material change throughout the thickness of the shell according to a power law and depend on temperature. The aerodynamic pressure is calculated based on the quasi-static aerodynamic theory. The behavior of the fluid is described in the framework of the potential theory. A mathematical formulation of the dynamic problem for elastic structure is developed based on the classical theory of shells and the principle of virtual displacements. Based on the results of numerical simulation the influence of different consistencies of the examined FG materials, thermal load, and internal flow velocity on the boundary of aeroelastic stability is analyzed.     

Single-walled carbon nanotubes modified carbon ionic liquid electrode for sensitive electrochemical detection of rutin

The single-walled carbon nanotubes (SWCNTs) modified carbon ionic liquid electrode (CILE) was designed and further used for the voltammetric detection of rutin in this paper. CILE was prepared by mixing graphite powder with ionic liquid (IL) 1-butyl-3-methylimidazolium tetrafluoroborate and liquid paraffin together. Based on the interaction of SWCNTs with IL present on the electrode surface, a stable SWCNTs film was formed on the CILE to get a modified electrode denoted as SWCNTs/CILE. The characteristics of SWCNTs/CILE were recorded by different methods including cyclic voltammetry, electrochemical impedance spectroscopy and scanning electron microscopy. The electrochemical behaviors of rutin on the SWCNTs/CILE were investigated by cyclic voltammetry and differential pulse voltammetry. Due to the specific interface provided by the SWCNTs-IL film, the electrochemical response of rutin was greatly enhanced with a pair of well-defined redox peaks appeared in pH 2.5 phosphate buffer solution. The oxidation peak currents showed good linear relationship with the rutin concentration in the range from 1.0 × 10^− 7 to 8.0 × 10^− 4 mol/L with the detection limit as 7.0 × 10^− 8 mol/L (3σ). The SWCNTs/CILE showed the advantages such as excellent selectivity, improved performance, good stability and it was further applied to the rutin tablets sample detection with satisfactory results.     

多室内环流反应器中液体循环量的试验验证与模拟

目的 对液相氧化脱硫多室内环流反应器液体循环量的影响因素进行模拟和验证。方法 采用CFD数值模拟,基于欧拉-欧拉多相流模型,对液相氧化脱硫多室内环流反应器进行气液两相流模拟,考查了酸气流量和空气流量对液体循环量的影响。结果 利用数值模拟得到的液体循环量与利用靶式流量计测得的液体循环量误差小于10%。当酸气中H₂S体积分数不超过3%时,液体循环量(z)与酸气流量(x)、空气流量(y)之间的关系式为：z=-474.996+0.358x+0.487 3y。结论 欧拉-欧拉两相流模型能够准确地预测液相氧化脱硫反应器内液体循环量。     

铁电驻极体-液晶高弹体光电转换器性能分析

基于在紫外光照下可变形的液晶高弹体与铁电驻极体材料,设计了一种光电转换器模型器件。该模型器件能实现在紫外光照射下的电信号输出功能。建立了光电耦合分析模型,并分析了紫外光光强对产生感应电荷的影响。结果表明,该模型器件可指导开发一种能够测量一定光强范围内紫外光强度的光电传感器。     

乳化基质自然储存失稳机理研究

为更有效研发高稳定性乳化基质,避免因乳胶基质失稳造成的生产和工程安全事故,务必深入研究乳化基质自然储存失稳机理。首先总结一般乳液的五大失稳机理:分层、絮凝、相反转、奥氏熟化和聚合,理论分析了乳化基质的失稳的机理可能为奥氏熟化和聚合。然后对制备的三种乳化基质进行自然储存和高低温循环实验,并使用激光粒度仪全程检测平均粒径变化。实验结果可知三种乳化基质的平均粒径都在±0.2μm范围内变化,属于仪器测试误差。则乳胶基质的平均粒径在老化过程中无变化,计算可知乳化基质不存在奥氏熟化和聚合过程。最后使用显微镜观测到乳化基质析晶的三个过程:晶核生成、晶体生长、晶体聚集。因此,乳化基质在自然储存老化过程中,不存在分层、絮凝、相反转、奥氏熟化和聚合,主要失稳机理是内相过饱和无机盐水溶液的析晶。     

某牌号低活化马氏体钢 U 形件成形工艺研究

目的为商用聚变堆包层第一壁生产提供新的加工思路和参考方法。方法在不同工艺参数条件下进行了某牌号低活化马氏体钢U形件的成形实验;分析了挤压温度、挤压速度和圆角半径对某牌号低活化马氏体钢U形件成形效果的影响。结果试件的尺寸精度达到要求,U型流道直壁厚度尺寸误差不大于7.6%,直壁高度误差不大于8.0%,截面面积误差小于4.5%,保证了流道的等截面性。结论该工艺提高了试件的成形尺寸精度和材料的利用率,具有较大的理论和实践意义。     

高性能制动系统用炭纤维增强炭和SiC双基体(C/C-SiC)复合材料

C/C-SiC制动材料具有密度低、耐高温、制动平稳、摩擦因数高、磨损少和环境适应性强等优点,是一种能满足高速高能载制动的高性能轻质材料。本文以针刺炭纤维整体毡为预制体,采用化学气相渗透法制备C/C多孔体,然后熔融渗硅制得C/C-SiC材料;研究了C/C-SiC材料的组织结构、力学性能及其失效模式、摩擦磨损性能及机理,同时介绍了中南大学研制的C/C-SiC制动材料的应用现状。     

基于地下水流动地埋管热作用距离分析研究

地埋管换热器周围温度场随着运行时间变长不断向远处扩散,地下水流动使得埋管热作用距离沿流动方向大大增加。通过饱和含水层内地埋管换热模型,得到了地下水流动作用下埋管热作用距离的近似表达式,分析了地下水流速、土壤导热系数和孔隙率对热作用距离的影响。借助于地埋管热作用测试平台,分析了地下水流动作用下埋管热作用距离和热恢复特性,结果表明：地下水流动使得埋管热作用距离远大于纯导热模式,且热作用距离在埋管轴向不同埋深处大小不一,建议在地下水流速大于1×10-6m/s的地质区域,沿地下水流动方向设置埋管间距为8~10m。